State of the Art Report COMBINED USE OF NDT
Transkript
State of the Art Report COMBINED USE OF NDT
State of the Art Report COMBINED USE OF NDT/SDT METHODS FOR THE ASSESSMENT OF STRUCTURAL TIMBER MEMBERS Editors: José Saporiti Machado and Mariapaola Riggio & Thierry Descamps State of the Art Report COMBINED USE OF NDT/SDT METHODS FOR THE ASSESSMENT OF STRUCTURAL TIMBER MEMBERS Edited by José S. Machado Mariapaolla Riggio Thierry Descamps Year of publication: 2015 ISBN 978-87325-094-2 This publication is supported by COST Published by: UMONS - Université de Mons No permission to reproduce or utilise the contents of this book by any means is necessary, other than in the case of images, diagrammes or other material from other copyrights holders. In such cases, permission of the copyright holders is required. Disclaimer The views and propositions expressed herein are those of the respective authors and, unless otherwise stated, not represent the official view of COST Association or any organisation mentioned in this report. Also they are not responsible for the use which migth be made of the information and for the external websites referred in this publication. PREFACE COST Action FP1101 ‘‘Assessment, Reinforcement and Monitoring of Timber Structures” is a research network established under the support of the European framework supporting trans-national cooperation in different scientific domains across Europe (COST). The main objective of COST Action FP1101 was to increase the acceptance of timber in the design of new structures and supporting the safety and serviceability of existing structures. For these purposes this Action supported a series of activities (short-term scientific missions, training courses, workshops and conferences) aiming to develop and disseminating methods to assess, reinforce and monitor timber structures. This state of the art report has been prepared by the Working Group 1/Task Group 2: “Combination of NDT/SDT for the assessment of timber structures on site”. The present report is divided in four broad themes that describe some of the achievements and reflections among research groups in the last decades in several topics related to the scope of TG2 : • Part I includes general matters related to the use of NDT/SDT methods such as calibration, reliability of field measurements, statistical approaches to derive properties, as well as to update and combine information from different sources; • Part II includes the application of NDT/SDT methods for predicting the socalled reference properties and also specific methods aimed at determining other mechanical/physical properties whose estimation is important for the assessment of particular problems associated to timber members; • Part III deals with issues fundamental to the evaluation of the nature, extent and causes of local features that can induce failures, damage and vulnerabilities (e.g. aging, mechanical damage, delamination, fissures and biological deterioration); • Part IV includes a group of chapters highlighting the application of NDT/SDT methods in specific contexts. Editors are indebted to the COST Action FP1101, and to all authors, reviewers and COST members who contributed to the preparation of this report. The Editors José S Machado Mariapaola Riggio Thierry Descamps Leader of Task Group 2 Leader of Working Group 1 “Assessment of Timber Structures” Short Term Scientific Missions officer CONTENTS PART I – ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Reliability of prediction by combining direct and indirect measurements José S. Machado 1 Standardization of non-destructive methods in the assessment of existing timber structures Guillermo Íñiguez-González, Francisco Arriaga, Miguel Esteban, Daniel F. Llana 15 Multi sensor approach combined with multivariate analysis for assessment of timber structures Jakub Sandak, Anna Sandak, Mariapaola Riggio 23 Hierarchical modelling of timber reference properties using probabilistic methods: Maximum Likelihood Method, Bayesian Methods and Probability Networks Hélder S. Sousa, Jorge M. Branco, Paulo B. Lourenço 33 Quantitative assessment of the load-bearing capacity of structural components using NDT, SDT and DT inspection methods Gerhard Fink, Jochen Köhler 45 PART II – ASSESSMENT OF REFERENCE PROPERTIES Methodology and protocols for routine assessment of wooden members with spectroscopy Anna Sandak, Jakub Sandak, Mariapaola Riggio 53 Structural analysis of porous media by means of thermal methods: Theory and monitoring measurements Olivier Carpentier, Thierry Chartier, Emmanuel Antczak, Thierry Descamps, Laurent Van Parys 61 Prediction of mechanical properties by means of semi-destructive methods Michal Kloiber, Miloš Drdácký 69 Practical procedure for estimating the density of timber with portable X-ray equipment Thomas Lechner, Roger Kliger 93 A methodology for the determination of the timber density through the statistical assessment of ND measurements aimed at in situ mechanical identification Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo 107 Evaluation of the influence of defects on the mechanical properties of timber through the analysis of multiscale specimens, based on NDT and DT Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo 111 Screw withdrawal resistances for reliability-based evaluation of timber in existing structures Nobuyoshi Yamaguchi 115 Combined method for the in situ mechanical identification of ancient timber based on NDTs Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo 131 Combine information from visual and NDT/SDT methods Artur Feio, José Saporiti Machado 137 Assessment of timber floors by means of non-destructive testing methods Tiago Ilharco, Thomas Lechner, Tomasz Nowak 145 PART III – ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Application of imaging techniques for detection of defects, damage and decay in timber structures on-site Mariapaola Riggio, Jakub Sandak, Steffen Franke 163 Assessing the integrity and strength of gluelines Philipp Dietsch, Thomas Tannert 175 Mapping of cracks in glulam beams and assessing the effect of environmental conditions Philipp Dietsch 189 Estimation on-site of decay in timber structures by means of pene tration methods Alessandra Gubana, Ezio Giuriani 203 PART IV – CASE STUDIES Assessment through NDT of the state of timber structures of the historic buildings of Catalonia Marcel Vilches Casals, Carles Labèrnia Badia, Vladimir Rodríguez 209 SDT methods as part of a conservation process Dulce Franco Henriques, André Santiago Neves 217 Advanced model based assessment of existing structures Kiril Gramatikov, Toni Arangjelovski, Marija Docevska 223 PART I ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Reliability of prediction by combining direct and indirect measurements José S. Machado Department of Structures, LNEC, Portugal, [email protected] Abstract Several non and semi-destructive testing (NDT and SDT) methods have already been developed for in situ assessment of structural timber member’s properties or deterioration level. The use of these methods as auxiliary tools to the traditional visual strength grading method can only be current if a fully comprehension of their limitations and reliable exploitation of their possibilities is achieved. This chapter discusses the possibility of obtaining more reliable predictions by combining information from NDT and SDT methods taking into account possible sources of uncertainty. SDT methods can provide direct measurements of a desired wood’s property (e.g. density or mechanical properties) and then be used to cross-validate the information obtained from indirect measurements (e.g. drilling resistance, stress wave velocity). The discussion is based on an example of prediction of bending modulus of elasticity through the combined information obtained from a stress wave NDT and a tension SDT method. Introduction Structural timber members present a high variability of properties (between and within members) being influenced by various variables. Among these variables wood species, density, defects and moisture content are the ones mostly taken into account during the survey of timber structures. Considering the large spectrum of variables involved and the difficulties in assessing their influence on the global mechanical behaviour of a structural timber member, several non and semidestructive testing (NDT and SDT, respectively) methods have been developed. The description and limitations of these methods were already analyzed in recent reports [1, 2]. Visual strength grading (VSG) was the first NDT to be developed and is still the basic tool used in the assessment of timber structural members. VSG provides reliable results (meaning over conservative) and a long-term experience of its application in situ. However these over conservative values lead often to the demoli- 1 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS tion of structures showing no signs of damage or deformation after several years (in some cases centuries) in service. To support expert’s decision other NDT and SDT methods were developed as auxiliary tools to VSG for the allocation of more reliable (meaning closest to the real value) mechanical characteristics to structural timber members in situ. However several shortcomings explains why their applications is limited and the final decision is still based solely on expert’s opinion and application of a simplified set of visual rules. NDT and SDT methods can be differentiated based on the type of information provided: • Local (limited to a small volume of the element) or global (all volume of the element). • Direct measurement or an indirect measurement of the desired property (density, strength, stiffness). • Qualitative or quantitative measurements. In the present chapter direct methods are the ones that provide a direct evidence of the mechanical or physical property of a wood member under examination. This definition includes methods that although providing a direct reading will require further information in order to extrapolate local to global behaviour. Other meaning is found in literature considering direct methods those not involving the need for empirical models (e.g. tension of micro-specimens) [3]. Direct methods can include the removal or not of wooden material. Proof-loading is an example of a NDT method capable of deliver a direct measurement of the global modulus of elasticity of timber beams in service [4]. However this method can only be applied in certain situations [5]. In some cases the removal and testing of structural members in the laboratory provides a direct information that can increase the reliability of NDT/SDT predictions. However this destructive procedure is dependent upon the possibility of removal of timber members (e.g. not suitable in historic structures) and results have again to take into account the gross wood’s variability between members. Direct assessment of physical and mechanical properties can be obtained by some SDT [6]. Indirect methods (NDT or SDT) are frequently applied in situ based on uni or multivariate empirical models (e.g. regression analysis) linking indirect measurements (e.g. ultrasonic modulus of elasticity, drilling resistance) to desired properties (e.g. static modulus of elasticity, density). Unfortunately on most cases the existent regression models are characterized only by its coefficient of determination and nothing is mentioned about the uncertainty of the different models. Wood complexity and general difficulties associated to performing measurements in situ require a careful planning of the inspection works. This should begin always by settling on the property or properties to predict. Given a certain property the second step includes the choice regarding: NDT&SDT methods to apply; locations of testing; number of data to obtain from each method; and, suitable data analysis procedures. 2 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Regarding data analysis it should be considered the restrictions regarding extraction of samples which only allows that only a few samples can be obtained and analyzed (small sample size). Also the majority of NDT and SDT methods provide local properties and only concern clear wood properties. For the prediction of the global behaviour of a timber member these information needs to be combined with information from defects (mostly knots and slope of grain). The present chapter discuss the possible improvement of the reliability of predictions based on the combination of NDT and SDT methods. NDT/SDT methods Indirect estimators Direct estimators Material properties Core Density Core drilling Edyn Em Stress waves Time-of-flight Tension test Etension Fig. 1. NDT&SDT methods used for predicting the static modulus of elasticity. Edyn – Dynamic modulus of elasticity; Em– Bending modulus of elasticity Core drilling (SDT), stress waves (NDT) and tension tests (SDT) are used as example for the discussion, Figure 1. The use of these methods for the prediction of two reference properties (density and modulus of elasticity) is analysed taking into account possible sources of errors, the effect of small sample size, the high spatial variation of properties inside a timber member and possible error propagation. Joint use of direct and indirect measurements As for other material a more precise and accurate assessment of timber members in situ can be achieved by joining information from different sources [7]. This combination of information can be done by: 3 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS • considering both as independent variables in a common empirical model (e.g. multiple regression analysis); • using direct readings to calibrate the indirect readings made in situ. This calibration includes validation of prior regression models as well as to quantify adjustment factors (e.g. wood moisture); • using both data as independent predictions of the property – possibility of cross-validation of the prediction. • using first a fast technique as a preliminary screening of the structure followed by a second time-consuming technique in areas selected from the results of the first technique (e.g. thermography followed by drilling resistance for assessing presence and extension of decay). Although considered above as autonomous paths they can in fact act together. Uncertainties involving in situ evaluation Whatever the path followed it must be bear in mind that predictions are always affected by errors, including aleatory (high spatial variability inside a timber member – within the cross section and length) and epistemic errors (lack of knowledge on the material or models, associated to the test method and human errors). These errors lead to a certain degree of uncertainty of the prediction made using NDT and SDT “…the estimate of even single parameters using established methods can be contaminated by significant errors and caution must be exercised in interpreting experimental data.” [8]. The awareness of the type of error is only important as a mean to recognize what are the possibilities to diminish the amount of error. In the assessment of existing elements the uncertainty can be considered as epistemic (the errors are only due to our incapacity to get the necessary information, to deal with human errors or to apply the correct test methods) [9]. Wood’s variability (aleatory error) can as a rule of thumb be considered known using the values provided in Table 1. These values should be regarded as start up values possible to be adapted to any particular situation (type or quality of wooden members, amount of information possible to be collected on site). Table 1 Coefficients of variation for clear wood and structural timber Property Clear wood [10] Structural timber [11]1) Density 10 10 Tension strength parallel to grain 25 30 Bending strength 16 25 Compression strength parallel to grain 18 20 Modulus of elasticity in bending 22 13 1) Values for European softwood and corresponding to a number of tests equal to 10 4 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS This uncertainty is always present since the number of samples or measurements possible to be made are limited and the extrapolation process (local to global assessment) is always complex given the nature of a timber member – heterogeneous, anisotropic and hygroscopic. The limitations associated to the different NDT and SDT methods usually applied are described in a recent report [2]. Uncertainties associated to NDT/SDT methods Density prediction using core drilling Density is an important property given his positive direct impact in the strength and stiffness of wood. Some of issues involved in the determination of density in situ are discussed in [8]. It is also used to predict the modulus of elasticity through the determination of the dynamic modulus of elasticity. Density can be predicted using core drilling (SDT), drill resistance (SDT), penetration resistance (SDT) and pull-out resistance (SDT) [12]. The accuracy and precision of density’s prediction model is strongly dependent on the variability showed by each individual timber member. Density’s variation occurs along its length and within the cross-section (width and depth). The error of prediction can be partially dealt if the NDT or SDT method is applied taking into consideration important characteristics of the member (namely wood species, growth ring pattern and spatial variation inside the member) and if a sufficient number of readings are collected. Statistical models allow having an estimative of error as function of the number of readings collected, Figure 2. However this error is underestimated since it does not consider a possible spatial variation which usually occurs in wood. Consequently the sample size effect on error given by models as the one illustrated in Figure 2 only provides guidance for maintaining a certain level of precision and does not ensure the accuracy of our prediction. Core drilling is a multifunction SDT method capable of providing information about wood species, moisture content, strength and density. The determination of density of core samples can be done according with standard procedures. Since the number of readings is limited (due namely to level of destruction made to the timber member) and considering the level of variability that can be found in a sole timber member the reliability of density’s prediction is highly dependent on: the number of readings; and, the way they are carried out in order to ensure a proper representativeness of the material under observation. Therefore the accuracy of this SDT method depends strongly on expert decision about where to extract and 5 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS the length of the cores whereas precision are more related with the number of cores extracted. Fig. 2. Error as function of sample size and mean density (coefficient of variation of 10%) [13] To illustrate consider a timber member with a cross-section 304 mm x 148 mm and two possible annual ring patterns (quarter-sawn and boxed heart). A quartersawn pattern (A) can be considered closest to a homogeneous section. In this example the density of each layer of latewood and earlywood is randomly generated assuming a normal density probability function using data taken from [14]. No lengthwise variation is assumed. A collection of four cores taken perpendicular to the grain and with different depths was simulated. A boxed heart pattern (B) shows a cross-section variation of density was considered from the pith to the surface. Also no lengthwise variation was considered. In old timber structures large cross-section usually contains the pith inside showing an annual growth ring pattern similar to case B. For this case a comparison was made between taking four wood cores from the edges or taking two from the edges and two from the faces. For all cases a bootstrap method was applied running 10000 iterations. Figure 3 shows the result of the different simulated cases. Figure 3 shows the importance to take into account the variation of properties inside a timber member in the prediction of density by a core drilling method. Depending on the type of growth ring pattern, cross-section variability and type of core samples (depth and extraction procedure) density prediction’s error can vary in average from 0% to 15%. An estimation of the lengthwise and cross-section variability can be obtained by using another SDT method – drilling resistance. The variation of growth ring width is another source of variability not taken into account in the present simulation. Density values are affected by moisture content and thus wooden cores they 6 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS can be dried and moisture content determined for carried out the necessary corrections. The need to apply correction factors are always a difficult issue being address in another chapter of the present publication [15]. Fig. 3. Estimated error associated with density prediction through core drilling. ∆ - cross-section variability; s – type of sampling (1 – all samples taken at the edge; 2 – two samples taken at the edge and other two on the faces) 7 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS The accuracy in density’s prediction is important since this variable will be used for predicting the dynamic modulus of elasticity or directly the mechanical properties. Other NDT/SDT methods for predicting density are available being some described in other chapters [16]. Modulus of elasticity prediction using stress waves Static modulus of elasticity can be predicted by tension and/or compression tests (SDT) [17, 18], dynamic response (NDT) [19], stress waves (NDT) and load test (NDT) [12]. The prediction of the static bending modulus of elasticity (Em) is usually obtained in situ using the correlation with the dynamic modulus of elasticity (Edyn), regression equation below. E m = a + bEdyn + ε The dynamic modulus is obtained by applying stress waves NDT methods in situ. Information about the use of stress waves for in situ assessment of structural timber can be found in [12]. Wood is an orthotropic material being the equations of motion for bulk waves given by Christoffel’s equation [13]. However considering the complexity of wood material and the experimental conditions on site a simplification is made and it is applied the equation for isotropic solids and obtaining a prediction of the dynamic modulus of elasticity (Edyn) as showed above. ( ))( 2 1 + υ 1 − 2υ Edyn = V ρ (1 − υ ) ) Considering the complexity of determining in situ the Poisson’s ratio the above simplified equation is generally applied. E dyn 2 =V ρ K (1 + υ )(1 − 2υ ) =1 (1 − υ ) Assuming K = The component of the equation regarding the coefficient of Poisson is considered a determinist value. The use of this equation is supported in different studies. Considering the values given in Table 2, for a stress applied along the grain a mean k value could probably be found between 0.39 and 0.57. Nevertheless since the uncertainties surrounding k factor (random) are merged with other uncertain8 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS ties (density and TOF measurements) and taken into account by a final regression curve the real value of k is not significant. Table 2 Average Poisson’s ratio for Softwoods and Hardwoods [22] Coefficient Softwood Hardwood vLR 0.37 (0.06) 0.37 vLT 0.42 (0.07) 0.50 vij – ration for deformation along the j axis caused by stress along the i axis TOF determination can be affected by: the lack of proper coupling between transducers and wood (wood surface roughness, lack of coupling agent); slope of grain or presence of other defects; uncertainty about wave path length [23, 24]. To minimize the error several readings (at least 5 [20]) should be carried out along the length of the beam. Regarding density small samples can be taken from timber members for determination in the laboratory. This procedure can be done through core drilling as seen in the previous section and possible errors associated were already mentioned. Finally TOF should be corrected accordingly with the temperature and moisture content of the beam. The combine information from stress waves and core drilling provide a prediction of the dynamic modulus of elasticity (Edyn). Once obtained the dynamic modulus of elasticity a prediction of the static modulus of elasticity is generally done by applying empirical models (regression curves). The correlation between this two variables can varied from 0.58 to 0.96 depending upon the dimension (clear wood or structural wood), treatment and age of timber specimens [24]. Modulus of elasticity prediction using tension strength tests Modulus of elasticity parallel to grain shows moderate dependence to type of loading being a common value used for design of timber structures. However the modulus of elasticity in compression is lower that in bending which in turn is lower than in tension [25] for structural timber elements. Nevertheless it can be considered independent of the load involved for clear wood specimens [25]. Information about the modulus of elasticity in bending of clear wood can then be obtained from tension tests carried out on small samples removed from timber members in situ [6]. This information although limited in terms of possible number of tests when compared with the possible readings obtained from stress waves can nevertheless provide us the possibility to: validate the values obtained from the indirect method; and, increase the reliability of our prediction. 9 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Combining information from indirect and direct methods To illustrate different options for combining information obtained from direct and indirect methods data from previous works will be used [26]. In these studies density and modulus of elasticity were obtained using the SDTs and NDT methods aforementioned. However before trying to combine this information they should be careful analysed. A forest plot (Figure 6) can be used to evaluate if the results of both tests are consistent (values ranging in a similar interval). Fig. 6. Forest plot showing the mean and 95% confidence intervals for the results obtained from Edyn and Et (values in N/mm2) The result obtained allows us to consider that the data obtained from the two testing methods although not coincident can be accepted as being coherent. Unfortunately the values obtained from these two methods showed a high correlation coefficient (r2 = 0.85) representing a possible conflict with one of the assumptions of regression analysis (independency of independent variables). The questions related with excessive multicollinearity does not have any standard metric and so it is a decision of the expert to make about using or not a multiple regression model in this circumstances. In the present case a Meta-analyse technique is used and the combining of information is made trough an inverse variance method, see equation bellow. −2 Ecomb = ω 1 × E1 + ω 2 × E 2 + ... + ω n × E n and ωi = σ i n n å σk k=1 Where n estimators of the variable E are combined as a weighted average according with their variance ( σ). The combined predicted value can then be used as explanatory variable (Ecomb) in a simple regression model. Two models are then available for predicting Em: one as function of Edyn (r2 = 0.72); and, the other as function of a combined value Ecomb (r2 = 0.77). The two models are very close in terms of capacity of explained the Em variability. These regression models assumed that independent variables are measured without errors and the error is only associated to the dependent variable [27]. However for the present analysis it will be taken into account also the uncertainty related with the independent variables (Edyn and Ecomb), scenario 10 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS more close to reality. For that purpose a Bayesian analysis applying a Markov Chain Monte Carlo (MCMC) method is used to drawn inferences about the models and parameters. MCMC algorithms generate a Markov chain sequence of parameter values (the values at a given state of the chain depends only upon the previous state) being these parameters generated randomly (Monte Carlo). MCMC was carried out by running Winbugs inside R software trough R2WinBUGS package (1 chain, 1000 burn-in iterations, 9000 used iterations). Figure 7 shows the prediction for beam P20 and P21. a) b) Fig. 7. Predicted Em distribution for: a) beam P20 and b) beam P21, using model Em(Edyn) – red – and model Em (Ecomb). Real stiffness showed in the graphs by a dashed vertical line For both beams considering the uncertainties of the variables it is clear that a closer approximation to the real stiffness is obtained using the combined information. Final remarks Assessment of timber structures is always done by crossing information from different sources. However this process is generally based on a series of individual results obtained from different NDT/SDT methods and that the expert uses to take an informative decision about the structural health of the structure. The possibility of combining in one single model the information provided by two independent methods, as for other materials (e.g. concrete), can lead to a more reliable prediction of that property. The need to consider the uncertainties associated to each test method, the need to understand the assumption behind a particular statistical model and finally the need to asses the robustness of the final model are also matters that should be considered. The complexity of wood makes that any final decision relies heavily on the expert capability of extracting valuable information from the test methods applied, his/ her experience and particular conditions regarding the structure under inspection. This heterogeneous information (qualitative and quantitative) makes bayesian methods a suitable data analysis method to be applied. 11 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS References [1] Dietsch P, Köhler J (2010) Assessment of timber structures. Shaker Verlag, Aacher. [2] Kasal B, Tannert T (2010) In situ assessment of structural timber. Springer. [3] Kasal, B (2013) Structural health assessment of in-situ timber – An interface between service life planning and timber engineering. In 9th Meeting of Northern uropean Network for Wood Science and Engineering (WSE). Leibniz University of Hannover. Brischke, C. & Meyer, L. (eds). p. 157-164. [4] Riggio M, Tomasi R, Piazza M (2014) Refurbishment of a traditional timber floor with a reversible technique: Importance of the investigation campaign for design and control of the intervention. International Journal of Architectural Heritage 8:74-93. [5] Srpčič J (2010) Load tests (Proof Loading). In: Dietsch P and Köhler J (Eds) Assessment of timber structures, Shaker Verlag GmbH, Aachen, p 96-99. [6] Kloiber M, Drdácký M (2014) Prediction of mechanical properties by means of semidestructive methods. In J S Machado, Mariapaola Riggio and Thierry Descamps (Eds) Combine use of ndt/sdt methods for assessment of structural timber members, this issue. [7] Verma S K, Bhadauria S S, Akhtar S (2013) Review of nondestructive testing methods for condition monitoring of concrete structures. Journal of Construction Engineering article ID 834572. [8] Kasal B (2012) State-of-the-art in situ evaluation of structural timber – some critical observations. Revista Portuguesa de Estruturas 11:79-85. [9] Kiureghian A D, Ditlevsen O (2009) Aleatory or epistemic? Does it matter?. Structural safety 31: 105-112. [10] Forest Products Laboratory (2010). Wood Handbook – wood as a engineering material. General Technical Report FPL-GTR-190. U.S. Department of Agriculture, Forest Service, Forest Products Laboratory, Madison, 508 pp. [11] JCSS (2006). Probabilistic model code. Part 3.5 – Timber. ISBN: 978-3-909386-79-6, Joint Committee on Structural Safety. [12] Höls M, Dietsch P (2010) Assessment of timber structures. In: Dietsch P and Köhler J (Eds) Assessment of timber structures, Shaker Verlag GmbH, Aachen, p 14-21. [13] Zar J H (1996) Biostatistical analysis. 3rd ed. Prentice-Hall International, Inc. [14] Fries A, Ericsson T (2009) Genetic parameters for earlywood and latewood densities and development with increasing age in Scots pine. Ann. For. Sci. 66:404 [15] Iñiguez-González G, Arriaga F, Esteban M, Llana D F (2014) Standardization of non-destructive methods in the assessment of exsting timber structures, In J S Machado, Mariapaola Riggio and Thierry Descamps (Eds) Combined use of NDT/SDT methods for the assessment of structural timber members, this issue. [16] Faggiano B, Grippa M R, Marzo A (2014) A methodology for the determination of the timber density through the statistical assessment of ND measurements aimed at in situ mechanical identification. In J S Machado, Mariapaola Riggio and Thierry Descamps (Eds) Combined use of NDT/SDT methods for the assessment of structural timber members, this issue. [17] Drdáchy M, Kloiber M (2013) In-situ compression stress-deformation measurements along the timber depth profile. Advanced Materials Research 778:209-216. [18] Kasal B, Anthony R (2004) Advances in in situ evaluation of timber structures. Progress in Structural Engineering and Materials 6:94–103. 12 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS [19] Ilharco T, Lechner T (2014) Assessment of timber floors by means of non-destructive testing methods. In J S Machado, Mariapaola Riggio and Thierry Descamps (Eds) Combine use of ndt/sdt methods for assessment of structural timber members, this issue. [20] Dackermann U, Crews , Kasal B, Li J, Riggio M, Rinn F, Tannert T (2014) In situ assessment of structural timber using stress-wave measurements. Materials and Structures 47:787-803. [21] Bucur V (1995) Acoustics of wood. RC Press, New York. [22] Bodig J, Goodman R (1973) Prediction of elastic parameters for wood. Wood Science 5:249-264. [23] Chapman M J, Norton B, Taylor J McA, Lavery D J (2006) The reduction in errors associated with ultrasonic non-destructive testing of timber arising from diferential pressure on and movement of transducers. Construction and Building Materials 20:841-848. [24] Kasal B, Lear G, Tannert T (2010) Stress waves. In: B Kasal and T Tannert (Eds) In situ assessment of structural timber. [25] Gehri E (1997) Timber as a natural composite: explanation of some pecularities in the mechanical behaviour. Case: Assessment of the modulus of elasticity of timber parallel to grain. In: Görlacher R (Ed) International Council for Building Research Studies and Documentation – Working Commission W18 – Timber Structures, Vancouver, Paper 30-6-3. [26] Machado J S, Lourenço P B, Palma P (2011). Assessment of the structural properties of timber members in situ – a probabilistic approach, in: SHATIS’11 International Conference on Structural Health Assessment of Timber Structures, Lisboa. [27] Gillard J (2010) An overview of linear structural models I errors in variables regression. REVSTAT – Statistical Journal 8:57-80. 13 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 14 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Standardization of nondestructive methods in the asssessment of existing timber structures Guillermo Íñiguez-González, Francisco Arriaga, Miguel Esteban, Daniel F. Llana ETSI de Montes, Forestal y del Medio Natural, Universidad Politécnica de Madrid, Spain. [email protected] Abstract The aim of this paper is to define the reference conditions and to propose modification factors to standardize the nondestructive variables recorded by different NDT, in order to gain uniform practical data and to develop a procedure for the standardization of timber assessment. Introduction The standardization process consists of the development of a common NDT procedure for the evaluation of structural timber properties. This process could be based on previous works (Íñiguez-González et al. 2013) and should include the following features: - Compilation of nondestructive test results from different research groups and studies, taking into account the species studied and devices used; - The creation of a standardized data sheet to compare results, based on the adjustment factors proposed; - Standardized equations. This paper therefore focuses on the second and third features. Background 2.1 Nondestructive variables The following variables are usually measured for the in situ assessment of timber 15 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS properties by means of nondestructive techniques: Time of flight (or equivalent velocity) The propagation of stress waves through material can be used to estimate its mechanical properties, mainly stiffness. Time of flight (TOF) or the equivalent velocity, is the main parameter measured. Attenuation can also be recorded and is related to strength properties. Two types of waves are used: sonic stress waves for frequencies within the audible range, and ultrasonic stress waves at frequencies above 20 kHz. Natural frequency In this method timber pieces are made to vibrate longitudinally or transversely by means of an impact in the corresponding direction. The vibration of the piece occurs primarily in the system Eigen frequencies. These frequencies are related to the stiffness properties of the piece and its dimensions/geometry. In the case of longitudinal vibration, it is also possible to obtain the equivalent velocity of stress wave transmission. Pullout resistance The pullout resistance method consists of the measurement of the withdrawal force of a screw with a known diameter inserted into a timber piece to a certain depth. This force is related to the density of the timber. Penetration depth This method is based on a similar principle to that of material hardness measurement, and it consists of measuring resistance to the penetration of a hard solid piece. Penetration depth is related to the timber density in the outer part of the piece of wood. Drill resistance This method mainly focuses on gathering data on the internal condition of timber members and trees. It uses a small diameter drill (1.5-3.0 mm) to bore into timber members while measuring resistance to penetration (energy consumed at constant velocity). Resistance to drilling is proportional to density. 16 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 2.2 Factors affecting nondestructive variables Moisture content The moisture content (MC) of timber depends on the hydrothermal conditions of the surrounding air. In a normal dry condition inside a building the MC of timber is from 8 to 12 %; this is slightly higher, 10 to 16 %, if the building is close to the coast. MC can be measured with electrical resistance equipment, according to the EN 13183-2:2002 standard. A reference value of 12% MC is usually adopted. Under usual conditions the range of MC variation is about ±4% (12±4%). Temperature In general, the mechanical properties of wood decrease when it is heated and increase when it is cooled. However, in the practical range from -10 to 50 ºC the effect is negligible; for example, in structural mechanical timber design it is assumed that the properties of timber do not change and are not affected by temperature below 50 ºC. Consequently, the effect on measured nondestructive variables is very small. Size/length The size effect may have an influence on some local nondestructive variables such as pullout resistance and penetration depth, as a consequence of the sawn pattern and cross-section size of the piece. In the case of large cross-sections, the outer wood of the cross-section usually has narrow rings, and the direction of probe penetration is more radial than it is tangential. On the other hand, small or narrow cross-section pieces may have juvenile wood in the outer part of cross-section, so that tangential penetration is possible. Wave velocity propagation is independent of frequency. But different commercial devices work at different wave frequencies, and the means used to detect signal start and stop may differ. The result is influenced by signal attenuation and therefore depends on the length and size of the piece. It is more difficult to establish a reference value for the size and length factors. Positioning of sensors/angle to the grain This factor affects the measurement of time of flight (or the equivalent wave propagation velocity). The best positioning of sensors for measurements is at each end of the piece, obtaining the velocity parallel to the grain. This is not possible in practice in existing structures because the ends of pieces are not accessible. It is therefore common practice to take measurements at an angle 17 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS to the grain, positioning the sensors on opposing faces at the maximum possible distance or, in the central portion of a span, obtaining the velocity for a certain angle. For frequent dimensions of timber pieces and cross-section slenderness (width/thickness = 1-2) and length (length/depth of the beam = 17-22) the angle with respect to the grain varies from approx. 2 to 6 º. In some situations only the lower face of the piece is accessible, and in this case sensors are placed on the same face, obtaining velocity parallel to the grain but under special conditions. 3. Standardization proposal 3.1 Reference conditions Moisture content 12% moisture content of timber is proposed as reference value to correct the nondestructive measurements (stress wave, ultrasound wave velocity and penetration depth). This value corresponds to the target MC for coniferous timber in service class 1 according to Eurocode 5 (EN 1995-1-1:2004). Service class 1 is characterized by a MC in the materials corresponding to a temperature of 20ºC and a relative humidity of the surrounding air only exceeding 65% for a few weeks per year. Temperature 20ºC is the reference value proposed in general, and according to the definition of mechanical properties in Eurocode 5. But considering its low effect on nondestructive variables this correction may be neglected in frequent variable conditions (-10 to 50ºC). Size/length The effect of size is considered here in terms of length, and 2.7 m is the proposed reference length to correct nondestructive measurements (stress wave and ultrasound wave velocity). This value is based on standard bending test slenderness (span/depth = 18) and the reference depth for bending strength of solid timber in Eurocode 5 (150 mm, 18•150 = 2700 mm). In practice length may usually be in the range from 3 to 6 m, and considering the reference value of 2.7 m the maximum effect would be a 7% variation in velocity. 18 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Positioning of sensors/angle to the grain The end to end positioning of sensors, measuring the velocity parallel to the grain, is the proposed reference position of sensors and reference angle. In practice the angle may usually be in the range from 2 to 6º, so the maximum effect would be a 6% variation in velocity. 3.2 Modification factors Moisture content The reference velocity of stress wave propagation, v12 (referred to 12% MC) may be obtained by equation 1, from velocity at H % MC, vH, vH v12 = 1 − ( H − 12) k H (1) Where kH is the adjustment factor for MC obtained as the ratio between the linear variation of velocity relative to MC (∆velocity/∆MC) related to velocity at 12% MC. A preliminary value of 0.01 (1% velocity decrease for every 1% MC increase) is proposed for this, as it is a common result in several research works. The reference depth penetration of the Pilodyn 6J Forest, P12 (referred to 12% MC) may be obtained by equation 2 from depth penetration at H %, PH, P12 = PH 1 + ( H − 12) k P (2) Where kP is the adjustment factor for MC obtained as the ratio between the linear variation (depth/MC) related to depth penetration at 12% MC. A preliminary value of 0.02 is proposed (approx. 2% depth penetration increase for every 1% MC increase) for this factor. There are other experiences suggesting that its effect be neglected for practical purposes. Temperature The reference velocity of stress wave propagation, v20 (referred to 20 ºC temperature) is obtained by equation 3 from velocity at T ºC temperature, vT, v 20 = vT 1 − (T − 20 ) k T 19 (3) PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Where kT is the adjustment factor for temperature obtained as the ratio between the linear variation of velocity relative to temperature (∆velocity/∆T) related to velocity at 20 ºC. This factor has been obtained in several research works with a value close to 0.00075 (a 0.075% velocity decrease for every 1 ºC temperature increase). In practice the temperature may usually be in the range from 5 to 35 ºC, and considering the reference value of 20 ºC the maximum effect would be 1.12 % of variation in velocity. Size/length The reference velocity of stress wave propagation, v2.7 (referred to a reference length of 2.7 m) is obtained by equation 4 from velocity at L length in m, vL, v 2.7 = vL 1 − ( L − 2.7 ) k L (4) Where kL is the adjustment factor for length obtained as the ratio between the linear variation of velocity relative to length (∆velocity/∆L) related to velocity at reference length 2.7 m. Positioning of sensors/angle of the grain The reference velocity of stress wave propagation, v0 (parallel to the grain and end to end) is obtained by equation 5, from velocity angle α in sexagesimal degrees (α ≤ 10º), v,α v0 = vα 1 − α kα (5) Where kαis the adjustment factor for angle obtained as the ratio between the linear variation of velocity relative to angle (∆velocity/∆α) related to velocity parallel to the grain and end to end. This factor was obtained in several studies with a value close to 0.01 (a 1% velocity decrease for every additional grade increase in angle deviation) for ultrasound waves (at 22 kHz). Finally, if velocity is measured only using sensors in the lower face of the piece, these values should be divided by a factor of 0.972 to obtain the velocity v0. 20 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 4. Conclusions and future work Given the lack detected in the state of the art, research work compiling nondestructive testing values measured in coniferous and deciduous species is being undertaken in Spain. This has the purpose of collecting existing test results measured in raw material and existing structures with different devices and procedures. A testing protocol has also been designed and proposed in order to make the results of future nondestructive tests by different researchers comparable. Although this study does not yet include sufficient material to propose a grading method of timber based on nondestructive testing results, it does mark the route to this goal. Acknowledgments Ministerio de Ciencia e Innovación: Proy.: BIA 2010-18858. Plan Nacional I+D+i 2008-2011. Proy.: BIA 2006-14272. Plan Nacional I+D+i 2004-2007. Proy.: AGL 2002-00813. Plan Nacional I+D+i 2000-2003. References EN 13183-2. (2002). Moisture content of a piece of sawn timber. Part 2: Estimation by electrical resistance method. European Committee for Standardization. Brussels/Belgium. EN 1995-1-1. (2004). Eurocode 5. Design of timber structures. Part 1-1: General. Common rules and rules for building. European Committee for Standardization. Brussels/Belgium. Íñiguez-González, G., Llana, D.F., Montero, M.J., Hermoso, E., Esteban, M., García de Ceca, J.L., Bobadilla, I., Mateo, R., Arriaga, F. (2013). Preliminary results of a structural timber grading procedure in Spain based on non-destructive techniques. Proceedings of 18th International Nondestructive Testing and Evaluation of Wood Symposium. Madison, Wisconsin, USA. Pp. 386-395. 21 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 22 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Multi sensor approach combined with multivariate analysis for assessment of timber structures Jakub Sandak1, Anna Sandak1, Mariapaola Riggio2 1 CNR Ivalsa, S.Michele all’Adige (TN), Italy, [email protected], [email protected] 2 Wood Science & Engineering, Oregon State University, USA, [email protected] Abstract Numerous methods are used currently for existing timber structure assessment, including continuous monitoring of the structure performance on-site. However, its comprehensive characterization is often problematic issue due to wood anisotropy and heterogeneity. Trends for using multiple sensors simultaneously become more popular due to realistic representation of the real-world cases and advancement in hardware development. Multi-sensor approach even if possessing plenty of advantages require integration of non-destructive testing methodologies and data handling techniques to currently assess, monitor and predict wooden members properties. It is crucial to assure proper pre-processing of the signals from sensors, appropriate data fusion and optimal data analysis. The paper presents sucessful applications of the different data analysis techniques used for the assessment and monitoring timber structures. It is assumed that, after additional developments, such methodologies can provide supplementary data to be considered when inspector decision is made in order to support selection of optimal conservation process. Introduction Currently blooming engineering research provides us with numerous methods to be used for improving (reengineering) existing structure assessment routines, including also continuous monitoring of the structure performance. The availability of novel statistical tools to handle many variables simultaneously is another stimulus for rapid changes within the field of measurement technology and the sensors domain. Current trend for using multiple sensors simultaneously is more favorable than a single sensor approach due to far better representation of the real-world cases: the world is multivariate. 23 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Multi-sensor monitoring generates new issues and challenges, where the fusion of different sources of information is fundamental. Data collected from different types of sensors are often based on diverse physical phenomena, therefore interpretations of results is complicated. A general flowchart of the multi-sensor approach in timber structures assessment is summarized on Figure 1. It consists of several layers, including sample/object/case, sensors measuring member properties (through generating various types of data), and numerical models/tools to deal with such data in order to support expert in decision making. Sample Samples, cases or objects are the physical units on which the evaluation/measurements are performed. It can be a single wooden member or the whole structure, depending on the scope of evaluation and/or the goal of inspection. There are numerous sample(s) characteristics of interest when assessing timber structures, including: material properties degradation stage of wooden members due to biotic and a-biotic agents presence, position and incidence of strength-affecting defects in wooden members presence of damp areas and not uniform moisture distribution in wooden members mechanical damage in wooden members and connections geometrical alterations in the wooden members and assemblies overall performance of the structure and others. Sensors The visual assessment of timber structures on can be complemented by a series of instrumental techniques, giving information on unreachable object, about not-visible features, and on measurable/quantifiable parameters. The range of sensing techniques suitable for characterization of wood within structures is very wide and includes: vision systems in various spectral ranges; visible, infrared, thermovision, hyperspectral cameras measurement of electromagnetic radiations penetrating structure of wood; γ-rays, X-rays, microwaves, radar detectors analysis of mechanical/stress waves propagation; vibration; ultrasound sensors, accelerometers, microphones, laser vibration-meters semi-destructive methods; drilling/penetration/cutting equipment as well as screw withdrawal portable testers portable spectrophotometers in visible, near-infrared, mid-infrared, XRF spectral bands 24 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS wood moisture meters of various types Environment condition monitoring systems including measurements of temperature, relative humidity, solar radiation, rain events and intensity, among others Fig. 1. Multi sensor approach combined with multivariate analysis for assessment of timber structures Pre-processing The pre-processing of raw signals is a routine task usually performed before any further data evaluation. Several treatments are available, including: electronic signal manipulation, amplification, filtering, compensation, etc. numeric signal manipulation; normalization, filtering, correction, derivative, 25 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS integration, noise reduction, smoothing, interpolation, averaging, convolution, etc. numerical processing; compression, filtering, wavelet analysis, Fourier transform, etc. The optimal selection of signal pre-processing is crucial for the overall performance of the multi-sensor system, as well as the presentation of the results/parameters/ data. Even if all the existing sensors help in characterization, the human contribution to the structure assessment is indispensable. Data types The final output of the sensor (following the pre-processing procedures) is very diverse and depends on the sensor itself, the moment of data analysis, and nature of investigated object/structure, among others. Various sorts of data may be accessible, including: single/multiple variables such as scalars or vectors; value at a given time of measurement, change of this value (in the function of time, temperature, pressure, frequency, etc) measured with constant time laps or randomly waves, in the form of series of measurements, with defined starting point and distance between measurement points; such as stress-waves, vibrations, radar signals, microwaves images, or spatially resolved data, in the form of matrices (a rectangular array of numbers/variables arranged in rows and columns); gray, color, xray absorption, thermal images spectra, where series of data are representing frequency, wavelength, wavenumber resolved signals; UV-, Vis-, NIR-, IR-, XRFspectra hyperspectral/multispectral cubes, what are hybrids of images and spectra where each pixel represents the full spectra in a given range Data fusion The data fusion strategies are different when combining data in real-time or when analysis can be performed after measurement on the archived data. In the first case, dedicated interfaces are indispensable and such data fusion systems are rather complex/case-dependent. Whilst data evaluation can be performed in post-process mode, the data fusion is rather straightforward. It can be carried out with the help of different software tools (suitable for dealing with various signals/sensors) and accessing diverse databases. The most common result of the data fusion process is a spreadsheet containing 26 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS series of parameters extracted from various sensors corresponding to single sample/ case, collected at a given time or period of time. The size of the spreadsheet may vary depending on the system complexity, number of sensors utilized, quantity of samples/cases and/or duration of the measurement/monitoring. In general, the more complex (in terms of the number of variables and samples) collection of fused data the more reliable/generalized numerical models may be created. It has to be stated that having huge data sets is not equal to possessing “information”. In fact, high number of data may be cause of disturbance, misinterpretations or confusion, especially when “conventional” data analysis techniques are applied. Multivariate analysis (MVA) techniques, which allow more variables to be analyzed at once, are thus an alternative. The MVA can be divided into three groups: exploratory data analysis (data mining) – attempts to find the hidden structures in large and complex data sets classification models – are useful when identification of unknown sample/ object within one of previously established classes is required regression analysis and predictive models – are used for developing statistical models on the base of available reference data. Number of software packages suitable for MVA and for non-linear systems is already available on the market including, among others, Unscrambler X, OPUS, SIMCA. There is also a high number of dedicated modules for various software development environments such as C++, R, Matab or LabView, in some cases offered as an open source code. A list of MVA techniques suitable for applications toward timber structure assessment is presented below. Cluster analysis Cluster analysis (CA) is a statistical method used for matching multivariate data into particular groups according to their similarities. CA divides similar samples into groups called classes or clusters. Clustering methods belongs to unsupervised statistical algorithms; therefore do not require previous information about the objects’ memberships, which are obtained according to the data’s intrinsic characteristics, or dissimilarities. The clustering can be displayed in the form of a dendro-gram where the heterogeneity explains the similarity between the samples. The higher the heterogeneity, the higher is the difference between samples. Principal Components Analysis Principal Components Analysis (PCA) is a powerful statistical method for decorrelation of highly correlated data and to reduce the high dimensional data set to 27 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS lower dimensions. PCA decomposes a linear combination of original variables into few PC (principal components or factors). Each PC explains part of the data set variability. The number of significant factors is case dependant, but as a rule it should be as low as possible. In analogy to cluster analysis, PCA searches for unique properties of samples and separates set of input data into groups of peculiar similarities allowing visualization of natural clustering of the data. Identity test Identity test is a method extending use of Principal Components Analysis for differentiation of sample/cases and classification of unknown samples within previously defined groups. The identification of the unknown sample/case is based on computation of principal components by using loadings corresponding to the model. The resulting components are then compared to each group within the model. The result of such comparison is the sample distance called hit quality. The better sample match with the model group, the smaller is the distance. The hit quality of each comparison is weighted against threshold corresponding to each modeled group/class. Three possibilities of unknown sample identification are possible as a result of the identity test: the sample is identified as one of the modeled classes (hit quality < threshold in case of only one class) the sample is identified as probably belonging to more than one modeled classes, therefore not unique identification is possible (hit quality < threshold in case of more than one class) the sample is identified as none of the modeled classes (hit quality > threshold in case of all classes) SIMCA Soft Independent Modeling of Class Analogy (SIMCA) is another classification/ identification algorithm using Principal Components Analysis for differentiation of sample classes. In analogy to identity test, set of meaningful principal components is derived from the data set. The difference lays in modeling of classes, as in SIMCA each class is modeled separately (local models) and number of principal components may vary between classes. The prediction of a probable class membership for new samples/observations is performed by determination of best fitting to the respective class (local model). 28 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Partial Least Squares Partial Least Squares (PLS) is a statistical method considered as an expansion of Principal Components Analysis toward quantitative analyses. Basically, PLS finds a linear model describing some predicted variables in terms of other observable variables. The development of PLS model starts with computation of principal components on the base of calibration dataset. The obtained principal components are regressed in the next step against reference variables to be predicted. The PLS model has to be validated after calibration. The coefficient of determination, the rootmean square error of prediction and ratio of standard error of prediction to sample standard deviation are commonly accepted indicators of the PLS model quality. Multiple linear regression Multiple linear regression (MLR) is a multivariate analysis tool for modeling the relationship between two (or more) explanatory variables by fitting a linear equation to the reference data. MLR can also be used to estimate the linear association between the predictors and responses, in analogy to Partial Least Squares. Another use of multiple regression is to understand the functional relationships between the dependent and independent variables, by discovering the cause of the variation. The relationship between all predictors and a given response is summarized by the regression coefficients. Expert systems The most common perceptive of the expert systems is a rule-based programming. In this programming paradigm, rules are used to represent heuristics, which specify a set of actions to be performed (or decisions to be taken) for a given situation. A rule is composed of an if portion and a then portion. The if portion of a rule is a series of patterns which specify the facts (or data) which cause the rule to be applicable. The then portion of a rule is the set of actions to be executed when the rule is applicable. Fuzzy logic The easiest method to emphasize “knowledge” is to use not exact expressions, avoiding precise quantifications and classifying variables into rough values/sets. The scientific usage of such semantics is implemented within fuzzy logic expert systems. The value of each variable (obtained from one or more sensors) is 29 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS “fuzzyfied” according to pre-defined classes. As a result, detailed numerical value of variable is replaced by the fuzzy value such as “low”, “medium” or “high”. The set of fuzzyfied variables is then propagated to the module where if-then rules are tested. The output of the if-then module is a fuzzy number. It has to be “defuzzyfied” in order to make it a numerical/predicted value and become compatible with the following steps of evaluation and/or decision making. Neural networks Neural networks (NN) are widely used for processing of very complex and multivariable data sets. NN are very functional and have a number of great advantages; they have a parallel computation nature, can be applied in various applications, can continuously learn and adopt themselves for changing circumstances. NN is alike a “black box” as the knowledge acquired by the NN is hidden in the neuron weights. The set of variables is propagated to the input of the NN. The properly trained NN will process the input vector and will generate an output – predicted value to be later used for decision making or other actions. Back propagation algorithm is the most popular method for NN training, even if other procedures (including nonsupervised learning) are also available. Decision The overall purpose of characterizing wooden members with different sensors, as well as developing MVA solutions to deal with multivariate data, is to assist the inspector in making the correct decision regarding the structure assessment, safety and optimal maintenance. It is impossible to generalize the final reasoning process, and to even think to reduce the importance of the inspector in the final decision making, as each wooden structure is a unique case. It is clear, however, that the result of multivariate analysis has to be handy, reliable and intuitive for interpretation. Conclusions The proper timber structure assessment is of great importance to assure safe service of buildings as well as to preserve cultural heritage objects for future generations. A multi-sensor approach may be a very attractive alternative to conventional nondestructive method assessment and can provide supplementary data to be considered when inspector decision is measured. The problematic issue is, however, the high number of data/signals to be dealt as a result of measurement with several sensors. It is important, therefore, to assure proper pre-processing of the signals 30 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS from sensors, appropriate data fusion and optimal data analysis. The multivariate analysis systems can be implemented for various applications. Exploratory analysis are the most basic, but also most useful for preliminary data screening and identification of trends within data. Very important task is to continuously upgrade the models. In a perfect case, the software system should acquire new knowledge automatically along the service. It is assumed that, after additional developments, such methodologies can serve as assisting tools for non-destructive assessment of the wooden structures, service life prediction of structural elements and to support selection of optimal conservation process. 31 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 32 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Hierarchical modelling of timber reference properties using probabilistic methods: Maximum Likelihood Method, Bayesian Methods and Probability Networks Hélder S. Sousa ([email protected])a*, Jorge M. Branco a a ([email protected]) , Paulo B. Lourenço ([email protected]) a ISISE, Department of Civil Engineering, University of Minho, Portugal * corresponding author: ISISE, University of Minho, Department of Civil Engineering, Azurém, 4800-058 Guimarães, Portugal Abstract In recent decades, an increased interest has been evidenced in the research on multiscale hierarchical modelling in the field of mechanics, and also in the field of wood products and timber engineering. One of the main motivations for hierarchical modelling is to understand how properties, composition and structure at lower scale levels may influence and be used to predict the material properties on a macroscopic and structural engineering scale. This chapter presents the applicability of statistic and probabilistic methods, such as the Maximum Likelihood method and Bayesian methods, in the representation of timber’s mechanical properties and its inference accounting to prior information obtained in different importance scales. These methods allow to analyse distinct timber’s reference properties, such as density, bending stiffness and strength, and hierarchically consider information obtained through different non, semi or destructive tests. The basis and fundaments of the methods are described and also recommendations and limitations are discussed. The methods may be used in several contexts, however require an expert’s knowledge to assess the correct statistic fitting and define the correlation arrangement between properties. 1 Application Wood is a natural material that by itself has its own hierarchical structure, which is defined as the number of levels of scale with recognized structure. Hierarchical modelling requires the distinction and differentiation between different scales, 33 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS such that a homogenization step may be taken to each of those scales in order to define similar properties within a given scale. In [1], the hierarchical levels of timber were defined regarding the structural member as the main unit of analysis. In that case, three levels were defined: micro (material), meso (local) and macro (global). At the material level, several attempts have been made to hierarchically model the stiffness and strength of timber elements, by considering the presence of weak sections separated by segments of clear wood [2-5]. Early, in [6], a stochastic model of hierarchical series system was used to represent the bending strength of spruce regarding the anticipation of failure in a weak section with defects. The model parameters were defined regarding Maximum Likelihood estimates, and assuming that the estimated parameters are applicable in the series system model for the full uncut beams, a theoretical bending strength distribution function was obtained in dependence of number of defect clusters within the span of constant bending moment loading. A strong test of the prediction power of the model was established by experiments with 54 long beams from the same population of beams from which the small test pieces were cut. Also in [4], a hierarchical model was built for the multi-scale variability of modulus of elasticity (MOE) that included an explicit representation of the stiffness variability between timber boards and the stiffness variability within boards. All parameters of the hierarchical stiffness model were estimated based on a sample of 30 randomly selected timber boards within the strength class L25 of Norway spruce grown in southern Germany. The elements were differentiated along its length in weak sections and in clear wood sections and a model was proposed by definition of the mean modulus of elasticity within an element and the differences between that mean and the results within sections of the same element and between other elements. These values were modelled by probabilistic distributions with the parameters obtained using the Maximum Likelihood method. In [5], a hierarchical model for inferring on the reference properties of timber was proposed by considering the distinction between clear and knot wood zones. This work, however, presented a framework for timber members in service and thus differentiated from the previously mentioned. The model procedure was based in three main steps: i) visual identification of clear and knot wood zones; ii) nondestructive prediction of the properties of clear wood zones; iii) prediction of the reference materials using clear wood properties and applying a knot factor for predicting the strength reduction effect of knots on clear wood properties. The application of this procedure to maritime pine beams evidenced a good relationship between experimental and predicted global modulus of elasticity (r2 between 0.76 and 0.55). Nevertheless, for bending strength weaker results were obtained, evidencing the need for improvement in the method for determining the strength reduction effect of weak zones. In [7], Bayesian methods were used to update the mechanical properties of timber and reliability assessment was performed using First Order Reliability Methods 34 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS (FORM). The results showed that different degrees of belief in the updating data may significantly influence the reliability level. The used updating data were derived from non-destructive test (NDT) results obtained with ultrasound, resistance drilling and pin penetration equipments. The tests were conducted on chestnut wood specimens, and were combined with results from compressive strength parallel to the grain tests. The uncertainty of the different NDT results was also modelled by Maximum Likelihood estimates. Hierarchical modelling has also been carried out by use of Bayesian Probabilistic Networks (BPN) for the analysis of variability of timber mechanical properties [810]. BPNs are used to represent knowledge based on Bayesian regression analysis describing the causal interrelationships and the logical arrangement of the network variables. In [8], a hierarchical model was used to determine the influence of the origins (different tree growth locations) and cross-sectional dimensions of timber elements on the probability distribution of its material properties. On that work, BPNs were used to describe and inference on the dependence of different origins and dimensions of sawn structural timber on the relevant timber material properties conditional on indicator values assessed by machine grading indicators (Fig. 1). Following, the parameters of the prior probability distribution functions as well as the regression parameters were estimated as random variables with mean values, standard deviations and correlations using the Maximum Likelihood method. cross-section dimension influence variables material properties NDT indicators origin minimum tension strength Modulus of elasticity mean density strength indicator stiffness indicator density indicator Fig. 1 Example of a proposed BPN for inference on timber material properties, adapted from [8]. 35 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS The work in [10] considered the findings and results of a multi-campaign experimental campaign [11] as input data for the construction of the hierarchical levels and its interrelationships within a BPN inferring on the bending stiffness and strength of different size timber elements. In that case, the probabilities within the BPN were updated through Bayes' theorem regarding the belief propagation within the arrangements of nodes of different considered BPNs. The results were modelled by posterior distribution probabilistic parameters, accounting the results of Maximum Likelihood estimates and χ2 tests initially performed to the global sample. In that work, BPNs were developed in order to infer the influence of local data (smaller size specimens), with respect to both visual inspection and bending tests, on the results of stiffness and strength of structural size elements. An example of a studied BPN is presented in Fig. 2, with the results of different prior information in visual inspection grading given in Fig. 3 by cumulative frequency functions. Visual grading was considered as parent node in the analysis, as it provides a link between scales and, also as it is commonly an available parameter in the assessment of existing timber structures. Visual grading VI Structural size S VI Beams VIB MOE bending Em,l VI Boards VIb Fig. 2 Example of a proposed hierarchical model for inference on bending modulus of elasticity (MOE) regarding different scales on visual grading, adapted from [10]. 36 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS VIboard = I VIbeam = 75 no evid. frequency (%) 100 I 50 II III 25 NC 0 0 10000 20000 2 MOE (N/mm ) Fig. 3 Cumulative frequency distributions results obtained through a hierarchical BPN inferring on bending stiffness regarding different evidences on visual grading, adapted from [10]. When assessing a timber element by visual inspection several works have analyzed the accuracy obtained by automatic systems and manual graders, and also comparing the effectiveness and subjectivity of different inspectors [9,12-13]. In [9], BPNs were applied to infer on different scales of visual inspection accounting the information provided by inspectors with different levels of expertise. In that case, the use of BPNs permitted to individually assess the accuracy in stiffness prediction of different level of inspectors, and also by combination of their information. By use of a parallel combination for prior information, it was evidenced the significance in combining information by several inspectors even with similar or inferior individual accuracy. Moreover in that study, due to the large variability in the visual grading process, a second opinion improved the global efficiency, even if provided by a less experienced inspector. 2 Methodology 2.1 Maximum Likelihood method A possible way of defining the Maximum Likelihood method may be taken by the following premises [1]. Considering that the parameters θ = (θ 1, . T , θ n) of the distribution of X are known, the joint probability of a random sample X1, X2, ..., Xn can be written as: 37 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS f X ( x | θ ) = f X1 , f X 2 ,..., f X n (x1 , x2 ,..., xn | θ ) = f X1 (x1 ) f X 2 (x2 )... f X n (xn ) = = ∏ f X (xi | θ ) (1) i=1 However, it is often the contrary situation that is present in engineering applications, such that a sample xˆ1 , xˆ2 ,..., xˆ n is observed and the distribution parameters are unknown. In that sense, Eq. 1 can be understood as a relative measure for the likelihood that the distribution determined by the parameters θ is appropriate in the statistical definition of the sample x̂ . Along the full domain of all possible parameters θ the likelihood L(.) that the parameters belong to the sample is: n L(θ | xˆ1 , xˆ 2 ,..., xˆ n ) = ∏ f X (xˆ i | θ ) (2) i =1 The Maximum Likelihood estimates can be defined by the parameters θ which maximize the likelihood function L(.) over the domain of θ, thus being assumed as the most likely to represent the data sample, as: θ = max L(θ | xˆ1 , xˆ 2 ,..., xˆ n ) θ (3) The Maximum Likelihood method besides being used to fit the statistical parameters in distribution functions can also be used to fit the parameters in linear and non-linear regression analysis [14]. Also when considering a sample of results taken from tests a linear regression may be estimated including an uncertainty parameter or also called lack-of-fit parameter. For parameter estimation for linear regression lines, the following linear regression model in x1, ..., xm – space is considered: y = α 0 + α 1 x1 + ... + α m x m + ε (4) where α0, α1, ..., αm are the regression parameters and ε models the lack-of-fit. ε is assumed to be Normal distributed with expected value 0 and standard deviation σ ε . It is assumed that n sets of observations or test results of (x,y) are available and denoted as: (x1, y1), ..., (xn, yn). The regression parameters are determined using a Maximum Likelihood method. The likelihood function is written with xij being the j th coordinate of the i th observation: m L(α 0 , α1 ,...,α m ) = ∏ P( yi = α 0 + α1 xi1 + ... + α m xim + ε ) i =1 38 (5) PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS or, as in this case if it is used that ε is Normal distributed and σ ε is included as a parameter to be estimated, then it follows: m 1 i =1 2πσ ε L (α 0 , α 1 ,..., α m , σ ε ) = ∏ 1 y − (α + α x + ... + α x ) 2 0 1 i1 m im (6) exp − i 2 σ ε The log-likelihood function becomes: ln L (α 0 , α 1 ,..., α m , σ ε ) = − n ln ( m 1 y − (α + α x + ... + α x ) 0 1 i1 m im 2πσ ε − ∑ i 2 σ i =1 ε ) 2 (7) Finally, the optimal parameters are determined from the optimization problem: max α 0 ,α 1 ,..., α m ,σ ε ln L (α 0 , α 1 ,..., α m , σ ε ) (8) 2.2 Bayesian Probabilistic Networks BPNs are used to represent knowledge upon a system based on Bayesian regression analysis describing the causal interrelationships and the logical arrangement of the network variables. BPNs are represented by directed acyclic graphs (DAG), composed by a set of nodes, representing each system variable, connected by a set of directed edges, linking the variables according to their dependency or cause-effect relationship. The causal relationship structure of a BPN is often described by family relations that differentiates child node variables with ingoing edges (effects), from parent node variables with outgoing edges (causes) [15]. A (parent) node without any ingoing edges, thus without any parent node converging to it, is often called a root node. The direction-dependent criterion of connectivity evidences the induced dependency relationship between variables and is classified as converging, diverging or serial (or cascade), according to its arrangement [16]. Each variable node represents a random variable, either defined as a continuous random variable or as a finite set of mutually exclusive discrete intervals. In a BPN it is possible to coexist different nodes with either continuous or discrete variables, in so called hybrid BPNs. The main objective of a BPN is to calculate the distribution probabilities regarding a certain target variable, by considering the factorization of the variables' joint distribution based on the conditional relations within the developed generic algorithm. In this light, the DAG is the qualitative part of a BPN, whereas the conditional probability functions serve as the quantitative part. Therefore, the algorithms themselves are indifferent to the scope for which the BPN is employed, and thus have been employed in several different real-world problems, 39 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS besides the hierarchical modelling of reference properties, such as in diagnosis, forecasting, automated vision, sensor fusion, manufacturing control, and information retrieval [17]. A review of application of BPNs in environmental modelling is found in [18], while a review in BPNs applications on dependability, risk analysis and maintenance is provided by [19]. The applicability and framework for construction of BPNs in the field of reliability analysis has been addressed in e.g. [20-21]. In the case discrete states are used, each random variable is defined by conditional probability tables, with the exception of nodes without parents which, in that case, are defined by their marginal probabilities. Taking as example a converging BPN with two parent nodes (A and B) with corresponding marginal probabilities P(Ai) and P(Bi) for each given state i (i = 1, 2, 3,... n with n = number of states), the conditional probability of the child node (C) given states of A and B is calculated as: P(C A, B) (9) The joint probability of all nodes is then calculated by the multiplication of the conditional probabilities of the individual nodes, as: P(C, A, B) = P(C A, B) ⋅ P( A) ⋅ P(B) (10) The marginal probabilities of the child node C are obtained by the sum of the individual joint probabilities in every state, as: P (C ) = ∑ ∑ P (C , A , B ) A (11) B One of the main advantages of BPNs is that information may be easily implemented to the network allowing for an update of the target variable. By instance, if information about the state of a parent node is known with certainty, then is referred that an evidence, e, is given in that state. Back to the example of the converging BPN, considering that information is given to the state of parent node A by evidence eA as it belongs to state 1 (i = 1), therefore A = A1 and the probability P(A1) = 1, the probability distribution of the remaining variables of the network can be updated following Bayes theorem, as: P(C , B A1 ) = P (A1 C , B ) ⋅ P(C , B ) P( A1 ) (12) By application of Eq. 12 the posterior joint probabilities are obtained regarding the prior given evidence. The previous methodology can also be extended to converging BPNs with more than two parent nodes, or even to diverging or serial BPNs, being most often found that complex engineered systems are composed by the combination of smaller BPNs with these different arrangements. 40 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 3 Recommendations In the Bayesian probability methods, probabilities are considered as the best possible expression of the degree of belief in the occurrence of a certain event. The Bayesian probabilistic approach does not consider that probabilities are direct and unbiased predictors of occurrence frequencies that can be observed in practice. The only consideration is that, if the analysis is carried out carefully, the probabilities will be correct if averaged over a large number of decision situations [22]. To fulfil that consideration it is necessary that the subjective and purely intuitive part is neither systematically over conservative nor over confident. Therefore, calibration to common practice on the average and to empirical data may be considered as an adequate path to that aim. In the case of BPNs, it is recommended that the parents nodes are composed by indicators with strong correlations with the child node (reference property in analysis) given, as instance, by high coefficients of determination. After determining the indicators with higher predictive power, the dependencies within the DAG are created with different levels of hierarchy according to expert decision. The levels of hierarchy should attend to the source of the data, its relevance and both its size and material scale. When considering decay in timber elements, dynamic BPNs should be implemented as to incorporate a time dimension, mainly by adding a direct mechanism for representing temporal dependencies among the variables, see e.g. [23-24]. Dynamic BPNs have also been extended to the modelling of deterioration as reported in [25], while aspects of optimization inspection and maintenance decision regarding deterioration have also been addressed by BPN analysis in e.g. [26-28]. In a probabilistic analysis, as the inference on characteristic values is of special interest in the field of structural safety assessment, it is also recommended that special focus is given to the extreme values of the distributions. Therefore a scheme for estimating the parameters of probability distributions focusing on the tail behaviour should also be addressed, as considered in [29] where a censored Maximum Likelihood estimation technique was used. 4 Limitations Bayesian methods allow quantifying an approximation about the statistical uncertainty related to the estimated parameters, regarding both the physical uncertainty of the considered variable, as well as the statistical uncertainty related to the model parameters. Therefore, they offer a suitable method for parameter 41 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS estimation and model updating. However, for making this possible, it is necessary to take into account the measurement and the model uncertainties in the probabilistic model formulation. Since Bayesian methods grant the opportunity to incorporate different considerations about the uncertainty of models in the upgraded stochastic model, the comparison between different experts’ results may be regarded as a limitation, such that a consensus about a comparison basis has not yet been established. Nevertheless, in the case of the construction of a BPN, experts often promptly assert the causal relationships among variables in a domain, without pre-ordering the variables in different levels. In almost all cases, by doing so, results in a BPN which conditional-independence implications are accurate [30]. Another limitation of Bayesian methods is the overall requirement of a sufficient large sample for a reliable analysis. In a parallel BPN, it should also be noted that a small sample may lead to the situation that the joint probability factorization may not be possible due to the non occurrence of a given intersection of evidences. In this case, when using discrete variables the construction of a BPN is highly dependent of the choice of the intervals’ range. Both the Maximum Likelihood method and Bayesian methods are statistic tools that may consider data from different sources, such as different NDTs, SDTs or destructive tests, or even their combination. However, these data must be classified and arranged with respect to its relevance and dependability, in order to obtain an adequate hierarchical modelling and inference on different reference properties of timber. References 1. Köhler J (2007) Reliability of timber structures. PhD thesis, Institute of Structural Engineering Swiss Federal Institute of Technology, Zurich, Switzerland 2. Riberholt H, Madsen PH (1979) Strength of timber structures, measured variation of the cross sectional strength of structural lumber. Report R 114, Structural Research Lab., Technical University of Denmark 3. Isaksson T (1999) Modelling the variability of bending strength in structural timber. Report TVBK-1015, Dept. of Structural Engineering, Lund University, Sweden 4. Fink G, Köhler J (2011) Multiscale variability of stiffness properties of timber boards. In: Faber, Köhler, Nishijima (ed) Applications of Statistics and Probability in Civil Engineering. Taylor & Francis Group, pp 1369-1376 5. Machado JS, Palma P (2011) Non-destructive evaluation of the bending behaviour of inservice pine timber structural elements. Mater Struct 44(5):901-910 6. Ditlevsen OD, Källsner B (1998) System effects influencing the bending strength of timber beams. In: Proceedings of 8th IFIP WG 7.5 Working Conference, Krakow, Poland, pp 129-136 7. Sousa HS, Sørensen JD, Kirkegaard PH, Branco JM, Lourenço PB (2013) On the use of NDT data for reliability-based assessment of existing timber structures. Eng Struct 56:298-311 42 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 8. Deublein M, Schlosser M, Faber MH (2011) Hierarchical modelling of structural timber material properties by means of Bayesian Probabilistic Networks. In: Faber, Köhler, Nishijima (ed) Applications of Statistics and Probability in Civil Engineering. Taylor & Francis Group, pp. 1377-1385 9. Sousa HS, Branco JM, Lourenço PB (2013) Effectiveness and subjectivity of visual inspection as a method to assess bending stiffness and strength of chestnut elements. Advanced Materials Research, vol 778. Trans Tech Publications, pp 175-182 10. Sousa HS (2013) Methodology for safety evaluation of existing timber elements. PhD thesis, Civil Engineering Department, University of Minho, Guimarães, Portugal 11. Sousa HS, Branco JM, Lourenço PB (2014) Use of bending tests and visual inspection for multi-scale experimental evaluation of chestnut timber beams stiffness. J Civ Eng Manag (in press) 12. Lycken A (2006) Comparison between automatic and manual quality grading of sawn softwood. Forest Prod J 56(4):13-18 13. Grönlund U (1995) Quality improvements in forest products industry: classification of biological materials with inherent variations. PhD thesis, Luleå University of Technology, Swe-den 14. Sørensen JD (2003) Statistical analysis using the Maximum-Likelihood Method, Aalborg University, Aalborg, Denmark 15. Bayraktarli YY, Ulfkjaer J, Yazgan U, Faber MH (2005) On the application of Bayesian probabilistic networks for earthquake risk management. In: Proceedings of 9th international conference on structural safety and reliability, Rome, Italy 16. Pearl J (1988) Probabilistic Reasoning in Intelligent Systems: Networks of Plausible Inference. Morgan Kaufmann Pub. 552pp 17. Heckerman D, Mamdani A, Wellman MP (1995) Real-world applications of Bayesian networks. In: Communications of the ACM 38(3):24-26 18. Aguilera PA, Fernández A, Fernández R, Rumí R, Salmerón A (2011) Bayesian networks in environmental modelling. Environ Modell Softw, 26(12): 1376-1388 19. Weber P, Medina-Oliva G, Simon C, Iung B (2012) Overview on Bayesian networks applications for dependability, risk analysis and maintenance areas. Eng Appl Artif Intel 25(4):671-682 20. Langseth H, Portinale L (2007) Bayesian networks in reliability. Reliab Eng Syst Saf 92(1):92-108 21. Marquez D, Neil M, Fenton N (2010) Improved reliability modelling using Bayesian networks and dynamic discretization. Reliab Eng Syst Saf 95(4):412-425 22. Vrouwenvelder ACWM (2002) Developments towards full probabilistic design codes. Struct Saf 24(2):417-432 23. Allen JF (1981) An interval-based representation of temporal knowledge. In: Proceedings of 7th International Joint Conference on Artificial Intelligence, Vancouver, Canada, pp 221-226 24. Ghahramani Z (1998) Learning dynamic Bayesian networks. In: Adaptive processing of sequences and data structures. Springer Berlin Heidelberg. pp 168-197 25. Straub D (2009) Stochastic modelling of deterioration processes through dynamic Bayesian networks. J Eng Mech 135(10):1089-1099 26. Friis-Hansen A (2000) Bayesian networks as a decision support tool in marine applications. Department of Naval Architecture and Offshore Engineering, Technical University of Denmark 27. Attoh-Okine NO, Bowers S (2006) A Bayesian belief network model of bridge deterioration. In: Proceedings of the ICE-Bridge Engineering, 159(2):69-76 43 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS 28. Montes-Iturrizaga R, Heredia-Zavoni E, Vargas-Rodríguez F, Faber MH, Straub D (2009) Risk Based Structural Integrity Management of Marine Platforms Using Bayesian Probabilistic Nets. J Offshore Mech Arct Eng 131 29. Faber MH, Köhler J, Sørensen JD (2004) Probabilistic modelling of graded timber material properties. Struct Saf 26(3):295-309 30. Heckerman D, Breese JS (1996) Causal independence for probability assessment and inference using Bayesian networks. In: IEEE Transactions on Systems, Man and Cybernetics, Part A: Systems and Humans 26:826-831 44 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Quantitative assessment of the load-bearing capacity of structural components using NDT, SDT and DT inspection methods Gerhard Finka and Jochen Kohlerb 1 a ETH Zurich, Institute of Structural Engineering, Zurich, Switzerland b NTNU, Department of Structural Engineering, Trondheim, Norway Introduction In timber constructions a significant number of failures and damages have been detected within the last decades, well-known documentations are e.g. Frühwald et al. (2007), Blaß & Frese (2010) and Kohler et al. (2011). In many cases, only a partly damage of the construction accord (e.g. a single structural component, a single connection, a group of components, etc.), whereas the remaining (nonfailed) structural members are apparently unaffected - they might be also damaged due to additional loading caused by load redistribution. In such cases the corresponding engineer has to make a decision for the repair alternatives. This might be an exchange of the failed member(s), a reinforcement of the non-failed members or in the worst case a complete renovation of the entire construction. However, to make the optimal decision, it is essential to estimate the load-bearing capacities of the remaining structural members; thereby it has to be considered that the load-bearing capacity is composed of the load-bearing capacity at the time of construction and the deterioration during utilization (Fink & Kohler 2014b). In many situations the estimation of the remaining load-bearing capacity is rather complicated and connected to large uncertainties. However, under the consideration of information available, such as the target material properties, the age of the building, the history of load (e.g. amount and duration of load) or the amount of the damage, a first estimation can be made. Often this first estimation is not sufficient to make a final decision. In such cases different non-destructive, semi-destructive and destructive inspection methods (referred to as NDT, SDT and DT) can be performed to enhance the estimation. In this chapter a summary about the quantitative assessment of the load-bearing capacity of structural components based on information available and the results of different NDT, SDT and DT inspection methods using Bayes updating is presented (for a more detailed description see Fink & Kohler 2014a). At first information is classified according their characteristics in respect to a qualitative 45 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS assessment of the load-bearing capacity of structural components. Afterwards, the corresponding updating-procedure is introduced. The application of the updating procedure is illustrated on two selected examples. In the last part of this chapter, the application of Bayes updating for the decision support is introduced. 2 Updating For the estimation of the actual load and the resistance of a structural system, the way of treating available information is of particular importance. To do this, the structural model (static system), the applied load, the geometrical properties and especially the material properties of the structural components have to be considered. One handsome approach to combine different types of information is the socalled Bayes updating. Using Bayes updating, given information (so-called prior information) will be updated with additional information; e.g. the results of a NDT inspection. The prior information can be the planed conditions (if available), such as the target material properties or (if nothing better available) the assessment of an expert. The Bayes approach is related to the quality of the prior information and the characteristics of the information used for updating. For this purpose, the information is classified according the characteristics necessary for Bayes updating. Thereby it can be distinguished between so-called equality type information and inequality type information. Equality type information are measured variables, whereas inequality type information denotes information that some variable is greater than or less than some predefined limit. Furthermore, it can be differentiated between direct information (direct measurements of the quantity of interest) and indirect information (measurement of some indicator of the quantity). For the different types of information the corresponding updating procedure is introduced (according to Rackwitz 1983, Faber 2012, Faber et al. 2000, Fink & Kohler 2014b). The general scheme for updating the parameters having equality type information is given in Eq. (1). The inspected parameter, here the loadbearing capacity of the structural members, is represented by the variable X with the probability distribution function FX(x). The parameters θ = ( 1, 2, ..., n)T of the distribution function are not precisely known; they are product of engineering knowledge, physical understanding or earlier observations of the quantity. In general the parameters θ are expressed as random variables specified by the so-called prior density function f Q' ( θ ) . The uncertain parameters θ can be updated with new T information (new observations of realizations of the variable X,x^ = ( x^1, x^2 ,..., x^n ) ). ^ f Q' ' ( |x) ^ denote the posterior distribution function of the parameters θ, L(θ x) de- 46 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS note the likelihood function (representing the knowledge gained by the new information), and n is the number of observations. f ' '' ( x ) = ∫ f X ( x θ) f '' (θ x^)d θ Q f Q'' (θ x^ ) = f Q' ( θ)L(θ x^ ) ∫ f Q' (θ )L(θ x^ ) θ (1) The load-bearing capacity of the structural members can also be updated having inequality type information. Assuming a structural member will be proof loaded up to specific stresses effect σ l without failure. Thus the load-bearing capacity of the structural members can be represented by the variable X following a truncated distribution function. In Faber et al. (2000) the following approach is proposed to calculate the load-bearing capacity FR'' (r); here FR' (r) is the prior distribution function of the resistance: F ' (r ) − FR' (σ l ) FR'' (r ) = R 1 − FR' (σ l ) r ≥ σl (2) The principle of updating using equality type information and updating using inequality type information is illustrated in Fig. 1 on two examples. In both examples, the bending strength of GLT beams (strength class GL24h) is updated. One time with equality type information and one time with inequality type information. The characteristic value of the bending strength fm of strength class GL24 is fm,k = 24 MPa. The bending strength fm is assumed to be lognormal distributed with COV = 0.15, in accordance to JCSS (2006). Thus, the logarithm of the bending strength is normal distributed: ln(fm) ~ N(µ’, σz), with σz ≈ COV = 0.15. In Fig. 1 (left), the bending strength fm of GLT beams is updated with the results of three bending tests fm,i = 22, 30, 35 MPa (equality type information). All three test results are within the expected range, but slightly below the expected value. As a result the predictive bending strength of the not tested GLT beams is slightly reduced, in particular within the upper tale of the distribution function. In the second example (Fig. 1, right), the bending strength f m of the GLT beams is updated after proof loading. The load is applied constantly over the entire construction and corresponds to σl = 22 MPa. In this example no GLT beam failed under this load and thus it is obvious that the loadbearing capacity of all GLT beams is at least equal to the specific load effect: fm > σl = 22 MPa. As a result, in Fig. 1 (right), the lower tail of the predictive distribution function is truncated. 47 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Fig. 1 Schematic illustration of the principle of (left) updating using equality type information, and (right) updating using inequality type information 3 Decision support The presented summary about the quantitative assessment of the load-bearing capacity of structural components using NDT, SDT and DT inspection methods concludes with a discussion about the application of Bayes updating for the decision support. Two fields of application are discussed: - Support the corresponding engineer to choose the optimal inspection methods: Using the Bayes updating combined with the assumption of possible outcomes the optimal inspection method as well as the optimal number essential test can be estimated. Such pre-investigations can be very efficient for the choice (type and amount) of inspection methods. As a result useless inspections can be avoided and the total cost of the renovation (inspection costs and repair costs) can be minimised. - Support the corresponding engineer to find the optimal decision: Under consideration of the information available and all test results (NDT, SDT, and DT) the load-bearing capacity of the non-failed structural members can be estimated using Bayes updating. This can support the corresponding engineer to make a final decision. References Blaβ H.J. & Frese M. (2010). Schadensanalyse von Hallentragwerken aus Holz. Karlsruher Berichte zum Ingenieurholzbau 16, KIT Scientific Publishing, Karlsruhe, Germany 48 PART I- ENHANCEMENT OF NDT/SDT INFORMATION THROUGH STATISTICAL/PROBABILISTIC MODELS Faber M.H. (2012). Statistics and Probability Theory: In Pursuit of Engineering Decision Support, vol 18. Springer Verlag Faber M.H., Val D.V. & Stewart M.G. (2000). Proof load testing for bridge assessment and upgrading. Engineering Structures 22(12):1677-1689 Fink G. & Kohler J. (2014a). Quantification of different NDT/SDT methods in respect to estimate the load-bearing capacity. under preparation Fink G. & Kohler J. (2014b). Risk based investigations of partly failed or damaged timber constructions. In: Materials and Joints in Timber Structures, Springer, pp 67-75 Frühwald E., Serrano E., Toratti T., Emilsson A. & Thelandersson S. (2007). Design of safe timber structures - How can we learn from structural failures in concrete, steel and timber? Tech. rep., Lund University, Sweden JCSS (2006). Probabilistic Model Code Part III - Resistance Models (3.05 Timber). http:// www.jcss.byg.dtu.dk/Publications/Probabilistic Model code Kohler J., Fink G. & Toratti T. (eds) (2011). Assessment of Failures and Malfunctions. Shaker Publishing Company, Aachen, Germany Rackwitz R. (1983). Predictive distribution of strength under control. Materiaux et Construction 16(4):259-267 49 50 PART II ASSESSMENT OF REFERENCE PROPERTIES 51 52 PART II- ASSESSMENT OF REFERENCE PROPERTIES Methodology and protocols for routine assessment of wooden members with spectroscopy Anna Sandak1, Jakub Sandak1, Mariapaola Riggio2 1 CNR Ivalsa, S.Michele all’Adige (TN), Italy, [email protected], [email protected] 2 Wood Science & Engineering, Oregon State University, USA, [email protected] Abstract Current procedures for characterization of wood members on-site are often limited to few characterizations (visual inspection supported by the localized resistance analysis and moisture content estimation). The development of electromagnetic wave-based methods, such as spectrometric techniques, electric and optical methods, as well as the increasing availability of portable instruments, has opened up new perspectives for on-site characterization and monitoring of building materials. The objective was to highlight the potential of the infrared spectroscopy as a tool capable of providing complementary information for the expert inspection assessing the timber structures. Advantages and drawbacks of the techniques are illustrated together with recommendations regarding samples presentation, correct measurement as well as data evaluation. Finally examples of sucessful application of infrared spectroscopy for assessment of selected wood properties are presented. Introduction Nondestructive testing (NDT) methods find a particular place among analytical methods used for structure assessment due to the limited amount of required sample, or in case of portable instruments possibility of performing measurement directly on-site. Unfortunately many of instrumental methods, even possessing plenty of advantages, are rarely applied on-site due to the lack of standardized procedures. Infrared spectroscopy, in both near and mid ranges, is a well known technique with a great potential for chemical characterization of materials. It is useful for identification of various organic compounds, on the base on their selective absorption of radiation in the infrared region. As an effect of this phenomenon, the infrared radiation reflected from the surface can be used for estimation of the physicchemical structure of the surface. Several researchers are focused on the evaluation of physical and mechanical properties of wood or estimation its degradation level. The objectives of this research are to highlight potentials and limitations of 53 PART II- ASSESSMENT OF REFERENCE PROPERTIES proposed techniques and to provide list of requirements for correct implementation of spectroscopy in routine assessment of wooden members. Strength and limits of IR spectroscopy Traditional infrared (IR) technique is used to analyze solid, liquid or gases by means of transmitting the infrared radiation through the samples. The Attenuated Total Reflectance (ATR) allows measurement without necessity of complicated sample preparation and furthermore provides good spectral reproducibility. The advantages of this technique are: • little or no sample preparation; • possibility to measure samples that are too thickor too opaque for traditional transmission IR; • relatively fast measurement (minutes, depends on resolution); • possibility of measurements solids, powders or liquids; • possibility for determination of many components simultaneously; • high degree of precision and accuracy; • information related to chemical fingerprint; • direct measurement with very low cost. The restrictions of this technique are related to limited dimension of samples, pH constrains of used crystals and necessity of good contact between the sample and the crystal. The FT-NIR technique is relatively simpler and possesses some very important advantages (in comparison to other analytical methods): • simple sample preparation (to assure controlled MC and surface finish) • non-destructive or semi-destructive testing (fast screening method applicable on site and more accurate estimation method with controlled samples in the laboratory) • relatively fast measurement (seconds, depends on resolution); • no residues/solvents to waste • possibility for determination of many properties simultaneously • high degree of precision and accuracy • direct measurement with very low cost The most important limitation of the FT-NIR is that the spectra are rather complicated and includes a complex overlapping of different overtones corresponding to vibrating functional groups. Consequently, data evaluation is necessary for proper interpretation and understanding of results. The resolution of the spectrometer is also limited, thus complicating the spectra interpretation even more. Moreover sensitivity to moisture variations, surface preparation, aging of surface affects measurement. It must be also highlighted that in case of assessment of timber structural members, with a certain thickness and length, sampling criteria must be defined so that global 54 PART II- ASSESSMENT OF REFERENCE PROPERTIES characteristics can be reliably inferred from a number of local (and superficial) measurements. Methodology and protocols for routine assessment of wooden members with spectroscopy Sampling and sample preparation Representative reference sampling is essential especially when heterogeneous material such as wood is investigated. Precise sampling criteria must be defined in case of assessment of timber structural members. It has to be optimized depending on the structure topology, member size, state of preservation and due to the purpose of measurement. It has to be also highlighted that any measurement of mid or near infrared spectra may provide information related only to the local wood characteristics and is limited to the subsurface of the member. Sample preparation and presentation significantly affect reliability of presented techniques. Milling procedure, particle size, and quality of the solid wood surface influence the performance of the models to predict chemical properties. Recommendations regarding milled wood samples were presented by Schwanninger et al. [1]. Also the effects of sample presentation (solid or milled) affect reliability and quality of the models [2]. It is also important to minimize influence of temperature and relative humidity of the environment during measurement. Therefore, if it is feasible to take small amount of material from the member on site, it is highly recommended to condition it in climatic chamber prior spectroscopic measurements. Recently it is also possible to perform measurements directly onsite, especially with modern, portable instruments. Particular attention should be focused however on moisture content of measured wooden members and further correction, for proper data mining and interpretation. Measurement procedure/sample presentation Until recently, the preparation of samples to be measured with infrared spectrometers has been rather complicated; for example through solubilization of the sample or preparation of potassium-bromide (KBr) pellets for sample analysis (10 to 20mg of material). Fourier Transform Mid Infrared Attenuated Total Reflectance (FT-MIR-ATR) is a relatively new advancement of traditional mid infrared spectroscopy. It uses a phenomenon of absorbing infrared energy during reflection from the measured surface. This technique allows measurement of the wood powder or even wooden block surface without time consuming KBr sample preparation. Some instruments equipped with external reflectance module allow measurement of large objects without contact. This technique might be particularlyuseful during on-site analysis by placing the instrument in front of the analyzed object. Fourier Transform Near Infrared (FT-NIR) spectroscopy offers 55 PART II- ASSESSMENT OF REFERENCE PROPERTIES even simpler measurement and its applicability for in-field measurement is good. Due to low absorption coefficients, bulk or thick samples of intact cellular structure can be measured [3]. Spectrometers equipped with fiber optic allow direct measurement of samples at a certain distance from the instrument (depending on fiber optic length). Use of fiber optic is most convenient approach for acquiring near infrared spectra. The reference light is emitted from the probe and reflected part of it is transmitted to the detector. The area of the detector varies and may cover from 1 to 20mm2. As a result, the spectrum acquired is an “average” from the surface area corresponding to the probe having direct contact with measured object. No any extra pressure is required, even if the probe positing (deviation from the perpendicular placement) may influence the spectra outline. FT-NIR does not require sample preparation or hazardous chemicals, making it quick and reliable for quantitative and qualitative analysis. It is ideal for rapid material identification and is also a powerful analysis tool capable of accurate multi-component quantitative analysis. Recently hyperspectral system able to measure and characterize whole surface with high spatial resolution become more used. Hyperspectral images add a new dimension (spatial resolution) to the field of spectroscopy. They provide a means of accurately quantifying and locating constituent variation within the field of view of the camera, in addition to the identification and quantification of bulk constituents provided by integrating spectrometers. The measurement distance vary from millimeters up to meter and the spatial information is acquired directly by the spectrometer optics, by means of controlled positioning of the sample. The spectral band of hyperspectral camera may include various spectral ranges (UV, VIS, NIR, IR) as well as Raman scatter. It provides the great possibility to characterize various physical-chemical properties of the surface with high spatial resolution. Collection of representative spectra The routine testing procedure for the measurements should be determined through a series of preliminary tests, in order to optimize the scanning procedure and improve the quality of results obtained from wood samples. Due to anisotropy and heterogeneity of wood, it is important to repeat measurements and average spectra. It is recommended to measure different samples on the corresponding/ analogous points (for example on the radial plane). According to Tsuchikawa and Schwanninger [4] spectra collected from transverse and radial surfaces provide better prediction than those from tangential surfaces. The measurement location can be selected randomly; however, any visible abnormalities of wood surface (such as resin canal, knot or discoloration) should be intentionally omitted, unless the measurement of defect rate is intended. 56 PART II- ASSESSMENT OF REFERENCE PROPERTIES Data evaluations NIR absorption spectra are often complex and normally possess broad overlapping absorption bands that require special mathematical procedures for data analysis. In contrary MIR absorption bands are well-resolved, assignable to specific chemical components. Moreover the signal-to-noise ratio of NIR is poorer than that of FTMIR-ATR and interpretation of spectra more problematical. However NIR spectra contain a lot of information related to hydroxyl groups linked to several chemical components, which, in case of wood, are very relevant also for the estimation of physical and mechanical properties of the material. Interpretation of spectra is very important and is highly recommended to include this step in routine analysis. Recently published works provides valuable information in regards of bands assignment [5-8]. Visual observation of spectra is also the easiest method to detect outliers caused by errors during measurement (not parallel position of fiber optic (in case of NIR) or incorrect contact between sample and crystal (in case of ATR). Spectra identification and qualification (quantitative analysis) can be done by comparing a sample spectrum to reference spectra of known materials (or in case of decayed samples with reference samples infested with various fungi). Quantification is done by using mathematical models and so-called multivariate data analysis (MVA): these approaches are generally referred as chemometrics. MVA techniques are statistical design tool for dealing with very large datasets, which allow more than two variables to be analyzed at once. Multivariate data analyses are usually divided into three groups: exploratory data analysis, regression analysis and classification models. Exploratory analysis (data mining), attempts to find the hidden structure in large complex data sets, examples are Cluster Analysis or Principal Component Analysis. Regression analysis and Predictive Models, such as Partial Least Squares Regression or Multiplicative Linear Regression, are used for developing the models from available data and predict desired response. Even if both spectral noise and reference method noise affect the accuracy and the precision NIR predicted values sometimes model based on the noisy reference data led to good results [9]. Classification Models (Cluster Analysis Test, Identity Test or SIMCA) allow separation of group of objects into one or more classes, on the base on distinguished characteristics. Figure 1 summarizes recommended protocol for routine assessment of wooden members. 57 PART II- ASSESSMENT OF REFERENCE PROPERTIES correct sampling optimal sample preparation proper sample presentation collection of representative spectra elimination of outliers spectra interpretation qualitative analysis quantitative analysis Fig. 1. Schema of proposed stages for wooden members characterization. Source: [10] modified. Application of spectroscopy for assessment of wooden members Spectroscopy allows understanding of chemical changes of the wooden material during various degradation processes. It allowed classification of decay type and prediction of modification of physical properties, as a consequence of the decay process. It has been also successfully applied for monitoring the weathering process of different wood species, understanding the weathering dynamic and estimating both exposure time and service life of wooden structures [10]. Reports related to characterization and evaluation of waterlogged wooden samples, both from archaeological site and recent wood during short term waterlogging are recently published [11-12]. Several researchers already proved applicability of infrared spectroscopy for species recognition, prediction of moisture content, density, tensile strength, mechanical stresses, bending MOE and MOR [4]. In 58 PART II- ASSESSMENT OF REFERENCE PROPERTIES general, spectroscopy works with all wood species. Most of up-to-data prediction models reported in the literature are valid for a single wood species only. However, the development of generalized chemometric model suitable for several wood species is of great interest [9]. The important concern is related to the timber surface in use, including oxidation, ageing and/or weathering [13]. As a consequence, chemometric models developed for one sample lot may not be functional for same wood samples, but processed with different preparation procedure. In such case, calibration transfer formula is necessary. It has to be mentioned, that spectroscopic measurements are related to the surface, therefore can not be straightly correlated with internal properties of the members. The solution is to combine sampling with other methods (e. g. radial coring for dendrocronological analysis or semi-destructive analysis) and acquire the spectra along the members depth (e.g. radial profile) [14]. The development of electromagnetic (EM) wave-based methods, such as spectrometric techniques, imaging techniques, electric and optical methods, as well as the increasing availability of portable instruments, has opened up new perspectives for on-site characterization and monitoring of building materials. Moreover the trend for material characterization by using multiple sensors simultaneously has become well accepted. It is more favorable than a single sensor approach due to far better representation of the real-world cases. The speed of measurement is comparable with other NDT for decay detection, such as dynamic indentation (Pilodyn®) and infra-red thermovision, among others. The other challenge is however the correct interpretation of measurement data assuring integration/fusion of all indicators as the multisensory data is usually correlated with each other. Conclusions Practical application of spectroscopy for timber structure assessment provides very essential supplement to the typical information collected traditionally with standard procedures. Special attention is focused here to highlight potentials and limitations of proposed techniques and to provide list of requirements for correct implementation of spectroscopy in routine assessment. Up to now several researchers confirmed advantages of spectroscopy for evaluation of wood properties. However application of this technique for on-site wooden members inspection requires a proper definition of sampling criteria, according to the properties investigated, as well as prior preparation of dedicated databases of high precision reference values. Those are essential to build reliable, flexible and sufficiently generalized models. The method then might be a tool assisting experts in the estimation of reference material properties, and other relevant mechanical/ physical characteristics, in a fast and repeatable way. 59 PART II- ASSESSMENT OF REFERENCE PROPERTIES Acknoledgments P art of the work was conducted within project BIO4ever (RBSI14Y7Y4) within call SIR funded by MIUR. References [1] Schwanninger M, Rodrigues JC, Pereira H, Hinterstoisser B. Effects of short-time vibratory ball milling on the shape of FT-IR spectra of wood and cellulose. Vibrational spectroscopy 2004;36(1):23-40 [2] Hein PRG, Lima JT, Chaix G. Effects of sample preparation on NIR spectroscopic estimation of chemical properties of Eucalyptus urophylla S.T. Blake wood. Holzforschung 2010;64(1):45-54. [3] Fackler K, Schwanninger M. How spectroscopy and microspectroscopy of degraded wood contribute to understand fungal wood decay. Appl Microbiol Biotechnol. 2012;96(3): 587– 599. [4] Tsuchikawa S, Schwanninger M A review of recent near infrared research for wood and paper (Part 2). Applied Spectroscopy Reviews 2013;48:560-587 [5] Rowell RM. Handbook of Wood Chemistry and Wood Composites, CRC Press. 2005 [6] Workman J, Weyer L. Practical Guide to Interpret Near-Infrared Spectroscopy. CRC Press, 2007. [7] Burns DA, Ciurczak EW. Handbook of Near-Infrared Analysis. CRC Press 2008 [8] Schwanninger M, Rodrigues JC, Fackler K. A review of band assignments in near infrared spectra of wood and wood components. J. Near Infrared Spectrosc. 2011;19(5): 287-308. [9] Rodrigues J, Alves A, Pereira H, da Silva Perez D, Chantre G, Schwanninger M. NIR PLSR results obtained by calibration with noisy, low-precision reference values: Are the results acceptable? Holzforschung 2006;60(4),402-408 [10] Sandak A, Riggio M, Sandak J. Non destructive characterization of wooden members using near infrared spectroscopy. Advanced Materials Research, 2013;778:328-334 [11] Sandak A, Sandak J, Babiński L, Pauliny D, Riggio M (2014) Spectral analysis of changes to pine and oak wood natural polymers after short-term waterlogging. Polymer Degradation and Stability, 99:68-79 [12] Riggio M, Sandak J, Sandak A, Pauliny D, Babiński L (2014) Analysis and prediction of selected mechanical/dynamic properties of wood after short and long-term waterlogging. Construction & Building Materials 68:444-454 60 PART II- ASSESSMENT OF REFERENCE PROPERTIES Structural Analysis Of Porous Media By Means Of Thermal Methods : Theory And Monitoring Equipment Olivier CARPENTIER*, Thierry CHARTIER*, Emmanuel ANTCZAK*, Thierry DESCAMPSº, Laurent VAN PARYSº * Civil Engineering Department, LGCgE, University of Artois (Bethune, France) ° CESM Department, Univerisity of Mons, Mons (Belgium) Abstract Thermal methods are based on the knowledge of both theory of heat and mass transfers and thermal sensors. To be effective, thermal analysis must be able to make the logical connection between the theoretical thermal behaviour of a medium under solicitations and the ability of sensors to measure thermal physical quantities. Concerning porous media like wood, thermal analysis is very complex, mainly because of the difficulty to accurately describe micro-structure geometry and its influence in thermal behaviour of whole wooden structure. A description of current thermal methods (non-destructive and semi-destructive testing methods) are given for both laboratory and in situ experiments. Latest advances in thermal analysis are also presented. In conclusion, examples of dedicated applications and possible connections with some non-destructive testing methods give the necessary information to identify perspective of development. Keywords: Monitoring, Diagnosis, Numerical analysis, Thermal sensors 1. Introduction Thermal metrology primarily responds to three needs [1]. The first is mastery of manufacturing process in which a monitoring or an automated control solution is needed. The second is to highlight thermal effects in a system for which there is no obvious numerical solution (local heat transfers in huge system). The third responds to the evaluation of thermo-physical properties of materials and interfaces needs in order to know and improve materials. This evaluation can add new fields of knowledge to numerical modeling of complex systems. The quantitative thermal analysis falls into this last category. 61 PART II- ASSESSMENT OF REFERENCE PROPERTIES 2. Thermal metrology Thermal metrology is based on the exploitation of measurable physical quantities, i.e. temperature and heat flux, respectively expressed as Kelvin (K) and Watt (W) in the international system of units. In addition to temperature and heat flux, two other groups of physical quantities are defined : physical quantities linked to the material itself and physical quantities linked to its interface with environment or surrounding objects. Only temperature and heat flux can be directly measured via thermal sensors. Evaluation of other physical quantities needs to master the resolution of inverse problems. Table 1. Example of several physical parameters that can be determined from thermal analysis Physical parameters Determined by... Direct measure- The resolution of an inment verse problem Temperature x Heat flux x Thermal conductivity x Thermal diffusivity x Thermal effusivity x Evaluation through others physical parameters Specific heat x density x Water content x Convection coefficient x Contact thermal resistance x Radiative surface characteristics x Enthalpy x Viscosity x Porosity x 62 PART II- ASSESSMENT OF REFERENCE PROPERTIES Thermal analysis methods of thermo-physical properties of materials have the same basic protocol. First, temperatures and/or heat flux are measured with thermal sensors. Then, one or several thermo-physical properties (e.g. thermal conductivity)associated with studied material are evaluated via the use of mathematical formalisms [2]. Finally, several thermo-physical properties may be seen from previous ones (e.g. water content given by thermal effusivity [3]). Solid, granular, liquid, gaseous or other phase change materials (PCM) [4] can be studied. Table 1. is given for a single material. But thermal methods can be extended to composite materials. It may be possible to have global information of a system while generally the purpose is to highlight the presence of thermal resistance inside the medium (e.g. poor adherence [5] or cracks). There are a lot of thermal methods because they cover a wide field of analyses: - destructive (probes [6]) or non-destructive methods (infrared thermography, IRT [7]), - local (studies on micro and nano-components [8]) or huge areas can be investigated (thermal Doppler for atmosphere analysis [9]), - monitoring over time [10], - methods can be used in laboratory or on site [11]. With regard to positive points, it should be pointed out that thermal methods are very widely used, adapted to many materials and have applications on site. The significant presence of these methods also involves the existence of a wide variety of sensors to meet the most varied individual needs and budgets. However, although thermal methods are widely used, they have some limits. Disadvantages are related to the use of specific thermal method but there are common denominators : - Thermal methods are usually slow compared to other mechanical methods (Thermal diffusion effects), - Absolute accurate temperatures (accuracy of about 50mK) are difficult to obtain, - Global analysis. It is difficult to link information to a space discretization (anisotropy), - Quantitative analysis usually needs thermal solicitations that can modify thermo-physical properties of the medium. - While thermal sensors are steadily improving, heat flux measurement is still difficult. To solve these problems, the use of coupled mechanical or optical methods with thermal method is usually the prescribed solution in order to determine in particular thermo-physical properties. 63 PART II- ASSESSMENT OF REFERENCE PROPERTIES 3. Thermal methods and wooden structures As stated above, there are a lot of thermal methods and it is not possible to provide an exhaustive list. So, we focus on thermal methods suitable for wooden structures. Wood is a porous material with a very complex microscopic architecture. Thermal methods usually employed consider wood as a homogeneous medium for a specific direction [12]. If on site applications were considered, non-destructive thermal methods (NDTM) should be retained and could be active or passive. If wooden structure could receive solar radiations (random solicitations), passive methods would be considered [13]. Out of this specific context, NDTM have to use artificial thermal solicitations in which a deterministic signal is used. Two kinds of methods could be employed in laboratory or on site : thermal methods with contact and contactless thermal methods. 3.1 Thermal methods with contact Guarded hot plate test (laboratory) [14], hot wire or hot plane (laboratory) [15] and the combined use of thermocouples and flux meters (in laboratory and on site) [16] are widely used. The principle of the procedure is based on the installation of sensors on the medium boundaries. Then, thermal solicitation (deterministic signal) creates a disturbance. Thermal sensors measure thermal response of the medium (temperature variation and/or heat flux). Global thermo-physical properties access (thermal conductivity, diffusivity and effusivity) is given by mathematical formalism (resolution of inverse problem) and depends on injected signal (step, sinus,). These methods can be very accurate and suitable for small samples with low rugosity on sample surface in order to limit thermal contact resistance between sensors and samples [17]. It is recommended to work with thermal sensors able to measure temperature and heat flux with a minimal accuracy of respectively 100 mK and 1 W/m2. Wood samples have to be adapted to sensors size. Measurement area of thermocouple is about one square millimetre but flux meters (plane sensors) have a measurement area from 25 cm2 to 400 cm2. Wood samples will usually have a volume greater than 100 cm3. Monitoring on site is often more difficult than carry out laboratory tests. So, another interesting recommendation is to create a database of thermo-physical properties of their own wood samples in order to easily specify limits of thermal methods carried out on site. 3.2 Contactless methods It is without question that IRT is the predominant NDTM without contact [18]. 64 PART II- ASSESSMENT OF REFERENCE PROPERTIES It is a well known method and applications are numerous [19-22], even if wood is often less studied than other building materials because of its complex thermal behaviour. IRT protocol is the same as active thermal methods with contact but instead of the determination of thermo-physical properties, the first objective is mainly to detect thermal contrast (directly or after post-processing image [23]). In wooden structures, defects usually detected are void, cracks or moisture [24]. Wood is a material with a low thermal conductivity, so it is recommended that thermal solicitations last long enough to have a good thermal diffusion in the medium. For a study on the first millimetres of a wooden structure, tests should last about ten minutes. For a deeper investigation (5 to 6cm), tests can last more than two hours. Thermal solicitations have to be low in order to not disturb thermo-hydro behaviour of porous medium [25]. 4. Data analysis Inverse methods are used for data processing. Numerical method is chosen according to the nature of injected signal and thermo-physical properties or thermal effect that need to be determined. There are temporal methods based on simplified description of thermal problem to solve (function series decomposition) or spatial and temporal interpolation (Finite Differences [26] and Finite Elements Methods [27]). Other methods are based on frequential description of thermal problem like thermal quadrupoles methods [28]. Signals like steps are usually used with temporal description to determine conductivity. To better characterize thermal behaviour of wooden structure, more complex signals (sinus, sweep [29], pseudo-random binary sequence PRBS [30],...) are the most used. Thermal diffusivity and thermal effusivity can be so determined. There is a correlation between thermo-physical properties that can be directly identified (conductivity, diffusivity and effusivity) and some physical quantities such as water content [3] or porosity [31,32]. Correlation functions can be established to link measurements on site to laboratory data. 5. Conclusions In summary, thermal methods can be used to determine thermo-physical parameters of wooden structures, other physical quantities (water content, porosity) and defect inside the medium (cracks, voids). On site global thermal analysis (IRT) works fine but makes anisotropic properties of wood difficult to evaluate i.e. thermo-physical properties are known for a specific volume and not necessarily for a specific direction. Thermal methods are still attractive even in terms of preliminary-structural 65 analysis. However, a precise diagnosis requires an association with otherNDT methods (e.g. ultrasound [33]). Data fusion is in constant development andNDT methods associations have to be followed with attention. Acknowledgements We would like to thank members of FPS COST Action FP1101 Assessment, Reinforcement and Monitoring of timber Structure for their informed advice and the quality of the discussions. References [1] Degiovanni A., Rémy B., (2005) Métrologie thermique : une histoire, un appareil, une application, In: JITH 2005, Tanger, Maroc [2] Brown M.E., Gallagher P.K. (2008) Vol.5, Chap1. Recent advances, techniques and applications of thermal analysis and calorimetry. Brown M.E (ed) Handbook of Thermal Analysis and Calorimetry, Elsevier Science B.V., Grahamstown [3] Antczak E., Chauchois A., Defer D., Duthoit B. (2003) Characterisation of the thermal effusivity of partial saturated soil by the inverse method in frequency domain, Applied Thermal Engineering, Vol. 23, Issue 12 [4] Zalewski L., Joulin A., Lassue S., Duthil Y., Rousse D. (2012) Experimental study of smallscale solar wall integrating phase change material, Solar Energy, Vol. 86, Issue 1 [5] Berglind H., Dillenz A. (2003) Detecting glue deficiency in laminated wood – a thermography method comparison, NDT & E International, Vol. 36, Issue 6 [6] Carpentier O., Defer D., Antczak E., Chartier T. (2012) Frequency methods applied to the characterization of the thermophysical properties of a granular material with a cylindrical probe, International Journal of Thermophysics, Vol. 33, Issue 1 [7] Carpentier O., Defer D., Antczak E., Duthoit B. (2005) The use of infrared thermography and GPS topographic surveys to monitor spontaneous combustion of coal tips, Applied Thermal Engineering, Vol. 25, Issue 17-18 [8] Hosokawa M., Nogi K., Naito M., and Yokoyama T. (2008) Chapter 6 – Evaluation methods for properties of nanostructured body. In Nanoparticle Technology Handbook, Elsevier Science B.V., New York [9] Clemesha B.R., Martins Jorge M.P.P., Simonich D.M., Batista (1997) A new method for mesuring the Doppler temperature of the atmospheric sodium layer, Advances in Space Research, Vol. 19, Issue 4 [10] Keo S.A., Brachelet F., Breaban F., Defer D. (2014) Steel detection in reinforced concrete wall by microwave infrared thermography, NDT & E International, Vol. 62 [11] Carpentier O., Brachelet F., Defer D., Aubagnac C., Cannard H., (2009) Characterization of defect under waterproofing layer by IR thermography and thermal impedance, In: NDTCE’09, Nantes [12] Maldague X., Wyckhuyse A. (2001) A study of wood inspection by infrared thermography, Part I and II, Res. Nondestr. Eval, Vol. 13 66 PART II- ASSESSMENT OF REFERENCE PROPERTIES [13] Carpentier O., Defer D., Antczak E., Chauchois A., Duthoit B. (2008) In situ thermal properties characterization using frequential methods, Energy and Buildings, Vol. 40,Issue 3 [14] ISO 8302:1991 Thermal insulation -- Determination of steady-state thermal resistance and related properties -- Guarded hot plate apparatus [15] ISO 8894-1:2010 Refractory materials -- Determination of thermal conductivity -- Part 1: Hot-wire methods (cross-array and resistance thermometer) [16] THERY, P. (1979) Fluxmètre calorifique, Brevet ANVAR [17] Guo W., Lim J., Bi X., Sokhansanj S., Melin S. (2013) Determination of effective thermal conductivity and specific heat capacity of wood pellets, Fuel, Vol. 103 [18] Maldague X.P.V. (2001) Theory and practise of infrared technology for nondestructive testing, John Wiley & Sons [19] Büyüköztürk O., Taşdemir M.A., Oğuz G., Akkaya Y. (2011) Non-destructive Testing Materials and Structures, Springer, In: Proceedings of NDTMS, Istanbul, Turkey [20] Arndt R.W. (2010) Square pulse thermography in frequency domain as adaptation of pulsed phase thermography for qualitative and quantitative applications in cultural heritage and civil engineering, Infrared Physics and Technology, Vol. 53 [21] Ludwig N., Redaelli V., Rosina E., Augelli F. (2004) Moisture detection in wood and plaster by IR thermography, Infrared Physics and Technology, Vol. 46 [22] Kortados, E.Z., Exarchos D.A., Stavrakos C., Moropoulou A., Matika T.E. (2013) Infrared thermographic inspection of murals and characterization of degradation in historic monuments, Construction and Building Materials, Vol. 48 [23] Du T., Brachelet F., Defer D., Antczak E. (2013) Quantitative evaluation of thermal diffusivity and thickness of mortar cover using induction thermography, In Nondestructive Testing of Materials and Structures RILEM Bookseries, Volume 6 [24] Taoukil D., El bouardi A., Sick F., Mimet A., Ezbakhe H., Ajzoul T. (2013) Moisture content influence on the thermal conductivity and diffusivity of wood– concrete composite, Construction and Building Materials, Vol. 48 [25] Krishnaiah S., Singh D.N. (2003) Determination of influence of various parameters on thermal properties of soil, In: International Communication of Heat Mass and Transfer 30 (6) [26] Ozisik N. (1994) Finite Difference Methods in Heat Transfer, CRC Press [27] Lewis R.W., Morgan K., Thomas H.R., Seetharamu K. (1996) The Finite Element Method in Heat Transfer Analysis, Jhon Wiley & Sons [28] Maillet D., André S., Batsale J.C., Degiovanni A., Moyne C. (2000) Thermal Quadrupoles : Solving the Heat Equation through Integral Transforms, JohnWiley & Sons [29] Von Seggern D. (1993) CRC Standard Curves and Surfaces, Boca Raton, FL: CRC Press [30] Mahmoudi Y. (2014) Effect of thermal radiation on temperature differential in a porous medium under local thermal non-equilibrium condition, International Journal of Heat and Mass Transfer, Vol. 76 [31] Lopez G., Basterra L.A., Acuna L. (2013) Estimation of wood density using infrared thermography, Construction and building materials, Vol. 42 [32] Carpentier O., Antczak E., Brachelet F., Defer D., Descamps T., Van Parys L (2014) Characteristization of density variations of historic timber structure by thermal methods, In: The 12th International Conference on Quantitative Infrared Thermography, Bordeaux, France 67 [33] Kandemir-Yucel A., Tavukcuoglu A., E.N. Caner-Saltik (2007) In situ assessment of structural timber elements of a historic building by infrared thermography and ultrasonic velocity, Infrared Physics & Technology, Vol, 49, Issue 3 68 PART II- ASSESSMENT OF REFERENCE PROPERTIES Prediction of mechanical properties by means of semi-destructive methods Michal Kloiber1, Miloš Drdácký1 1 Czech Academy of Sciences, Institute of Theoretical and Applied Mechanics Abstract Methods and devices for in-situ establishment of mechanical properties of wood have been recently developed in cooperation of Czech and US researchers. The development of new methods was motivated by requirements from engineers who need most accurate data of mechanical properties of specific elements when planning renovations of historic buildings. The established data replace mean standard values of strengths in their static calculations, which results in the demanded possible retaining of a larger amount of original material as the behaviour of the specific elements is safely assessed. The newly developed methods, which are described in this chapter, are tensile s tr e n gth o f s ma ll samples, compression strength of cores, compression strength in a drilled hole, and mechanical resistance to pin pushing. Although the devices for the testing of mechanical properties by the mentioned methods provide more accurate results than the methods used so far, they are not mass produced, which should change soon. Key words: semi-destructive testing, wood, in-situ assessment, strength, pin, resistance. 1 Tensile strength of small samples 1.1 Sampling and testing methodology The assessment of bending strength is important for in-situ assessment of timber elements as it is the prevailing manner of loading in e.g. ceiling constructions. Bending strength of integrated timber cannot be established without damage done to the construction. However, it is close to tensile strength and according to some authors it can be considered almost the same (Kasal and Anthony, 2004). Therefore, a new method to establish strength of integrated timber using small samples taken from its surface was devised. 69 PART II- ASSESSMENT OF REFERENCE PROPERTIES Samples for the establishment of tensile strength are extracted in a simple way using an adjustable circular saw. Sampling is carried out by two cuts inclined in an angle of 45° in relation to the element surface (Fig. 1) parallel to the grain. The cut depth is adjusted so that a triangular bar with rectangular sides of about 5–8 mm is gained. The saw runs in guides, which are fixed to the surface of a tested element by screws. The damage done to the surface is remedied by an insertion of triangular bar with the same dimensions; it can also be totally mended by restoration. During the production of a sample, the area of the bar section is reduced to about 8–12 mm2 in the central part, which corresponds to production of tensile samples in compliance with (ASTM Annual Book). The samples should not contain any natural defects (knots, cracks or other damage). Rectangular wooden blocks are glued to both ends of the samples (Fig. 2) in order to fix the small samples in coaxial articulated grips of the loading device during the tensile strength testing (Kasal et al. 2003). Fig. 1 Circular saw with guides, modified Fig. 2 Tensile test of a triangular bar The tensile sample is inserted in simple grips designed for this purpose and loaded in a common testing device (Fig. 2). The test is not standard but its concept is very close to the standard test in compliance with (ASTM Annual Book) as it uses the same simple layout eliminating parasite movement and a cross-section with a small number of annual rings. The test measures the tensile strength and the modulus of deformability to calculate the modulus of elasticity. The maximum tensile loading for each sample is the ultimate load and the tensile strength is determined by the formula: 70 PART II- ASSESSMENT OF REFERENCE PROPERTIES fc = where Fmax [MPa] 0,5 ⋅ bh ft – tensile strength [MPa], Fmax – ultimate load [N], b – triangular bar hypotenuse [mm], h – triangular bar height [mm]. The results gained by this test need not be correlated and can be declared comparable with the standard test. For the purpose of the construction safety assessment and dimensioning, mechanical properties established by the described test must be converted to technical properties of timber which take account of the locally measured strength of clean timber reduced by defects that commonly appear in large elements (knots, cracks, and others). The disadvantage of this method is the damage done to the surface of the assessed element, which is undesirable in the case of historic construction timber assessment (Drdácký et al. 2005). 1.2 Limitations The method for the establishment of tensile strength and modulus of elasticity uses small triangular samples that are taken from a relatively shallow surface part of a timber element, where the historic timber is often damaged by biotic factors. The method is very sensitive to fibre deflections in the sample and requires a careful choice of a sampling place and careful sampling. The cross-sections of the sample is small, which increases the effect of a higher earlywood proportion. This effect is negligible in larger cross-sections. As a result, the values of strength and modulus of elasticity will be highly variable. Therefore, it is necessary to think well about the places where samples are to be taken and also take account of potential damage. 1.3 Application examples The tests of tensile samples have been successfully used e.g. when investigating the quality of ceiling joists in the St. Mary’s Tower of the Karlstejn castle or strength values of the storage hall in the trade fair facilities in Brno (South Moravia – ČR). The method can be also used to determine the level of damage to the surface layer of the timber. As an example we can name the study into the effect of fire protection treatment that has been repeatedly applied to timber constructions of historic buildings. The application of agents with fire retardants on the basis of 71 PART II- ASSESSMENT OF REFERENCE PROPERTIES sulphate and ammonium phosphate has caused damage to timber surface referred to as “fibrillated surface” which gives the look of timber elements a “fuzzy” character. The in-situ surveys of damaged timber construction elements proved that the fibrillated timber layer manifests a considerable loss of cohesion and deterioration of mechanical properties. There was the question to what depth chemical corrosion reaches and how much mechanical properties are affected. Mechanical properties in particular levels of damaged timber were established by special tests of small tensile samples. The samples were taken from the truss construction of a former brewery malthouse in Děčín (North Bohemia – ČR) (Fig. 3). The surface of the timber investigated manifested an advanced level of fibrillation (Fig. 4). Fig. 3 Truss construction in the former brewery in Děčín Fig. 4 A detail of an analyzed beam surface The tensile strength parallel to the grain was tested using small triangular samples (5×5×7.5 mm) 200 mm long. The specially made small samples allowed for a more accurate establishment of a property investigated at various depths under the surface of the damaged timber. The samples were made from the superficial layer of the timber (0 – 5 mm – damaged layer) and the inner part of the timber (25 mm deep – undamaged layer, reference samples). The considerable deterioration of mechanical properties of timber in the damaged surface layer was manifested by a 50 % decrease in strength compared to the values ascertained in undamaged timber (Tab. 1). The surface was damaged to a depth of 5 mm, which was confirmed using small tensile samples (Kloiber et al. 2010). 72 PART II- ASSESSMENT OF REFERENCE PROPERTIES Table 1 Mean values of strength and modulus of elasticity from the tests of small tensile samples in the surface (damaged) and inner (undamaged) layers of timber Tensile tests parallel to the grain Beam side Strength S c (MPa) Modulus of elasticity M OE (MPa) surface inner surface inner Top 18.85 47.49 14801.66 12541.10 Bottom 17.52 55.16 16116.45 13957.38 Lateral 20.15 40.86 12444.37 13261.16 1.4 Summary The testing of small tensile samples is a direct and partially destructive method which can be used for the measurement of modulus of elasticity and tensile strength parallel to the grain. The method is not compromised by uncertain correlations between the measured and the estimated parameters. The tensile properties of small clean wood samples are measured directly but their information capacity is reduced by the high variability of results dependent on the effect of earlywood/latewood proportion. The method only gives information about timber in the close vicinity of the element surface, similarly to method Hardness test presented in Riggio and Piazza, 2011. 1.5 Recommendations It is recommended to choose a sufficiently large part of timber surface without defects – typically, a band of 20 mm x 300 mm is needed for the method application. Sampling demands that the guides are fixed either directly on the surface or on an auxiliary construction so that the sampled band area merges with the plane of the guides. The band axis needs to be in the same direction as the axis of the guides and the direction of fibres. It is recommended to determine the fiber direction using light scratching the surface between the annual rings. If, for the reasons of the element geometry, the sampling orientation cannot be maintained, it is necessary to correct the strength values measured based on table dependences (e.g Bodig, 1993). The samples in the test need to be loaded coaxially so that their bending and thus effect on measured quantities are prevented. Moisture content should be measured or controlled during sampling and laboratory testing as the values of mechanical properties decrease with increasing moisture content. Moisture content of 12% is recommended for the tests. Accurate measuring of sample dimensions is a prerequisite for the test interpretation and establishment of mech. properties. 73 PART II- ASSESSMENT OF REFERENCE PROPERTIES 2 Compression strength of cores 2.1 Sampling and testing methodology Testing of radial cores is a semi-destructive method. Samples are of a cylindrical shape (Fig. 5) and they are used to establish strength and modulus of elasticity in compression parallel to the grain using a special loading device (Kasal et al. 2003). The holes that remain after sampling are smaller than most knots that appear in timber elements and they do not reduce the element strength considerably meeting thus the requirements of conservation institutes regarding low invasiveness (Kasal and Antony, 2004). The sampling holes can be plugged to prevent moisture penetration, insect attacks, probability of decay or if aesthetic qualities are to be preserved (Kasal, 2003). Radial cores are 4.8 mm in diameter and the holes in the element are 10 mm in diameter. The length of the cores should be at least 20 mm to ensure reliability of results and elimination of result variability in consequence of early- and latewood alterations. Fig. 5 Taking a cylindrical sample Fig. 6 Equipment for sampling of radial cores Radial cores are taken using an electric drill with a special bit (Fig. 6), which was developed in ITAM, ASCR. Occasionally, soap or wax is applied to facilitate drilling. The drilling speed must be constant and the drilling is usually performed in steps to prevent damage to samples. The bit tip must be sharp and clean. Blunt and dirty bits cause damage to samples. The samples are transported to the laboratory in containers that prevent their damage and moisture content changes. The containers are marked with a number, place and date of sampling and other important information (Drdácký et al. 2005). 74 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 7 A detail of the loading device Fig. 8 An example of the stress-strain diagram for the compression test of a radial core The samples should be extracted from healthy and undamaged material in the radial direction because the tree-ring orientation is an important basis for correct testing. The shear forces that can be very high during drilling make the sampling conditions unfavourable. Therefore, the drill construction eliminates them. Due to the threat of drill sideways motion, the drill is fitted in a special device ensuring fixation and constant progress of the bit into the material. Radial cores can be used for examining other properties of wood such as density, moisture content, modulus of elasticity and compression strength parallel to the grain. It can also be used for the determination of the tree species, dendrochronological dating, microscopic analysis of decay, and visual evaluation of the element condition and the penetration of protective agents (Schwab et al. 1982). The actual testing of radial cores uses testing grips with grooves that facilitate loading in the direction perpendicular to the core axis, i.e. parallel to the grain (Fig. 7). Two linear-variable displacement transducers (LVDT) are used for monitoring the distance between the grips and thus the radial core deformation. A correct insertion of the radial core in the testing apparatus is critical for the correct determination of the compression strength and the modulus of elasticity. Wood has the highest strength in the grain direction, and uncentered radial cores in the grips lead to higher variability of results (Lear, 2005). The compression force and the core deformation are recorded in a stress-strain diagram, see Fig. 8. The compression strength is calculated as follows: fc = Fmax l ⋅ dc [MPa] where fc – compression strength [MPa], Fmax – load [N], load Fmax is taken from the diagram, see Fig. 8, l – radial core length [mm], dc – radial core diameter [mm]. Kloiber and Kotlínová (2006) found the correlation between the strength of radial cores and the strength of standard specimens in the longitudinal direction. 75 PART II- ASSESSMENT OF REFERENCE PROPERTIES Schwab et al. (1982) established the coefficients of determination in the interval R2 = 0.77–0.96 for the same dependence, in dependence on the wood species. Kasal (2003) found a strong dependence between moduli of elasticity in compression parallel to the grain for radial cores and (ASTM 143-94) samples (American Technical Standard), coefficient of determination R2 = 0.89. The variability of measuring is comparable for both methods (Kasal, 2003). One of the problems when establishing the regression between the properties of radial cores and standard specimens is the destructive character of both methods due to which both of the methods cannot be used for absolutely the same samples. 2.2 Limitations Due to the dimensions of the radial cores, this method is of local character. Therefore, it may not provide relevant information about the condition of the integrated timber because of wood variability. This inefficiency can be eliminated and the reliability increased by a higher number of samples taken from one element. However, this step would increase the damage done to the element, the time consumed, and the expenses of field measuring and the strength of the element would decrease (Kasal, 2003). The testing sample is extracted using a special bit which is fixed in an electric or manual drill (Fig. 6). The bit outer diameter is 9.5 mm. Speed is controlled during drilling so that the samples are not damaged. For the same reason, the bit tip needs to be kept sharp and clean. Blunt or dirty bits can cause that the samples look damaged or decayed, or they can be pushed outside the bit, which creates distortion of results. The samples should be extracted from healthy and undamaged material in the radial direction because the tree-ring orientation is vital for the correct test. The shear forces that can be very high during drilling make the sampling conditions unfavourable. Therefore, the bit inner diameter decreases towards the tip. To eliminate a possible sideways motion the bit is fitted in a special device which ensures fixation and constant speed towards the material. Radial cores can be used to establish physical, mechanical and strength properties of timber. When investigating moduli of eleasticity, it is necessary to release the load partially from the radial core during testing (Fig. 9) and then measure the elastic response of the core to the change of external loading only; otherwise, considerable inaccuracy occurs (Micka et al. 2006) as the total sample deformation is affected by the plastic deformation in the places of contact with the grips. Radial cores can also be used to determine density. This is especially important for valuable timber elements, in which every piece of material matters. The variability of the data gained is comparable with standard tests. However, radial cores need to be taken from undamaged places. 76 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 9 Stress-strain diagram force – compression with partial release Fig. 10 Correlation of pressure deformation characteristics of the radial cores with the number of annual rings. (Micka et al. 2006) 2.3 Application Radial cores have been successfully used for non-destructive surveys of timber constructions e.g. with the aim to find out mechanical properties of a timber construction of storage halls in the trade fair facilities in Brno (South Moravia – ČR) or the quality of the ceiling timber in the St. Mary’s Tower of the Karlstejn castle (Central Bohemia – ČR). In the case of the St. Mary’s Tower, we had a sample of an authentic beam from a damaged part of the building (emperor palace stables). We used this piece for calibration tests in compression parallel to the grain in compliance with (ASTM 143-94). We tested short columns cut from the beam with exactly oriented fibres. Further, radial cores were sampled so that each standard sample by ASTM was matched with two cores taken from each end of the specimen. In total, 38 radial cores were available. Typical deformation properties (modulus of elasticity in compression parallel to the grain) were investigated using both the radial core samples and the standard samples. The values correlated very well. The mean values for the modulus of elasticity and compression strength ranged around 7600 N/mm2 and 42 N/mm2, respectively. The characteristic values with 5% quantile followed, reduced based on the appearance of defects in the element. For the reduction, visual assessment was used (Drdácký et al. 2003). Further, non-standard tests were conducted using 12 radial cores from the joist of the treasure room ceiling. The found values of deformation characteristics correlate with the tests of cores from the reference beam from the emperor palace stables. The comparison shows that the mechanical properties of the treasure room ceiling timber elements were of the same quality as the reference beam whose strength and modulus were established by ASTM standard tests (Fig. 10). The values of mechanical properties showed a very high quality of the historic timber. 77 PART II- ASSESSMENT OF REFERENCE PROPERTIES These values can be used to determine design characteristics for the purpose of construction safety assessment in a common way (Drdácký et al. 2003). 2.4 Summary Radial cores are to be used for a direct establishment of physical (specific density), morphological (tree-ring width) and mechanical properties (compression strength parallel to the grain and modulus of elasticity) with a relatively high accuracy in defectless timber. The cores can also be used for microscopy, dendrochronology, visual assessment, and measuring of protective agent penetration. 2.5 Recommendations The cores need to be taken with a special hollow bit in the radial direction, i.e. the direction of a normal to annual rings so that the test of mechanical properties can be performed parallel to the grain. An area with a diameter of about 70 mm is needed for the sampling as the drill fittings need to be fixed. The fittings ensure the bit movement in the radial direction without deviations and allow for a gradual drilling into the demanded depth with constant speed. After the demanded core depth is achieved (usually 40 mm), the bit is taken out and a thin-walled tube is inserted. The tube is used to take the core out of the timber. The core is then pushed out of the tube. Broken or damaged cores are excluded from the test. Moreover, the core needs to be placed into the testing grips with high accuracy. Moisture content of 12% is recommended for the tests. Accurate measuring of sample dimensions is a prerequisite for the test interpretation and establishment of mechanical properties. 3 Compression strength in a pre-drilled hole 3.1 Testing methodology The range of the existing methods and devices lacked a solution enabling the measurement of mechanical properties of wood using gently destructive investigation of its behaviour when being loaded by a miniature loading jack inserted in a predrilled hole. Determine exact mechanical properties and strength grades important for structural design (Machado, 2013). During the application the dependence of deformation on the voltage is measured while symmetrically arranged grips ("stones") are being pushed apart in a pre-drilled radial hole with a diameter of 12 mm (Drdácký and Kloiber, 2013). The semi-destructive procedure of making a hole into the tested material allows the investigator to assess other aspects of the material condition (e.g. based on the core, sawdust, videoscopy, etc.). 78 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 12 A detail of a drawbar with a push-apart wedge and rounded grips Fig. 11 A view of the device The device (Fig. 11) is designed to measure mechanical properties of wood using gently destructive investigation of its behaviour when loaded by the miniature loading jack inserted in the prebu-drilled hole. The device can be used both in the laboratory and in the field to assess the condition and the quality of timber. The advantage of the device is the possible gradual recording of the force and shift of grips (loading jack) at different depths corresponding to the required dimensions of commonly investigated constructions. The device is laid on the tested unit (usually a constructional element of a rectangular profile) by means of a cylindrical shell, which allows for measuring in four positions of the pre-drilled hole. The shell arresting is provided by two grooved screws, for positions (core depths) 5– 25, 35–55, 65–85, and 95–115 mm. When the measuring part of the device is inserted in the drilled hole and the device is laid on the tested element, the rounded grips are pushed apart by the drawbar with a push-apart wedge (Fig. 12) into the walls of the hole. The maximum depth of possible loading on both sides is 1.5 mm. The rounded grips are 5 mm wide and 20 mm long. The grips also include flexible arms whose movement during pushing is provided by a push-apart bronze wedge fitted to the lower end of the drawbar by means of a pin and screw. The apex angle of the wedge is 15°. This angle is not self-locking and to release the grips it is sufficient to release the push-apart force (Drdácký and Kloiber, 2013). The force of the drawbar when pulling out is continually scanned and recorded. It is calibrated to the real force of the loading jack and simultaneously related to the measured distance of movement of the grips (Fig. 13). The signals are wirelessly transmitted to a portable computer, where they are processed. 79 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 13 Example of the device output: record of the force of grip pushing apart related to the measured distance of movement of the grips Kloiber et al. 2013 introduced the construction and usage of this new device for in-situ assessment of integrated timber. The application of the new device was verified. It was found out that the device is sufficiently sensitive to the natural differences between individual elements of healthy timber. Strong correlations were mainly found for the measured CSC (L) strength in compression parallel to the grain and SC (L) strength of standard samples assessed in compliance with ČSN 49 0111 (correlation coefficient 0.92). The relations were described by practically usable linear regression models. The measured compression strength parallel to the grain correlates with the other investigated timber parameters, e.g. density (correlation coefficient 0.87). Another parameter for the assessment of mechanical properties using the new device was MOD (L) modulus of deformability, which correlates well with MOE (L) modulus of elasticity parallel to the grain (correlation coefficient 0.87). The construction of the device is lightweight and due to its independence from the electrical grid, it is easy to use in the field. In contrast to other methods, the new device enables a highly accurate establishment of mechanical properties in the entire depth profile of the assessed element. 3.2 Limitations The prerequisites of an appropriate use of the method are drilling a hole through the wood fibres purely in the radial direction, where there is a regular alternation of earlywood and latewood within annual rings, and the orientation of the measuring probe parallel to the grain; in structural elements it is generally parallel to the axis of the element. Measuring is affected by a higher proportion of earlywood or latewood within a tree ring in the tangential direction, which leads to distorted results. The hole needed for the test is created by a bit which is fixed in an accumulator drill. To prevent sideways motion of the bit, the drill is fitted to a special stand which fixes it to the element. The outer diameter of the bit is 12 80 PART II- ASSESSMENT OF REFERENCE PROPERTIES mm. Speed is controlled during drilling so that the hole is not damaged. For the same reason, the bit must be maintained sharp and clean. Blunt or dirty bits can cause fibres being torn out of the hole walls, which distorts the results. The hole should be made to undamaged places of the element without visible defects and damage. An essential feature of the in-situ testing is the fact that the measuring of a loaded element is conducted with unknown internal forces present. It was proved by measuring the deformation around the drilled hole using image digital correlations that the state of tension recedes after drilling into a distance of about 2 mm from the hole edge and the measuring is thus not affected by the inner tension of the constructional element unless the element was damaged by the elasticity limit being exceeded. The above mentioned assertion has been verified by tests of a bended timber console (Maddox at al. 2014). 3.3 Application The method for the establishment of strength in a pre-drilled hole has been successfully used for the investigation of mechanical properties of the timber truss of the St. Mary’s Church in Vranov nad Dyjí from the 17th century (South Moravia - ČR) or when investigating the quality of a larch ceiling from the 14th century in Spišské podhradí (UNESCO site - SK). In the case of the Vranov nad Dyjí truss, four samples of tie beam ends were available. They were taken away because timber scarf joints were to be used instead of the damaged ends. The aim was to verify the application of the device using the wood of Silver Fir (Abies alba Mill.) in the common variability of properties of timber integrated in a historic building. The measuring by the new device was conducted in 135 positions. Decayed beam ends were also measured but due to the low values gained, the results were not taken into account. Mechanical properties were determined from the record of measured data in the form of a stress-strain diagram showing the force of drawbar pulling out, which was calibrated to the real force of grip pushing apart and simultaneously related to the measured distance of grip movement. Measured strength CSC was determined from the ratio of the ultimate load and the area of the grips. Modulus of elasticity cannot be calculated from the stress-strain diagram directly; however, the modulus of deformability was determined based on the force slope and deformation. The new device was verified by experiments based on the comparison of values measured during grips being pushed apart in a drilled hole and the results of standard sample testing by destructive tests in compliance with ČSN 49 0111 using a universal testing device. Two standard samples with dimensions 20x20x30 mm, complying to ČSN 49 0111 were cut from places adjacent to the positions measured by the new device. Compression strength parallel to the grain established based on the standard samples was correlated with the results of the new device. 81 PART II- ASSESSMENT OF REFERENCE PROPERTIES Strong correlations were mainly found for CSC (L) measured strength in compression parallel to the grain and SC (L) strength of standard samples (correlation coefficient 0.75). The relations were described by practically usable linear regression models. Similar dependences are found when the pin penetration device is used (Kloiber et al.). The initial tests conducted using timber from the historic truss construction showed that the new method is sufficiently sensitive to natural changes in properties (distribution along the element width). It should be noted that the natural material variability was increased by the presence of defects (knots and cracks). 3.4 Summary The advantages of this method include the high accuracy of the establishment of mechanical properties (measured strength and modulus of deformability in compression parallel to the grain) of timber tested and assessed in the field. In contrast to other methods, the new device is able to establish mechanical properties in the entire depth profile of the assessed element. The measuring is accurate if the drilling is oriented perpendicular to the grain in which direction early- and latewood alternate regularly within annual rings and if the grips are pushed apart parallel to the grain or parallel to the element axis in the case of constructional elements. The effect of larger proportions of earlywood or latewood in the tangential direction leads to a distortion of results. The results of measuring depend on the quality of the drilled hole production, i.e. it is necessary to check the bit constantly and replace blunt bits immediately. 3.5 Recommendations To guarantee the planeness of the drilled hole and to eliminate sideways motion of the bit, the drill needs to be fixed to the assessed element by means of a special stand during drilling. The stand can be fixed to the element directly or via an auxiliary construction. The fixing demands an area of 150 x 150 mm. To ensure a good quality of drilling, it is recommended to control the drilling speed, especially the bit progress into the hole. The hole should be drilled in undamaged places of the element without natural defects and visible damage. A higher number of holes improperly placed can affect the mechanical resistance of the element assessed. Like other in-situ methods used for the diagnostics of integrated timber, this method for the measurement of strength and modulus of deformability manifests a considerable dependence on the moisture content in the investigated material. Therefore, the measuring of moisture content in the tested place is an essential part of the test. 82 PART II- ASSESSMENT OF REFERENCE PROPERTIES 4 Mechanical resistance to pin pushing 4.1 Testing methodology A device for in-situ establishment of mechanical resistance to gradual pin pushing was developed in cooperation of the Institute of Theoretical and Applied Mechanics of the Academy of Science of the Czech Republic and the Department of Wood Science, Mendel University in Brno. The device measures the demanded values to the depth corresponding to typical dimensions of timber constructional elements and is applicable for an indirect establishment of density and mechanical properties of wood. Similar penetration test is based on repeated pin hammering into the wood by means of a hammer with a constant energy (Ronca and Gubana, 1998). Fig. 15 A detail of pin penetration through the device base during pin pushing Fig. 14 A view of the device for in-situ The device body can be fixed to the tested element in various ways, most often with a fabric strap (Fig. 14) or a roller chain. The device body can also be fixed to the tested element by mounting screws. After the device has been fixed to the object, a pin is gradually pushed into the timber perpendicularly to the device base (Fig. 15) by a toothed rack and pinion gear driven by two opposite manual cranks for both hands. The force of pin pushing is continuously recorded in relation to the distance measured (Kloiber et al. 2011). The measuring application processes the data, shows them in the real time and saves them. The progress of force measured 83 PART II- ASSESSMENT OF REFERENCE PROPERTIES in the real time is shown either in dependence on time x-t or in x-y mode together with pin displacement. During the measurement, basic characteristics are calculated by a PC. These are work [N.mm] as the area under the force curve related to the displacement, penetration length [mm], time of pin displacement [s] and the maximum and minimum force [N]. The mean force [N] necessary for pin pushing is calculated by dividing the area under the curve by the penetration depth. This parameter is of key importance for the assessment of the timber mechanical resistance. The continuous record of the force related to pin displacement is able to indicate a change in properties within the entire depth of pin penetration caused by either a natural distribution of properties or biodegradation. The curve of forces in the case of undamaged spruce (Fig. 16) corresponds to earlywood and latewood alternations within annual rings (latewood with a higher mechanical resistance and early wood with a lower mechanical resistance). The curve also describes the different tree-ring widths (increments) in the element cross-section. The general progress reflects the equal distribution of mechanical resistance in the cross-section, i.e. a balanced quality of sound spruce timber. When measuring the resistance of pine wood, there is again a visible difference between latewood and earlywood as well as tree-ring widths (Fig. 17). The record with increasing forces reveals that there is heartwood typical of pine wood with a higher density and mechanical resistance. The absolute values of forces correspond to the mechanical resistance to pin pushing in sound pine wood. Fig. 18 shows a record of measuring a spruce element containing biodegradation. The relative decrease in the zone with decay compared to sound wood and the absolute force values indicate a decrease in mechanical resistance. Fig. 16 Record of the force related to pin displacement - spruce wood Fig. 17 Record of the force related to pin displacement - pine wood 84 PART II- ASSESSMENT OF REFERENCE PROPERTIES To sum up, the device is applicable for a wide range of properties of sound as well as damaged wood. The test results manifest very good correlations of the mean force needed for pin pushing with wood density and strength determined using standard samples in compression perpendicular and parallel to the grain (Kloiber et al. 2009; Tipner et al. 2011). The measured parameter can be changed by a simple replacement of the indentation pin with a hook for withdrawal of screws or other fixings, as for example presented in Yamaguchi, 2011. Fig. 18 Record of the force progress and displacement of pin pushing into spruce wood with decay and feeding of wood-damaging insects (Tannert et al. 2014) 4.2 Limitations The device was designed and tested for the assessment of wood integrated in buildings, both sound or with various levels of degradation. The device records a relatively wide range of timber mechanical resistance to pin pushing caused by natural properties of different tree species as well as different levels of degradation. The resistance is affected by the species, wood quality and density but also moisture content (Tannert et al. 2014). These parameters need to be taken into account when interpreting the results. Potential wood defects, such as cracks, knots, foreign objects, etc. considerably distort the results. It is advisable to avoid measuring in places with wood defects, or interpret results of such measuring very cautiously. It is necessary to push the pin into wood in the direction perpendicular to fibres - only in the radial direction - where earlywood and latewood alternate regularly. 4.3 Application Visual inspection of the flat roof truss construction of the Čechy pod Kosířem Castle Orangery (North Moravia – ČR) conducted in 2011 proved that the truss and ceiling timber is locally damaged by wood rot and insects. Damaged places were found at the ends of tie (ceiling) beams, where rainwater had leaked and had provided favourable conditions for brown rot. The resulting rot changed physical properties of the timber (colour, decrease in density, increase in absorption, etc.). Wood mass was considerably disintegrated at some places. 85 PART II- ASSESSMENT OF REFERENCE PROPERTIES The wood-decaying insects identified as the cause of the general damage of constructional elements were Cerambycidae or Anobiidae. The attacked tie beam had to be replaced or fitted with scarf joints. The renovation needed to be approached with utmost caution and maintain the largest possible proportion of historic material. The construction of the Orangery truss was divided into 25 cross sections, each containing a tie (ceiling) beam and a rafter. The construction renovation of the truss was designed based on visual inspection and mainly results of mechanical resistance measuring by the diagnostic device with a pin 2.5 mm in diameter (Fig. 19). A third of the total volume of the elements was deemed for replacement. The accurate establishment of damage helped save a large part of the material, which despite the surface damage (Fig. 20) met the necessary mechanical properties to the same or higher extent than new timber. Fig. 19 Investigation of a tie beam condition using pin pushing Fig. 20 A detail of damage to a tie beam, which was left in the original position Fig. 21 shows the record of measuring of a tie beam with surface rot and damage by wood-damaging insect feeding. The measuring was conducted using the device with pin pushing method. The device was fixed to the element by a fabric strap and the force needed for pin pushing was developed continuously by two cranks (Fig. 21). The distance and force were recorded during pushing. The relative decrease in the zone with rot and feeding compared to sound wood and the absolute force values indicate a decrease in mechanical resistance caused by degradation to a depth of 15 mm only. 86 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 21 The record of measuring tie beam 8 northern end, where only 15 mm layer of surface was damaged 4.4 Summary The method of measuring the wood mechanical resistance to pin pushing can be used to estimate parameters of wood density and strength, up to a depth of 110 mm. By contrast to the commonly used Pilodyn, this method provides data about a larger cross-section part of the tested element and allows the researcher to identify internal defects hidden deep below the timber surface. The slow progress of pushing enables the researcher to quantify damage in any depth. The size of the resistance recorded is affected by the wood species, wood quality and density, as well as moisture content. These parameters need to be considered for a correct interpretation of results. Potential wood defects, such as knots, cracks, foreign objects, etc. distort the results considerably. 4.5 Recommendations The test demands a free area of 150x150 mm so that the device can be fixed. It is recommended to avoid measuring in places with defects as the interpretation of results is then difficult. Pin pushing is only accurate if the device is fixed perpendicular to the grain and if the pin penetrates the timber in the radial direction. The acceptable deviation is about up to 10° from purely radial direction. When the pin is pushed in the tangential direction, the results may be distorted as the pin then often penetrates the weaker earlywood only and does not enter denser latewood increments in heterogeneous wood types. The measuring of moisture content in the tested place is again an important part of the test. 87 PART II- ASSESSMENT OF REFERENCE PROPERTIES 5 Conclusion Testing of small tensile samples is a direct, partially destructive method that can be used for strength and modulus of elasticity measuring in tension parallel to the grain. The method is not hindered by uncertain correlations between measured and estimated parameters. However, the method is sensitive to deflections of wood grain from the sample longitudinal axis. The sample cross-section is small, which strengthens the effect of early- and latewood alternation in annual rings. This effect cannot be avoided, which means that the results (strength and modulus of elasticity) are highly variable and the selection of suitable places for sampling is vital. In-situ sampling and laboratory testing are time consuming and costly. The method only informs about superficial properties of an element without defects; moreover, it represents damage to the surface of the assessed element. The method of radial cores represents a smaller invasion in the material based on taking cylindrical samples that are used to test strength and modulus of elasticity in compression parallel to the grain using a special device. The holes that remain after the core is removed are smaller than most knots and are located not to deteriorate the element strength. The unfavourable effect of earlywood and latewood alternations within annual rings is sufficiently diminished if the core length is at least 20 mm. The cores can be used also for microscopy, dendrochronology, visual assessment and measuring of protective agent penetration. The core diameter is 5 mm only, i.e. the method is of local character. Due to the high variability of wood, the core may not provide a good idea about the mechanical properties of the element investigated. This deficiency can be countervailed by a larger number of cores taken from an element. In-situ sampling and laboratory testing are time consuming and costly, just as in the case of small tensile samples. To reduce the costs and the time needed, we devised a method for in-situ direct establishment of strength and modulus of deformability in compression parallel to the grain in a pre-drilled hole with 12 mm in diameter. With this method no sample needs to be taken for laboratory tests. The method measures mechanical properties very accurately in any depth of the timber element. The unfavourable effect of earlywood and latewood alternations within annual rings is counteracted by grips of 20 mm in length. Again, wood variability needs to be taken into account as it affects the mechanical properties determined locally. The method of pin pushing is the least invasive out of the presented methods. The hole created has 3 mm in diameter only. By contrast to dynamic indentor (Pilodyn), the length of the pin and thus the depth of the penetration into the investigated element allows for the identification of internal defects. Thanks to the slow progress of pushing, the values of mechanical resistance are gainedgradually. Mechanical resistance correlates well with mechanical properties. 88 PART II- ASSESSMENT OF REFERENCE PROPERTIES The disadvantage of this method is the necessity to fix the device to the element investigated. Just like the other invasive methods for timber diagnostics, this method depends heavily on internal factors, moisture content, and tree species. Table 2 A synoptic table describing the success rate of prediction of mechanical properties, the time consumed and the extent of invasive damage caused by the presented methods in comparison with commonly used methods Methods described in the chapter Tensile strength of m icrosam ples Com pression strength of cores Com pression strength in a drilled hole Mechanical resistance to pin pushing Mechanical properties in the elem ent surface 60-90 % 60-90 % 60-90 % 40-70 % Mechanical properties to a depth of m in. 100 m m 30-60 % 60-90 % 60-90 % 50-80 % Test tim e consum ption high high low low Extent of invasion high low low negligible Methods comm only used Mechanical resistance to pin penetration (Pilodyn) Mechanical resistance to screw w ithdraw al Hardness test (Piazza) Microdrilling energy Mechanical properties in the elem ent surface 50-80 % 50-80 % 50-80 % 30-60 % Mechanical properties to a depth of m in. 100 m m 30-60 % 30-60 % 30-60 % 40-70 % Test time consum ption negligible low low low Extent of invasion negligible low negligible negligible Acknowledgments This paper was created with a financial support from grant project DF11P01OVV001 “Diagnostics of damage and life span of Cultural Heritage buildings”, NAKI program, provided by the Ministry of Culture and research supported by the project CZ 1.05/1.1.00/02.0060 from the European Regional Development Fund and the Czech Ministry for Education, Youth and Sports. References 1. ASTM: Annual Book of ASTM Standards, Section 4. Construction. 04.10 Wood. ASTM, Philadelphia, PA. 2002. 89 PART II- ASSESSMENT OF REFERENCE PROPERTIES 2. ASTM: D 143-94 Standard Test Methods for Small Clear Specimens of Timber. ASTM International. For referenced ASTM standards, 2000. 3. Bodig, J.: Mechanics of wood and wood composites. Malabar: Krieger Publish. Comp. 1993, 712 pp. 4. ČSN 49 0110: The breaking strength in compression along fibres, 1980. 5. ČSN 49 0111: Tests of the properties of solid wood. Method of detection of the module of elasticity in compression along fibres, 1992. 6. Drdácký, M., Jirovský, I., Lesák, J., 2003, Non-destructive survey of masonry and timber structures of the Maria Tower on the Karlštejn Castle, Research Report ITAM-ARCCHIP, Praha, 2003, 62 p. 7. Drdácký, M., Jirovský, I., Slížková, Z.: On Structural Health and Technological Survey of Historical Timber Structures. Proceedings of the International Conference The Conservation of Historic Wooden Structures, Florence, Vol. I, 2005. pp. 278-284. 8. Drdácký, M., Kloiber, M.: In-situ compression stress-deformation measurements along the timber depth profile. In: Advanced Materials Research 778: Trans Tech Publications, 2013, pp. 209-216. 9. Kasal, B., Anthony, R.: Advances in in situ evaluation of timber structures. Progress in Structural Engineering and Materials. John Villey & Sons Ltd. London. UK. Vol. 6 No 2 April-June 2004, pp. 94–103. 10. Kasal, B., Drdácký, M. Jirovsky. I.: Semi-destructive methods for evaluation of timber structures. Structural Studies, Repairs and Maintenance of Heritage Architecture VIII. C.A. Brebia, Editor. Advances in Architecture. WIT Press. Southampton, 2003, pp. 835–842. 11. Kasal, B.: Semi-Destructive Method for In-situ Evaluation of Compressive Strength of Wood Structural Members. Forest Products Journal, 53 (11/12), 2003, pp. 55–58. 12. Kloiber, M., Drdácký, M., Tippner, J., Sebera, V.: New construction NDT device for in situ evaluation of wood by using compression stress-deformation measurements parallel to grain. In: 18th International Nondestructive Testing and Evaluation of Wood Symposium, 2013, September 24-27, Madison, Wis-consin, USA. FPL-GTR-226: pp. 585-592. 13. Kloiber, M., Frankl, J., Drdácký, M., Kučerová, I., Tippner, J., Bryscejn, J.: Change of mechanical properties of Norway Spruce wood due to degradation caused by fire retardants. In: Wood Research, Vol. 55(4): 2010, Slovakia. ISSN: 1336-4561, pp. 23-38. 14. Kloiber, M., Kotlínová, M., Tippner, J.: Estimation of wood properties using pin pushing in method with various shapes of the penetration pin. In: Acta Universitatis Agriculture et Silviculturae Mendelianae Brunensis, ISSN: 1211-8516, LVII, 2/2009, Brno, pp. 53-60. 15. Kloiber, M., Kotlínová, M.: Prediction of mechanical properties by means of radial cores in situ. In: In-situ evaluation & non-destructive testing of historic wood and masonry structures, RILEM Workshop, 10-14 July 2006, Prague, ISBN: 978-80-86246-36-9, pp. 56-65. 16. Kloiber, M., Tippner, J., Drdácký, M.: Semi-destructive Tool for "In-situ" Measurement of Mechanical Resistance of Wood. In: SHATIS´ International Conference on Structural Health Assessment of Timber Structures, June 2011, Lisbon, Portugal. 3 pp. 17. Kloiber, M., Tippner, J., Hrivnák, J., Praus, L.: Experimental verification of a new tool for wood mechanical resistance measurement. In: Wood Research 57(3): 2012, Slovakia. ISSN: 1336-4561, pp. 383-398. 18. Lear, G.Ch.: Improving the Assessment of In Situ Timber Members with the Use of Nondestructive and Semi-Destructive Testing Techniques. M.S. thesis – North Carolina State University, Raleigh, 2005, 137 pp. 90 PART II- ASSESSMENT OF REFERENCE PROPERTIES 19. Maddox, J., Drdácký, M., Kloiber, M, Kunecký, J.: In-situ assessment of strength of historic th wood In: 9 International Conference on Structural Analysis Historical Constructions, 2014. 20. Machado, J.S.: In situ Evaluation of the Reference Properties of Structural Timber Members. Use of Available Tools and Information. In: Advanced Materials Research, 2013, Vol. 778: pp. 137-144. 21. Micka, M., Minster, J., Václavík, P.: Compression test of a timber core – An-sys model and Moiré interferometry experiment. In Engineering mechanics 2006, Svratka, 2006, pp. 219/1-219/12. 22. Riggio, M., Piazza, M.: Hardness test. In: In Situ Assessment of Structural Timber: Discussion of Classical and Modern Non-Destructive and Semi-Destructive Methods for the Evaluation of Wood Structures; Series: RILEM State of the Art Reports, Kasal B.; Tannert T. (Eds.), Springer, 2011, Vol.7: pp. 85-95. 23. Ronca, P., Gubana, A.: Mechanical characterisation of wooden structures by means of an in situ penetration test. Elsevier Publishing Co., Oxford, England. Construction and Building Materials, 1998, Vol. 12(4): pp. 233-243. 24. Schwab, E., Wasshau, A., Willetneier, H.: Bohrkerne. Zur Beurteilung der Festigkeit holzerner Rammpfahle. Bauen mit Holz (9), 1982, pp. 566–570. 25. Tannert, T, Anthony, R., Kasal, B., Kloiber, M., Piazza, M., Riggio, M., Rinn, F., Widmann, R., Yamaguchi, N.: Recommendation of RILEM TC 215-AST: In-situ assessment of structural timber using semi-destructive techniques. In: Materials and Structures: 2014, Netherlands. ISSN: 1359-5997. DOI: 10.1617/s11527-013-0094-5 26. Tippner, J., Kloiber, M., Hrivnák, J.: Derivation of Mechanical Properties by Pushing of a Pin into Wood. In: 17th International Nondestructive Testing and Evaluation of Wood Symposium, 9/2011, Sopron, Hungary. ISBN: 978-963-9883-83-3, Vol. 2: pp. 575-582. 27. Yamaguchi, N.: Screw Resistance. In: In Situ Assessment of Structural Timber: Discussion of Classical and Modern Non-Destructive and Semi-Destructive Methods for the Evaluation of Wood Structures; Series: RILEM State of the Art Reports, Kasal B.; Tannert T. (Eds.), Springer, 2011, Vol.7: pp. 81-86. 91 PART II- ASSESSMENT OF REFERENCE PROPERTIES 92 PART II- ASSESSMENT OF REFERENCE PROPERTIES Practical procedure for estimating the density of timber with portable X-ray equipment Thomas lechner, PhDa), Robert Kliger, Professorb) a) NCC Construction Sverige AB and Chalmers University of Technology, Gothenburg, Sweden b) Chalmers University of Technology, Gothenburg, Sweden Abstract Wood density has a strong relationship with several mechanical properties, such as strength and stiffness. An X-ray image calibration procedure, which enables the determination of density for the in-situ assessment of timber structures, has been developed. This non-destructive method is useful for evaluating the internal condition for global assessments of the structure. Finally, a calibration wedge was set up to verify the procedure. The density calibration procedure from X-ray images was verified on a timber beam specimen, resulting in good agreement and an average accuracy of 97%. The values obtained from the image calibration presented a very good linear correlation between the measured density and the greyscale from X-ray images, with coefficients of determination (R2) ranging from 0.90 to 0.98. The main advantage compared with conventional techniques is the detection and quantification of internal damage, defects, disturbances and deterioration that may reduce the mechanical properties of the structure. This study shows good potential when it comes to the development of a viable tool for in-situ assessments of timber structures. In a subsequent step, the above-mentioned procedure was also implemented in two case studies of historical wooden structures in Sweden. This technique could be used indirectly in analyses of structural behaviour. Introduction Timber structures are generally complicated when it comes to condition assessment. This is particularly true in the case of structures and buildings of historical value, when ageing can be suspected of having a diminishing effect on their strength and stiffness or abnormal structural behaviour has been discovered. It is therefore of great importance to adopt structural health-monitoring techniques to assess the remaining load-bearing capacity of timber structures. Through the reliable and appropriate assessment and monitoring of timber structures, it is possible to detect any weaknesses at an early stage and appropriate action can then 93 PART II- ASSESSMENT OF REFERENCE PROPERTIES be taken to extend the service life of the structures. This kind of assessment often requires appropriate non-destructive testing (NDT) and quasi-nondestructive testing techniques. Improved, new methods based on scientific knowledge and guidelines are needed for their application. The application of digital imaging processing and increasing resolution has made it possible to quantify and assess components inside timber elements, such as the internal deformation of fasteners and the dimensions of hidden elements and strains [1]. However, the aim of this paper is to propose a practical methodology for assessing the density of timber in situ using X-ray measurements. These measurements are based on X-ray attenuation, as it is impossible to measure wood density directly with X-rays. Density is an important parameter when defining wood materials. Wood density is strongly related to stiffness and strength properties and can therefore be used in the evaluation of timber structures [2]. The definition is, however, problematic, as both mass and volume are dependent on moisture content. In this case, the estimated density relates to structural timber in the in-situ condition and the moisture content is related to the relevant service class. The basic principles of X-ray attenuation were used in this study to establish an in-situ calibration procedure to predict density on site. The method which will be described produces local property values of density measurements using an X-ray calibration procedure. Furthermore, this procedure can also be used to evaluate density distribution in all timber structures. The variation in density in a piece of timber can be seen using photographic imaging [3]. General specifications of the X-ray equipment Radiographic investigations can be conducted using X-ray densitometry, diffraction analysis, computed tomography (CT) and micro-tomography and they are mainly used for the quantitative assessment of wood properties of different species, the detection of deterioration and to acquire knowledge of whether the element is sapwood or heartwood by researching the density profile. These differences can be detected through the attenuation of X-rays [4-5]. X-rays are short-wavelength electromagnetic radiation travelling at the speed of light. These rays are not affected by electromagnetic fields and can be diffracted but not deflected. Emitted X-rays lose intensity and this appears as lighter/darker in terms of greyscale values (RGB) on the imager [6]. The penetration capability and intensity of the radiation are controlled by the electric potential (kV), the current (intensity, mA) of the X-ray tube and the expo- 94 PART II- ASSESSMENT OF REFERENCE PROPERTIES sure time. The penetration is the intensity projection on the image plate and it is governed by: The type of material and the material characteristics The material composition The density of the material The porosity of the material and its moisture inclusion The attenuation factor (µ) The penetration thickness of the X-rayed object. In digital form, the image can be expressed as a matrix and processed in an image-processing toolbox, such as the one in Matlab®, to quantify and compare relative positions in real-time radiography, for example. The equipment used in the studies was a battery-powered portable X-ray source, Inspector XR200® from Golden Engineering Inc. However, other X-ray equipment can be used in situ. The digital image plate system, DIMAP® from Logos Imaging Inc., was used to scan the photographic X-ray images using reusable phosphor-layered imaging plates that capture the intensity levels from the X-ray exposed objects. An example of an X-ray set-up, which includes the principle for the X-ray procedure, X-ray source and the digital image plate system, is shown in Fig. 1. The X-rays leave the tube at a certain exit angle, which is decisive for the minimum distance to the specific object to ensure the maximum utilisation of the imaging plate. The laser scanner releases the accumulated energy from the image plate and stores the image at selectable resolution on the laptop imaging software, where every single image can be post-processed in terms of specific details. The safety instructions from the manufacturer regarding the danger of X-rays must be followed carefully in order to avoid any kind of harm. Fig. 1 Example of X-ray system and recording process. The upper part illustrates the principle for the X-ray procedure, whereas the lower part shows the X-ray source and the digital image plate system, DIMAP® from Logos Imaging Inc. 95 PART II- ASSESSMENT OF REFERENCE PROPERTIES Applications of radiographic measurements Until recently, the opportunities for X-ray investigation have been used for the qualitative assessment of timber structures, but the opportunities to carry out quantitative evaluations are of great importance. A number of applications for using X-ray equipment on site, which can be useful for the evaluation of structural behaviour, are revised in this paper. Depending on the material properties, such as the chemical properties, density and thickness of the inspected object, the energy absorption will vary and this is reflected by the photographic image [3]. Anthony also investigated termite activity using infrared thermography and acoustic non-destructive methods but without satisfactory success when it came to quantifying the loss of material [3]. By comparing the measured intensities on a radiograph, the extent of deterioration in wood members could be quantified using image processing techniques [3, 6]. Image enhancement techniques are a common technique when adjusting digital images [7] to facilitate the interpretation of deteriorated wood. The primary benefit when using X-rays is the opportunity to determine the condition of structures on site. Further advantages are the ability to acquire precise dimensions by measuring the distances between the X-ray source, the imager and the object of interest, the ability to identify the physical condition of wood such as rot, for example, to estimate the structural capacity, identify the types of connection, such as nails, bolts and so on, to detect corroded areas and to identify the construction details for historical dating [6]. All these advantages involve some difficulties, especially in crack identification, which requires an adequate size of at least 2% of the member thickness and must be oriented parallel to the radiation in order to be detected [8]. Limitations to the intensity or energy level can also limit the investigation [8]. Real-time radiography (radioscopy) allows the study of component behaviour under moderate loads and it is particularly suitable for timber structures due to the density differences. There are also several limitations to using X-ray for detecting defects (including cracks). They can be discovered with visual inspections and may be related to chemical contamination, variations in the attenuation coefficients, variations in the dimensions and the distribution of moisture. Detection of corroded areas As corrosion in metal fasteners might cause severe failure, radiographic equipment can be used as a tool to detect corrosion inside the structure and, by taking appropriate action, the collapse of the structure could be prevented [3]. Using commercial image-editing programs, distances can be measured fairly accurately in relation to a reference unit and the actual capacity of the fastener can be 96 PART II- ASSESSMENT OF REFERENCE PROPERTIES recalculated. Fig. 2 shows a nail that has corroded as a result of a shrinkage crack in timber. Fig. 2 Deterioration of the metal fastener due to corrosion in the shrinkage crack of the beam. Reduction of cross-section Old timber may have lost its full capacity due to deterioration either as a result of insect attacks or due to shrinking cracks [9]. Moreover, fungal degradation may reduce a cross-section. When accessibility with an X-ray camera along the fibre direction is guaranteed, a more reliable cross-section can be obtained and predictions of the maximum permissible stresses at a specific point could be made with a reduced cross-section, before any strengthening or remedial work is carried out. “Timber-to-timber” hidden geometry Hidden metal details in a timber structure can be assessed using X-ray. However, this does not necessarily mean that hidden timber details can be visualised with sufficient accuracy. As part of the current investigation, a preliminary study has been carried out and it shows promising results in this field, cf. Fig. 3. Fig. 3 A hidden dowel with approximately the same density as the surrounding wood can be detected using X-ray. Original X-ray image (top left corner) vs. edited image. The numbers correspond to the mean density through the thickness of the beam at different positions. 97 PART II- ASSESSMENT OF REFERENCE PROPERTIES Density distribution in components The development of the equipment and methods for digital image analysis has made it possible to determine variations in apparent density values and distribution in timber and wood composites. These differences can be detected through the attenuation of X-rays passing through the material [5,10]. Determination of material properties through image calibration X-rays are already in use as a means of determining material properties and strengthening grade timber. The current methods are not suitable for in-situ assessment and are outside the scope of this article. In-situ methods for determining material properties are most probably available for materials with great homogeneity in their properties, such as steel [11]. As timber is a material with large-scale variations in all its physical and mechanical properties, these methods cannot be applied without further reflection and awareness of the scatter in the obtained results. Failure modes in metal fasteners In-situ X-ray imaging also provides an opportunity to determine the actual behaviour of dowels in joints, see Fig. 4 [3]. Obtaining the dimensions of non-visible fasteners or cross-section reductions, as well as the connection of joints that are decisive for the judgement of boundary conditions, offers an excellent opportunity for further interpretation in the structural analysis [4]. Moreover, the exact position of the plastic hinges (bent nails in Fig 4) can be easily determined. Fig. 4 The X-ray images show the behaviour of a nailed joint (left) and a bolted connection (right) [4]. 98 PART II- ASSESSMENT OF REFERENCE PROPERTIES Calibration procedure A practical methodology for assessing the density of timber in situ using X-ray measurements is proposed. First, the in-situ procedure, the preparation of the equipment and the need for a calibration wedge are described. The thickness of the member and the moisture of the X-rayed component have to be measured for calibration purposes. The calibration wedge, see Fig. 5, is placed by the component that is going to be imaged, wherever there is room (above, below or next to). In order to minimise the effects of the exit angle from the X-rays in the tube (larger dosage in the centre and less dosage at the edges), the targeted distance from the generator to the Xrayed object is between 2.5 and 3 metres [12]. In practical applications, this distance is seldom possible to achieve, so the effects on the image have to be adjudged in the evaluation process when the density variation is obtained. The parameters that may affect the measurement results include the distance to the object, the exposure time, the energy level and the irradiation geometry (such as source size and fan angle). Subsequently, the density evaluation process of the X-rayed component starts using image processing software. The first step here is to establish a density relationship from the calibration wedge by determining the mean greyscale values from the specimens with different densities. The density variation between specimens can be represented by a trend-line equation, see Fig. 5. The coefficient of determination (R2) in the equation should be 0.90 or higher and the number of specimens from the calibration wedge included on the image should be at least eight. The number of specimens included in the equation is dependent on the image disturbances and the distance to the X-rayed object. So, the number of specimens has to be evaluated from image to image. As a result, the calibration wedge should consist of 10 to 15 specimens with dimensions that can be captured on the image plate, cf. Fig. 1. 99 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 5 Example of X-rayed beam (on top): calibration wedge (below), consisting of eight clearwood specimens with varying densities, and its established trend-line equation (bottom). The mean greyscale of the inspected area (µmean) has to be determined and corrected in relation to reference values for moisture (±µMC). This mean value is then inserted in the trend-line equation, where a preliminary density value is obtained. Finally, this value is corrected in relation to reference values from the calibration wedge with a correction factor (∆RGB) for the thickness, according to Eq. (1). The ∆RGB value is tabulated in Tab. 1 and the µMC value is tabulated in Tab. 2. µmean_corr = µmean + (∆µMC) + ∆RGB Eq. (1) Image evaluation procedure Due to the cone-beam effect of the portable X-ray equipment, where the X-ray dosage is not evenly spread in the raw X-ray image, image corrections using imaging software, e.g. ImageJ®, are a great advantage in digital images and are needed in any visual application. The relevant attenuation ratio (I/I0) can be measured using imaging software, where I is the intensity of the X-ray beam after penetration of the sample and I0 is the initial intensity. The ratio can then be calculated as an average value over the energy spectrum [13]. In practical applications, this principle can be used as follows: to correct the defaults/noise level of the raw image, several small steps must be applied to evaluate the noise level and subtract it from the complementary background image without illumination. A further image with X-ray illumination accounting for the non- 100 PART II- ASSESSMENT OF REFERENCE PROPERTIES uniformity of the cone-beam effect to reach the final pixel grey value is needed. This principle of image correction due to background noise level was applied in the in-situ determination of the material density in the different projects. The principle for the image correction procedure is illustrated in Fig.6. (a) (b) (c) Fig. 6 The procedure in principle for image background correction due to the cone-beam effect according to [10] at micro-level: (a) raw image, (b) noise level due to cone-beam effect, (c) final corrected image. Calibration wedge The X-ray images of beams and joints can be calibrated in a further step towards obtaining their density by a calibration specimen comprising at least eight to 15 different wood specimens with different density characteristics, see the example in Fig. 7. The thickness (depth) of the specimens is restricted to 30 mm, which is the reference thickness for the thickness calibration. The specimens need to be conditioned at a relative humidity (RH) level of about 66%, which corresponds to about 12% (air-dried density reference level) in moisture content (MC). The conditioning process can be performed in a climate chamber with a constant temperature level of 20ºC, or, preferably, the specimens can be stored in a climate-controlled box where a saline solution (NaNO2; sodium nitrite) maintains the RH at a level of about 66% [14]. Fig. 7 Calibration wedge composed of wood specimens (in this case 13) with increasing density. Correction for thickness This section mainly provides the instructions for using the tabulated ∆RGB values, see Tab. 1. The ∆RGB values are based on the reference thickness of the calibration wedge, 101 PART II- ASSESSMENT OF REFERENCE PROPERTIES which is 30 mm. The values were taken from the study carried out at Chalmers University of Technology, and are the result of the principle of radiation energy absorption, when X-rays pass through the object [9]. First, a qualified expectation of the density range is formulated, i.e. typical softwood, for example, ranges in density between 300 and 500 kg/m3, as the ∆RGB value is a function of both the density of wood and the thickness of the object or specimen. Once the first estimated prediction of density is made, this first calculated density value can be further corrected for ∆RGB using linear interpolation between points representing 400, 550 and 800 kg/m3 respectively. However, only close to the range limits, i.e. 521 and 579 kg/m3 (second column in Tab. 1, for example), it may change very slightly. Due to many other uncertainties in the timber material, making this further correction is not thought to be necessary. The obtained value from Tab. 1 can then be inserted in Eq. (1) and the corrected mean value (µcorr) can be calculated. Tab. 1 Change in ∆RGB [RGB] on the image due to the influence of the thickness of the specimen – tabulated and graphical. 102 PART II- ASSESSMENT OF REFERENCE PROPERTIES Correction for moisture In this case, the appropriate factor for the measured MC should be inserted in Eq. (1). The µMC value between two moisture ranges has to be interpolated from Tab. 2. This procedure is optional, at least for the range between 8% and 16% MC, as the MC only has a small influence on the attenuation of X-rays. The influence of moisture that was captured in this study could reveal a larger scatter between different images. The µMC values are based on the reference MC for air-dried density conditions (12%) and decrease or increase linearly by approximately 1.25-1.75 [RGB] for every 1% change in MC. Tab. 2 Linear change in ∆µMC [RGB] on the image due to the influence of different moisture conditions in timber. ~MC [%] 6% 8% 10 % 12% 14 % 16% 20% 22% ~RHequ [%] 35% 43% 50% 66% 79% 85% 90% 93% ∆µMC [RGB] 7.5- 10.5 2.5-3.5 0 .0 2.5-3.5 5.0-7.0 5.0-7.0 103 10.0-14.0 12.5-17.5 PART II- ASSESSMENT OF REFERENCE PROPERTIES Limitations of the procedure The calibration of the images is made from a subjective point of view and has to be performed for each individual image. The uneven distribution of radiation dosage is restricted by the distance between the generator and the X-rayed object, so the light that appears from the power initiation of the X-ray tube has to be considered in the evaluation process, but the shadowed areas can easily be detected and excluded from the evaluation following an image evaluation procedure. The size of the image plate restricts the overall evaluation of the structural member. Imaging plates of several sizes are available. The method cannot be directly applied to composite structures and therefore requires further investigation and improvement. Discussion and conclusions Based on the results of a study carried out by [15-16], accurate estimates of the in-situ density of timber have been obtained using the procedure described in this paper. When using this procedure, the linear correlation is valid for timber densities within a range of 250 kg/m3 to 1000 kg/m3. Furthermore, adjustment for the thickness of the evaluated specimen has a significant influence on density and cannot be ignored when the density of timber is evaluated. The influence of the moisture content can, however, be ignored, as it has only a minor impact on the attenuation of the X-rays; at least for the range between 8% and 16% MC, which is typical for the structural timber in-situ in Service Classes 1 and 2 [17]. The influence of moisture could have produced a larger scatter between different images. Uncertainty relating to the accuracy of the method when it comes to obtaining the density values in situ can be attributed to various factors, such as the individual image and the conditions governing access to the object that is going to be X-rayed. The distance also impacts the individual images as a result of the cone-beam effect, which necessitates a background correction. It should, however, be remembered that this is a direct measurement method which is used to obtain the density of an object, with a calibration wedge in the actual image. Further development of the density calibration procedure is needed to apply the procedure to composite materials or wall elements with several different layers. As a general conclusion, digital radioscopy provides real potential for the development of a successful future tool for the in-situ assessment of timber structures and it is as easy or difficult to use as any other non-destructive method. It also contributes to the detection of failures and deterioration in the material in the early stages, which may provide a better basis for making correct decisions 104 PART II- ASSESSMENT OF REFERENCE PROPERTIES when it comes to repairing or replacing the timber in question and, by doing so, increasing the service life and durability of the structure. As commonly stated for timber engineering purposes, the density governs the stiffness and to some extent also the strength properties. The procedure can therefore be used in the analysis of structural behaviour. The density of timber components is also relevant for the examination and evaluation of mechanical connections. References [1] Kasal B., Adams A. and Drdacky M. (2008): Application of Digital Radiography in evaluation of Components of Existing Structures. RILEM Symposium on On Site Assessment of Concrete, Masonry and Timber Structures - SACoMaTiS 2008. Varenna - Lake Como, Italy. [2] Dinwoodie J. (2000): Timber: Its nature and behaviour. London, Taylor & Francis. [3] Anthony R. (2003): Examination of Connections and Deterioration in Timber Structures Using Digital Radioscopy. American Society of Civil Engineers, Vol., pp. 320-328. [4] Tomazello M., et al. (2008): Application of X-ray Technique in Nondestructive Evaluation of Eucalypt Wood. Maderas. Ciencia y tecnología, Vol. 10 (2), pp. 139-149. [5] Rinn F., Schweingruber F. and Schär E. (1996): Resistograph and X-ray density charts of wood comparative evaluation of drill resistance profiles and X-ray density charts of different wood species. Holzforschung, Vol. 50 (4), pp. 303-311. [6] N.C.P.T.T. (2005): Advances in Digital Radioscopy for Use in Historic Preservation. National Center for Preservation Technology and Training, pp. 125. [7] Maini, R and Aggarwal H (2010): A Comprehensive Review of Image Enhancement Techniques. Journal of Computing, Vol. 2 (3), pp. 8-13. [8] Lear G. C. (2005): Improving the Assessment of In Situ Timber Members with the Use of Nondestructive and Semi-Destructive Testing Techniques. Master of Science Master's Thesis, Civil Engineering, North Carolina State University. [9] Brozovsky J., Brozovsky J., Jr. and Zach J. (2008): An Assessment of the Condition of Timber Structures. 9th International Conference on NDT of Art. [10] Chen S., et al. (2010): Digital X-ray analysis of density distribution characteristics of woodbased panels. Wood Science and Technology, Vol. 44 (1), pp. 85-93. [11] Bateni A., Ahmadi M. and Parvin N. (2008): Prediction of density in porous materials by x-ray techniques. 17th World Conference on Nondestructive Testing. Shanghai, China. [12] Hughes J. F. and De Albuquerque Sardinha R. M. (1975): The application of optical densitometry in the study of wood structure and properties. Journal of Microscopy, Vol. 104, pp. 91-103. [13] Badel É. and Perré P. (2002): Predicting oak wood properties using X-ray inspection: representation, homogenisation and localisation. Part I: Digital X-ray imaging and representation by finite elements. Ann. For. Sci., Vol. 59 (7), pp. 767-776. [14] Nevander L. and Elmarsson B. (1994): Fukthandbok: Praktik och teori. Stockholm, AB Svensk byggtjänst. [15] Lechner T., Sandin Y. and Kliger I. R. (2013): Assessment of Density in Timber Using Xray Equipment. International Journal of Architectural Heritage: Conservation, Analysis 105 PART II- ASSESSMENT OF REFERENCE PROPERTIES and Restoration, Vol. 7 (4), pp. 416-433. [16] Lechner T. (2013): In-situ assessment of timber structures - Assessment methods and case studies. Doctoral Thesis, Civil and Environmental Engineering, Chalmers University of Technology, pp. 62. [17] EN 1995 (2004). Eurocode 5: Design of Timber Structures. European Standard EN 1995 :2004, Comité Européen de Normalisation CEN. 106 PART II- ASSESSMENT OF REFERENCE PROPERTIES A methodology for the determination of the timber density through the statistical assessment of ND measurements aimed at in situ mechanical identification Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo University of Naples Federico II, Dept. Structures for Engineering and Architecture, Italy [email protected]; [email protected]; [email protected] Abstract The research context [1-5]. A wide experimental activity has been developed in the framework ofthe Italian project DPC-RELUIS 2010 – 2013, Line 1, Task 1 and it is ongoing on the current DPCRELUIS 2014, with the aim to provide a procedure for in situ mechanical identification of ancient timber members made of old chestnut wood (Castanea sativa Mill.) by means of non-destructive techniques (ND) and to define standardized guidelines to be used for practical applications [STAR Paper 1]. The following specimens with standard dimensions according to UNI EN 480 (2004) UNI ISO and 3789 and 3132 Italian codes (1985) were obtained: structural elements in actual dimensions (SA), squared elements in small dimensions (SS) and defectfree specimens (DF). The following ND techniques are employed [4]: Hygrometric tests (H), for the evaluation of the moisture content of wood, Ultrasonic (U) tests, for the determination of the elastic properties of wood, Sclerometric (S) tests, for the assessment of the quality and surface hardness, Resistographic (R) tests, for the detection of density variations and internal defects of wood. Destructive tests (DT) in compression (C) and in bending (B) were performed in order to assess stiffness and strength properties, post-elastic behaviour and collapse mechanisms of chestnut timber. By means of a statistical approach, linear regression of the following relations are examined: correlations between NDT parameters, relating the L and T measures by U, S and R tests; correlations between DT parameters, defining the mechanical behaviour in C and B; NDT-DT correlations, using both simple and multiple models for ND estimation of density, modulus of elasticity and strength of the material. 107 PART II- ASSESSMENT OF REFERENCE PROPERTIES The definition of the methodology Based on the results obtained, the most reliable correlation for achieving the mechanical properties of timber is the one defining a relationships among the density and the mechanical properties. Therefore the correct determination of density is compulsory. To this purpose, a method that allows the in situ identification of density of old chestnut timber members, through the use of ND techniques, has been developed. Starting point of the procedure consists in the individuation of the most reliable correlation between the examined parameters. The best linear regression equation found is the one between the density (ρ) and the sclerometric (PT) and resistographic (Am,T) parameters in transverse (T) direction, for the small dimensions specimens. This could be used considering that SA and SS specimens show similar behaviour in terms of strength, stiffness and collapse modes. Tab. 1. Correlation between density [ρ (kg/m3)] and sclerometric [PT (mm)] and resistographic [Am,T (%)] measures The correlation allow for the determination of a so called theoretical value of the density (ρt), it being affected by some approximation. For enhancing the accuracy of the estimation of the actual density (ρs), which is measured in laboratory, a correction coefficient Cadj, ρ is introduced, obtaining a design density value (ρd = ρt/Cadj, ρ). Such a coefficient is defined as the maximum value (for the sake of safety) of the ratio ρt/ρs evaluated for every examined specimen, it being quite always larger than 1. The assumed value is Cadj, ρ=1.15. The proposed method allows the in situ density identification (ρd) of timber element by only ND tests with an error quantified at most as 13% of the actual value ρs (in reduction). Once estimated the density, the strength and modulus of elasticity both in compression and in bending are evaluated through the correlations with density obtained for SA specimens. Indications for executions In order to comply to the above procedure, indications for the executions are provided. After the preliminary phases consisting in traditional visual inspections for evidencing any possible significant defect or degradation, lack of members, 108 PART II- ASSESSMENT OF REFERENCE PROPERTIES together with the geometrical survey, the cross sections for testing should be identified. This is a very important task because the selected cross sections should be representative of the timber consistency. The number differs if the members is subjected to compression or bending. Then instructions for the application of sclerometric and resistographic tests are given, concerning either the preparation of the testing surface, or the mapping and the number of the shots (the last differing if the member is subjected to compression or bending), the data reading and elaboration. Conclusions The proposed method allows the in situ density identification ( ρd) of timber element by only ND tests with an error quantified at more as 13% of the actual value (ρs). The methodology also allows to perform NDT in the direction transverse to the axis of the tested member. In this way, it is possible to solve the problem of the access at the end sections of members, which often involves the inconvenience of dismantling the entire structures. Further experimental activities would allow to reach more robust correlations for in situ mechanical characterization of existing timber members. Acknowledgments The research activity was developed within the Italian projects PRIN 2006 and DPC-RELUIS 2010-2013 and RELUIS 2014 (B. Faggiano responsible of research unit). Authors acknowledge Letizia Esposito and Francesco Grasso for the contribution to the set-up of the method, given within the research activity. Main authors references [1] Faggiano, B., Grippa, M.R., Marzo, A., Mazzolani, F.M.: Experimental study for nondestructive mechanical evaluation of ancient chestnut timber. Journal of Civil Structural Health Monitoring: Volume 1, Issue 3, page 103-112, 2011. [2] Faggiano, B., Grippa, M.R., Marzo, A., Mazzolani, F.M.: Experimental analysis on old chestnut timber by means of non-destructive techniques. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June 2010. [3] Faggiano, B., Grippa, M.R., Marzo, A., Mazzolani, F.M.: Structural grading of old chestnut elements by compression and bending tests. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June 2010. [4] Grippa, M.R., Faggiano, B., Marzo, A., Mazzolani, F.M.: Combined methods for in situ mechanical identification of ancient timber structures based on non-destructive tests. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June 2010. 109 PART II- ASSESSMENT OF REFERENCE PROPERTIES [5] B. Faggiano, M.R. Grippa, B. Calderoni, 2013. Non-destructive tests and bending tests on chestnut structural timber. Advanced Materials Research Vol. 778 (2013) pp 167-174© (2013) Trans TechPublications, Switzerland, doi:10.4028/www.scientific.net/ AMR.778.167 110 PART II- ASSESSMENT OF REFERENCE PROPERTIES Evaluation of the influence of defects on the mechanical properties of timber through the analysis of multiscale specimens, based on NDT and DT Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo University of Naples Federico II, Dept. Structures for Engineering and Architecture, Italy [email protected]; [email protected]; [email protected] Abstract The research context: The work illustrated is part of the extensive experimental activity, developed within the Italian projects PRIN 2006 and DPC-RELUIS 2010-2013 and 2014 (B. Faggiano responsible of research unit) [1, 2, 3, STAR 1]. According to a defined investigation procedure, non-destructive (ND: hygrometric, sclerometric and resistographic) and destructive tests (D: compression and bending) on samples made of old chestnut wood were performed with the aim of obtaining reasonable ND-D correlations based on statistical elaborations for the prediction of wood density, stiffness and strength of the tested material. The paper focus The experimental activity was developed on multiscale specimens, such as structural timber and defect free clear elements, with the aim to evaluate the influence of natural defect patterns of material on both non-destructive parameters by sclerometric and resistographic tests and mechanical properties by compression and bending tests of timber. Multiscale specimens and tests methods The experimental campaign was developed on timber elements made of old chestnut wood (Castanea sativa Mill.), provided from roofing trusses of a masonry building of Naples, built up at the beginning of the 19th century. The 111 PART II- ASSESSMENT OF REFERENCE PROPERTIES investigations were carried out on both structural elements in actual and small dimensions (types SA and SS respectively) and defect-free (types DF) specimens with standard sizes, according to UNI EN 480 (2004) and UNI ISO 3789 and 3132 Italian codes (1985). Before the experimental tests, the conservation state of the selected samples was detected by checking wood defects and damage, such as longitudinal cracks due to shrinkage ring shakes, large isolated knots or knots groups. Ultrasonic (U), sclerometric (S) and resistographic (R) ND methods were used for SA and SS specimens, whereas compression (C) and bending (B) tests were performed on both S and DF elements. Fig. 1 summarises the multiscale specimens and tests types [3]. Fig. 1. Multiscale specimens tested in the experimental campaign. Experimental evidences The results of compression tests parallel to grain show that the presence of extended natural defects on SA reduces of about three times the compression strength of the base clear material, being the stiffness properties nearly similar each other (Fig. 2a). Furthermore, the bending strength of DF samples is about twice than the same one of SA and SS elements. It is also apparent that the bending modulus of elasticity in clear wood is slightly larger than in structural timber (Fig. 2b) [1, 2, 3]. Concerning the influence of macroscopic defects on NDT parameters, it is observed that the presence of superficial layers of wood with low consistence increases of about 18% the penetration depth values by sclerometric test in transversal direction. Moreover, extended knots and internal more resistant parts produce an increment of the resistographic amplitude of about 40%. 112 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 2. Average curves: a) Stress ( σc,0)-strain (εc,0) for C test; b) Strength (fm)-middle rotation (ϕ) for B tests. Acknowledgments The research activity was developed within the Italian projects PRIN 2006 and DPC-RELUIS 2010-2013 and 2014.. References [1] Faggiano B., Grippa M.R., Marzo A., Mazzolani F.M., 2011. “Experimental study for nondestructive mechanical evaluation of ancient chestnut timber”. Journal of Civil Structural Health Monitoring: Volume 1, Issue 3, page 103-112. [2] Faggiano B., Grippa M.R., Marzo A., Mazzolani F.M., 2010. “Structural grading of old chestnut elements by compression and bending tests”. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June. [3] Faggiano B., Grippa M.R., Calderoni B., 2013, “Non-destructive tests and bending tests on chestnut structural timber”. 2nd International Conference on Structural Health Assessment of Timber Structures (SHATIS’13), Trento, Italy 4-6 September. 113 PART II- ASSESSMENT OF REFERENCE PROPERTIES 114 PART II- ASSESSMENT OF REFERENCE PROPERTIES Screw withdrawal resistances for reliabilitybased evaluation of timber in existing structures Nobuyoshi Yamaguchi Dpt. of Building Materials and Components, Building Research Institute, Tsukuba, Japan Abstract Screw withdrawal measurement is a semi-destructive testing method, which are used in detailed inspections of existing timber structures. Screw withdrawal measurements had used wood-screws for probes; the method using metric-screw type probes with short-threads has been developed. The new screw withdrawal measurements are able to estimate physical/mechanical properties of timber such as their densities and shear strengths. Distribution of properties along the timber depths is also obtained from coaxial multiple withdrawal resistance measurements. Estimated properties from these screw withdrawals are applied for the evaluation of degradation of timber structures. Benchmark method, nominal value method and structural calculation method are proposed for the evaluation. The benchmark method and nominal value method use integrity indexes of components and joints of timber structures. Properties estimated from these screw withdrawals are also used in structural calculations of existing timber structures. These indexes and results of structural calculations are applied for the evaluation of existing timber structures. Physical/mechanical properties estimated from these screw withdrawals are able to apply for reliability-based evaluation of existing timber structures. Introduction Scales of Inspection Objects Timber structures use many structural timbers and other materials. The components have joints connecting them to the others. Integrity of structures is dominated by the integrity of their components and joints. Most of joints use fasteners such Structure Component & Joint Material Fig. 1 Scale of Inspection Objects 115 PART II- ASSESSMENT OF REFERENCE PROPERTIES as pins, nails, bolts and metal plates, etc. Interface of these timbers and metal hardware tend to accumulate water or humidity between them, these wet/humid interfaces between them accelerate degradation of timber and fasteners. The performance of these components and joints are dominated by the integrity of their materials. Fig.1 illustrates scale of inspection objects from structures to their materials. Integrity of structures is dominated by the integrity of their materials consequently. Homogeneous and Inhomogeneous Degradation of Components Homogeneous degradation of timber causes global degradation of components by weathering, aging and fungus, etc. Inhomogeneous degradation of timber causes partial degradation of components by fungus, insects, etc. Dense degradation of timber caused defects on the surface and inside of the components, and make effective cross-sectional areas of them reduced consequently. Strengths of the components are reduced by both of decrement of the cross-sectional areas and degraded stress capacity(strength) of the residual cross-sectional area of them. Global Inspection for Screening A flowchart of inspection and evaluation from phase 1 to 5 is proposed in Fig.2. In Phase 1, document and drawings on object structures, information on climate and environment and fungus/insects information around the structure are required to be accumulated as possible. Those are generally provided from owners and users of the object structures. Probable degradation areas of timber structures might be known by the people in surrounding communities empirically. Document and drawings of the structures are the bases of global inspection in Phase 2. Timber structures are composed of thousands of components; detailed inspections for all of components are not cost effective. Positions of detailed inspection are to be minimized. Screening of structures which identify the detailed inspection areas is effective to minimize the number of detailed inspections. Basic nondestructive testing methods as visual, sounding, knife test, small core sampling and others are applied for the structures. These basic inspections provide clues of probable degradation areas of the structures. Modern nondestructive testing are available such as X-ray, bore-scopes, etc [1,2]. These tests provide visual information of timbers behind finishing. Contact type nondestructive testing is able to provide visual information of components such as GPR, ultra-sound reflection tools, etc. Some semi-destructive testing is also used such as needle penetration, pin pushing, etc. Combined usage of information from owners, empirical knowledge in communities, non/ semi-destructive testing will realize cost effective inspections. Global inspection will result tentative map of detailed inspection positions of the structures. Information obtained from Phase 1 and Phase 2 would be the bases for cost effective inspections. 116 PART II- ASSESSMENT OF REFERENCE PROPERTIES Start Phase 1 Phase 2 Documents Information from Owner, Users Drawings Environment ,Climate Global Inspection Screening Non-destructive Non-contact testing (Remote) Contact testing Semi-destructive Fungus, Insects, etc. In situ Visual X-ray Knife test M.C AE Bore scope Needle Penetration Drilling resistance etc. Sounding Stress Wave GPR etc. Pin pushing, etc. etc. Tentative mapping of position of detailed inspection Phase 3 Detailed Inspection Non-destructive Contact testing Semi-destructive Dent Holes In situ Knife test M.C AE Bore scope Sounding Stress Wave GPR etc. In situ Hardness test Pin pushing, etc. Needle Penetration Drilling resistance Compression Laboratory Screw Withdrawals, etc Cores Compression Core sampling, etc. Micro-specimens Shear test of Glue lines Compression, etc. Tension Positions of additional detailed inspection Phase 4 a) Benchmark method b) Nominal value method Comparison with benchmark timber Comparison with nominal values of timber Integrity Index c) Structural calculation Residual properties of components and joints Structural calculation (Global or Partial) Analysis of serviceability Estimation of risk of failure Phase 5 Global or partial mapping of integrity index, lack of serviceability and risk of failure on structures Judgment of use, usage restrictions, repairs, reinforcement, demolish (Global and Partial) Fig. 2 Inspection and Evaluation of Timber in Existing Timber Structure 117 PART II- ASSESSMENT OF REFERENCE PROPERTIES Detailed Inspections In phase 3, detailed inspections are applied for the components and joints of structures. Physical/mechanical properties of components and joints are obtained from non/semi-destructive testing in situ and laboratories [1,3]. Non-destructive testing such as stress wave, acoustic emission (AE) tools will be available to obtain physical/mechanical properties. Semi-destructive testing such as pin pushing, needle penetration and drilling resistances will assist to estimate properties of timber. New semi-destructive testing measuring force-deformation relationship along the depths of timber is also proposed [4]. Results of detailed inspections may require additional inspection positions other than the tentative inspection positions derived from the global inspection. Physical/mechanical properties obtained from detailed inspections will be used in Phase 4. Screw withdrawal measurements for detailed inspections Screw withdrawal measurement is one of semi-destructive testing methods. Screw withdrawals were examined from 1980’s for inspection method of timber [5,6]. Screw withdrawal measurements are one of methods which leave scars in timber as other testing methods of needle penetration, pin pushing, drilling resistance and small core sampling, etc. Screw withdrawal measurements had used wood-screws, lag-screws and nails as probes. New screw withdrawal measurements method using metric-screw type probes with short-threads have been proposed [7]. Screw withdrawals are able to provide specific densities and shear strengths of timber. Screw withdrawals also provide distribution of them along the depths in timber [7]. Judgement After the detailed inspection in Phase 3, three evaluation methods of benchmark method, nominal value method and structural calculation method are prepared in Phase 4. Physical/mechanical properties obtained from detailed inspections are compared to the reference values in benchmark method and nominal value method. The benchmark method and nominal value method use relative comparison between residual properties and initial/original properties of timber. Estimated residual mechanical properties are also used in structural calculations. Benchmark method Benchmark timber is need in benchmark method. Benchmark timber is the reference selected from the same species as the object timber. The benchmark timber is required to have average properties of the object timber species. The same testing method should be applied for the measurement of properties of the object timber and the benchmark timber. Integrity index IBS of benchmark method is given from Equation (1). Index IB is ratio of measured properties of the object timber and the benchmark timber, which is defined in Equation (2). Pr and PB are measured properties of the object timber and the benchmark timber. Index IS correspond to 118 PART II- ASSESSMENT OF REFERENCE PROPERTIES the decrement of cross-sectional areas by inhomogeneous degradation is defined in Equation (3), where Ar is residual cross-sectional areas of the object timbers, and Ao is original/initial cross-sectional areas of them. Integrity of the object timber is evaluated by the integrity index IBS. In case of screw withdrawal resistance measurements, index properties are withdrawal resistances both of the object timber and the benchmark timber for the same directions to the grain. Benchmark method is available for non/semi-destructive testing methods, especially for the case that nominal values of physical/mechanical properties are not listed in wood handbooks, etc. I BS = I B × I S (1) Pr PB A IS = r Ao IB = (2) (3) Nominal value method In case benchmark timber is difficult to prepare, nominal value method will be alternative of benchmark method. Reference for the comparison is nominal properties of the object timber species. These nominal properties are generally the average or the lower limit (5 percentile) values listed in wood handbooks, etc [8,9]. Integrity index INS of nominal value method is given from Equation (4). Index IN is ratio of the properties estimated from the object timber and nominal properties of them, which is defined in Equation (5). Pr is estimated properties of the object timber. P N is nominal properties of the object timber species. Nominal value method requires less measurement works than those by benchmark method, however, need nominal properties of the object timber species. In case of screw withdrawal measurements, densities or shear strengths parallel to the grain are used for the index properties, because both of nominal values are listed in wood handbooks. Although shear strengths perpendicular to the grain is obtained from measured withdrawal resistances, the shear strengths parallel to the grain is not directly obtained from withdrawal resistances. Estimation of shear strength parallel to the grain is required in screw withdrawal measurements. I NS = I N × I S P IN = r PN (4) (5) Structural calculation method The other method is structural calculation. Structural calculations are applied for 119 PART II- ASSESSMENT OF REFERENCE PROPERTIES object structures or part of them. Structures are required to resist actual and design loads in principle. One of the methods to evaluate integrity level of existing structures is to calculate structural safety of existing structures with their residual properties against their actual and design loads. Structural calculations result stress level of components, safety level of joints, deformation of components and displacement of structures. These deformation and displacement are used for serviceability analysis of the structures. Stress level of the components and joists are used for risk analysis of failure of the structures. Structural calculations need principal mechanical property of components and joints of the object structure. Screw withdrawal measurements provide only densities and shear strengths of timber. MOR and MOE of timber are estimated from screw withdrawal resistances with velocities of stress waves. Compression of timber is also correlated with screw withdrawal resistances. Expedient inspection methods should be used for mechanical property estimation of structural components and joints. In order to estimate required mechanical properties, screw withdrawal measurements would be used with other inspection methods. Mapping and judgement Detailed inspections provide physical/mechanical properties of timber. These properties are used for integrity indexes of benchmark and nominal value methods. Integrity indexes, serviceability rank and risk of failure of the structures are mapped on the drawings and included in the inspection reports. Judgment for the future of the object structure is made such as use, usage restrictions, repairs, reinforcements and demolish of all or part of the structure. Value of the structures and cost of repairs and reinforcements of them are also considered for the judgements. Methodology Probes Screw withdrawal measurements had used nails, wood-screws and lagscrews. Wood-screw based probes with short-threads were developed, and probes manufactured from threaded rod with metric-screws were developed[7,10]. Shape of wood-screws is not standardized internationally; however, shape of metric-screws is standardized by ISO 261 and 724. Metricscrew probes are longer and have smaller diameters of their threads than typical wood-screws; the probes are suitable for measuring withdrawal resistances in deep of timber. The short-threads clarify measuring positions in deep timber, and reduce withdrawal resistances. Coaxial multiple withdrawal resistance measurements (CMWR) using long metric-screw type probe provide distributions of withdrawals along pre-drilled holes. The metric-screw probes have outer cylindrical shear planes around the threads. In case of timber, these shear planes have shear strengths correspond to shear directions. Fig.3 and Fig.4 show the 120 PART II- ASSESSMENT OF REFERENCE PROPERTIES probes for the screw withdrawal measurements which have short-threads and are manufactured from threaded rods of ISO standard metric-screws. Diameter, pitch and length of the probe thread in Fig.3 was 3.87mm, 0.7mm and 12.85mm respectively. The probe has double heads of conical heads on top for withdrawing and hexagonal heads below for screwing. Depth Indicator 15 5 Thread Length 15 20 Thread Diameter Fig 3. Short-thread of the Metric Probe for Screwing and Withdrawing Fig.4 Metric-screw Probe with Heads Equipment Tools for withdrawing and measuring Two cramp types of withdrawing tools are shown. Photo1 shows typical withdrawal tools developed by Prof. F.Divos [11]. Photo 2 shows withdrawal tool developed for the coaxial multiple withdrawal resistant (CMWR) measurements [12]. Load-cells are installed in these tools. Peak loads are indicated on the indicators connected to the load cells. Rate of withdrawing should be constant as possible. Electric screwdrivers are able to apply constant rate of withdrawing better than that by hands. Photo 1 Typical Withdrawal Tool Photo 2 Withdrawal Tool for CMWR 121 PART II- ASSESSMENT OF REFERENCE PROPERTIES Procedures Pre-drilled holes Wood-screws do not need pre-drilled holes, but lag-screws and metric-screw type probes need pre-drilled holes to screw them into timber. Pre-drilled holes are applied by drilling tools. These pre-drilled holes are required to be orthogonal to the surfaces of timber generally. Diameter of the pre-drilled holes used with the probes shown in Fig.3 was 3mm. Single Withdrawal Resistances The probes are screwed into the pre-drilled holes by hands or electric screwdrivers, etc. Single withdrawal resistance (SWR) measurements are used for typical withdrawal measurements. The probes are screwed into timber as Photo 3. The probes are able to be screwed into timbers through finishing such as gypsum boards and plaster, etc. Fig.5 shows withdrawal resistance measurements of timber behind the finishing. Multiple measurements of SWR are required to obtain reliable SWR values. Photo 3 Single withdrawals Fig. 5 Measurement of Timber behind Finishing Coaxial Multiple Withdrawal Resistances SWR is a method to measure withdrawal resistance at one depth position. In order to obtain distribution of withdrawal resistances along depth direction of timber, coaxial multiple withdrawal resistance (CMWR) measurements were developed [7,10,12]. Fig.6 illustrates procedures of CMWR using the same pre-drilled hole. The probe in Fig.6 equips attachment adjusting depths of the probe thread in timber. Typical procedures of CMWR are as follows. The probe is screwed into timber 20mm deep into the wood. The probe is pulled out and withdrawalresistances are measured simultaneously by the withdrawal tools. Then the probe is removed from the hole to get rid of sawdust from the hole. The probe is then screwed in 15mm deeper than before. The probe is also pulled out and withdrawal-resistance is measured simultaneously. The probe is removed from the hole to get rid of sawdust from the hole. These procedures are repeated. Tip positions of the probes in timber will be 20, 35, 50mm depths in this case. Multiple measurements of CMWR are required to obtain reliable CMWR values. 122 PART II- ASSESSMENT OF REFERENCE PROPERTIES 1. Pre-drill 2. Screw Probe into Pre-drilled Hole 3. Pull out Probe & Measure 4. Screw Probe deeper than Before 5. Pull out Probe & Measure again Fig. 6 Procedure of CMWR Measurement Normalized Withdrawal Resistance (NWR) Measured withdrawal resistances are affected by the area of outer cylindrical shear plane around the probe threads. Removing the effect of dimensions of the probe threads, measured withdrawal resistances were normalized by the outer cylindrical area of the thread. These normalized withdrawal resistance (NWR) is obtained by Equation (6)[12]. NWR indicates estimated shear strength of wood on the outer cylindrical shear plane shown in Fig.7. When the probe is screwed into the timbers from their longitudinal surfaces, direction of the estimated shear strength (NWR) will be RT-direction (radius or tangential direction = perpendicular to the grain) of timber. (6) τ P Rt Lt π : Estimated shear strength (NWR) : Withdrawal resistance : Diameter of the thread (peak to peak) : Length of the thread of probes : Circular Constant 123 [N/mm2] [N] mm] [mm] PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig.7 Cylindrical Shear Plane around Probe Thread Application Density Withdrawal strengths of wood-screws are correlated with densities of timber, withdrawal resistances of wood-screws are calculated using equations with density terms [8]. Fig.8 and Fig.9 are examples of relationship between measured densities and withdrawal strengths. Fig.8 shows relationship between timber densities and withdrawal strengths of typical wood-screws [13]. Fig.9 shows relationship between densities and NWR of metric-screw probes [14]. The tests in Fig.9 used three coniferous species. NWR(–RT) in Fig.9 means NWR for radius(R) or tangential(T) directions of timber, those are for perpendicular to the grain directions. Both figures show clear correlations between densities and withdrawals. A regression equation between densities and withdrawal strengths is proposed in Fig.9. A regression equation in Fig.9 is obtained using three coniferous species totally. Withdrawal forces include the effect of thread dimensions; however, NWR exclude effects of thread dimensions. Fig. 8 Densities-Withdrawals Relationships by Wood-screws [13] 124 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig.9 Densities-NWR Relationships by Metric-screws[14] Shear strength Perpendicular to grain NWR is shear strengths on outer cylindrical planes around the threads of probes. Withdrawal measurements are applied for perpendicular to grain in general; NWRs obtained from these withdrawal measurements are for perpendicular to grain direction. Measured NWRs by withdrawal measurements are shear strength perpendicular to the grain, but it is difficult to measure shear strengths perpendicular to the grain by typical shear strength tests using chair type block specimens. Parallel to grain Typical shear strengths of timber are those parallel to the grain. Nominal shear strengths listed in typical wood handbooks are those for parallel to the grain direction [8,9]. Nominal shear strengths are obtained from shear strength tests based on testing standards(ASTM D143, JIS Z2101). Shear testing standards uses chair type specimens which have flat shear planes, use offset distance between two loading shear planes parallel to the grain. NWR is shear strengths on cylindrical shear plan e s, have no offset, for perpendicular to the grain. Fig.10 shows relationship between densities of timber and measured shear strengths(L) Sh L parallel to the grain [14]. A regression equation between strengths(L) ShL and densities is proposed in Fig.10. A regression equation in Fig.10 is obtained using three coniferous species totally. The specimens used for the tests of Fig.9 and Fig. 10 were end-matched. Shear strengths(L) ShL are able to be calculated from NWRs of withdrawal resistances using these two regression 125 PART II- ASSESSMENT OF REFERENCE PROPERTIES equations shown in Fig.9 and Fig.10. Regression equations in Fig.9 and Fig.10 are examples respectively. Fig. 10 Densities-Shear Strength( L) ShL Relationship [14] CMWR Depth (mm) Fig.11 shows comparison of averaged NWRs distributed in depth direction measured by SWR and CMWR measurements. The depth direction was perpendicular to the grain. CMWR used a 105x105x105mm specimen of Douglas-fir with nine predrilled holes and six depth positions for CMWR measuring respectively. SWR used twenty seven 30x30x30mm specimens with a pre-drilled hole and a depth position respectively. These specimens for CMWR and SWR were cut off from the same timber. Those were also end-matched and depth-matched. NWR distribution 100 90 80 70 60 50 40 30 20 10 0 CMWR (105mm) SWR (30mm) 0 10 NWR (N/mm2) 20 Fig.11 Distribution of NWRs by CMWR and SWR Measurements 126 PART II- ASSESSMENT OF REFERENCE PROPERTIES by CMWR measurements was just about close to that by SWR measurements; distributions of NWRs for depth direction are measured by CMWR measurements [12]. Compression Relationship between compression and screw withdrawal/pull-out force was studied [15]. Fig.12 shows one of these results. The withdrawal/pull-out force values are correlated with compression strengths of timber. Fig.12 Compression-Pull out Force Relationship[15] M OR Relationship between MOR and screw withdrawal resistances is known from 1990’s. F.Divos et al. proposed Equation (7) and Equation (8) which predict MOR of coniferous and hardwood species respectively. Screw withdrawal forces and velocities of stress wave are used in these equations. The applied units in these equations are: MOR[MPa], F[kN], ν[km/s]. Screw withdrawal forces F were measured using wood-screws. Diameter and length of their threads was 4mm and 18mm. 2.7mm diameter pre-drilled hole was made in timber to accommodate screw. The results are shown in Fig.13. In sound wood, longitudinal transmission velocities generally fall within the range of 3.5 - 5 km/s. Screw withdrawal forces using wood-screws for transverse direction of timber generally fall with the range of 1 – 3.5 kN. These withdrawal forces are considered to be equivalent to 4.5 – 15.5 N/mm2 of NWR. The correlation coefficient between measured and predicted MORs by Equation (7) and Equation (8) was 0.74 [1,11,16]. 2 MOR = 0.809 F × ν + 26.8 2 MOR = 1.258 F × ν + 36.9 (7) (8) 127 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig.13 Measured and Predicted MOR Relationship [11] M OE Relationship between static MOE and screw withdrawals of timber were examined. Static MOE were correlated with dynamic MOE. Static MOE(E) was predicted by Equation (9) with regression coefficients a and b, density and stress wave speed v. The densities were estimated from measured screw withdrawals with their regression coefficients. Predicted MOE (E) was correlated wiht the actual static MOE [3, 13]. E = a + bρν 2 (9) Reliability-based Evaluation In case that the structural performance and design loads are probabilistic, structural safety is evaluated stochastically. Reliability-based integrity analysis of existing timber structures will be realized by structural calculations using residual mechanical properties of timber obtained from detailed inspections such as screw withdrawals and others. Further Application/Calibration of Output from Nondestructive Testing Non-destructive testing method is expected to provide physical/mechanical properties of materials, but information obtained from non-destructive testing is limited. For example, applying screw withdrawal tests in conjunction with nondestructive testing for the same location of the same timber, relationship between non-destructive testing output and screw withdrawal resistances are obtained. Output from non-destructive testing could be calibrated by the physical/mechanical properties estimated from 128 PART II- ASSESSMENT OF REFERENCE PROPERTIES screw withdrawals. Calibrated output provided from non-destructive testing is more informative and useful than those without calibrations. Limitations Screw withdrawal is one of cost effective inspection methods. But the followings are limitations of screw withdrawals. Screw withdrawals leave holes on timber. Repair of the holes may be required. Knots are often hidden in object timber. Screw withdrawals provide very large withdrawal resistances when the probe is in and around knots hidden in object timber. These withdrawals should be eliminated preventing the false estimation of timber properties. Screw withdrawal measurements are time consuming. CMWR measurements are more time consuming than SWR. In order to obtain reliable results from screw withdrawal measurements, multiple measurements of screw withdrawals are required. Screw withdrawal measurements need skills for pre-drilling and withdrawing. Lengths of drills for the pre-drilling and metric-screw probes are limited. References [1] Bohumil Kasal, Thomas Tannert, In Situ Assessment of Structural Timber, Springer, RILEM State of the Art Reports, Volume 7, 2010 [2] Mariapaola Riggio, Ronald W.Anthony, Francesco Augelli, Bohumil Kasal, Thomas Lechner, Wayne Muller, Thomas Tannert, In situ Assessment of Structural Timber using Nondestructive Techniques, Materials and Structures, DOI 10.1617/s11527-013-0093-6, 2014 [3] Thomas Tannert, Ronald W.Anthony, Bohumil Kasal, Michal Kloiber, Mau-rizio Piazza, Mariapaola Riggio, Frank Rinn, Robert Widmann, Nobuyoshi Ya-maguchi, In situ Assessment of Structural Timber using Semi-destructive Techniques, Materials and Structures, DOI 10.1617/s11527-013-0094-5, 2014 [4] Kloiber, M., Drdácký, M., Tippner, J., Sebera, V.: New construction NDT device for in situ evaluation of wood by using compression stress-deformation measurements parallel to grain. In: 18th International Nondestructive Testing and Evaluation of Wood Symposium, 2013, September 24-27, Madison, Wisconsin, USA. FPL-GTR-226: pp. 585-592. [5] Talbot, J.W. unpublished research, Pullman, WA: Washington State University, 1982 [6] Robert J. Ross, Roy F. Pellerin, Nondestructive Testing for Assessing Wood Members in Structures, General Technical Report FPL-GTR-70, Forest Products Laboratory, US Department of Agriculture (1994) 129 PART II- ASSESSMENT OF REFERENCE PROPERTIES [7] Nobuyoshi Yamaguchi, Shiro Nakajima, Hirofumi Sakuma, Inspection Method of Wood Integrity Using Distribution of Resistances to Axial Withdrawals of Wood-Screw Probes, Proceedings of 15th international symposium on nondestructive testing and evaluation of wood, Duluth (2007), pp.233-241 [8] Wood Handbook, 2010 Edition, Forest Products Society, Madison, WI, USA (2011) [9] Wood Industry Handbook, ISBN 4-621-07411-3 C3550, Forest and Forest Products Research Institute, Maruzen, Japan (2004) in Japanese [10] Nobuyoshi Yamaguchi, Withdrawal resistances by screw-based probes for in-situ assessment of wood, Proceedings of international conference on structural health assessment of timber structures (SHATIS’11), Lisbon (2011) [11] Ferenc Divos, Laszlo Nemeth, Laszlo Bejo, Evaluation of the Wooden Structure of a Baroque Place in Papa, Hungary, Proceedings of 11th international symposium on non-destructive testing and evaluation of wood, Washington State University, USA (1998) , pp.153-160 [12] Nobuyoshi Yamaguchi, “In situ Assessment Method of Wood using Normal-ized Withdrawal Resistances of Metric-screw Type Probes”, Advanced Materials Research Vol.778 (2013), pp.217-224 [13] Cai, Z., Hunt, M.O. R.J. Ross, and L.A. Soltis, Screw Withdraw-al - A Means to Evaluate Densities of In-situ Wood Members, Proceedings of the 13th International Symposium on Non-destructive Testing of Wood, Forest Products Society, Madison, USA, pp.277-281, 2002 [14] Nobuyoshi Yamaguchi, Inspection Method of Integrity of Wood Components in Existing Timber Construction (Part 4) In situ Evaluation using Screw Probe Withdrawals, (in Japanese), Summaries of Technical Papers of Annual Meeting, Structure III, Architectural Institute of Japan, 2014, in Japanese, Print Pending [15] Gilfillan, J.R., Christie, D. and S.G. Gilbert, The Residual Strength of Timber Degraded by Woodworm Infestation, Proceedings of Durability of Building Materials and Components 8(Volume One), NRC Research Press, Ottawa, Canada, pp.714-722, 1999 [16] Ferenc Divos, Evaluation of Single Members in Historical Structures, RILEM meeting, Prague, May 30. 2005 130 PART II- ASSESSMENT OF REFERENCE PROPERTIES COMBINED METHOD FOR THE IN SITU MECHANICAL IDENTIFICATION OF ANCIENT TIMBER BASED ON NDTS Beatrice Faggiano, Maria Rosaria Grippa, Anna Marzo University of Naples Federico II, Dept. Structures for Engineering and Architecture, Italy [email protected]; [email protected]; [email protected] Abstract The research context. A wide research activity based on experimental tests and statistical analysis, is ongoing at the Department of Structures for Engineering and Architecture of the University of Naples Federico II, by the research team leaded by B. Faggiano, composed by M.R. Grippa, A. Marzo, L.Esposito. The research aims at providing a methodology for in situ mechanical identification of ancient timber members by non-destructive techniques [1, 2]. In particular the main goals are: database collection through laboratory NDT and DT investigations; mechanical characterization of old chestnut defect-free and structural elements through compression and bending tests; elaboration of experimental results for evaluating the influence of typical defect patterns on timber performances; identification of reliable NDT-DT correlations to be used in situ for the estimation of wood density, strength and stiffness properties; definition of standardized guidelines for practical applications. The starting point is the research carried out within the national project PRIN2006 “Consolidation of timber structures” (Prof.M. Piazza coordinator, B. Faggiano responsible of research unit) and the international project PROHITECH “Earthquake Protection of Historical Buildings by Reversible Mixed Technology” (2004-2008, prof. F.M. Mazzolani coordinator). The activity is actually developed in the framework of the Italian projects DPC-RELUIS 2010 – 2013 and 2014 (B. Faggiano responsible of research unit). The study is articulated in three main phases correlated each other, such as experimental investigations, data processing, structural identification by combined NDT-DT relationships. Supplying of the test material The experimental campaign is developed on timber elements made of old chestnut wood (Castanea sativa Mill.), provided from roofing trusses of masonry buildings 131 PART II- ASSESSMENT OF REFERENCE PROPERTIES in Naples, dated beginning of 19th century. Tests are performed on both structuralelements and defect free specimens with standard dimensions, according to UNI EN 480 (2004) and UNI ISO 3789 and 3132 Italian codes (1985), in order to evaluate the influence of defect patterns on both non-destructive quantities and mechanical properties measured through destructive tests [3, 4, 5]. Specimens have the following features (Fig. 1): Fig. 1. Specimens tested in the experimental activity. Structural elements in actual dimensions (SA): from trusses king posts, 14 elements (SA-C) for compression tests parallel to grain, D 14.5-16 cm mean equivalent diameter, 6D length; from the trusses struts, 10 elements (SA-B) for bending tests, D 15-16.5 cm mean diameter, 19D length; Squared elements in small dimensions (SS): from 11 S A-C specimens, after destructive tests: 20 samples 5x5x30 cm for ND and D tests in compression parallel to grain (SS-C); 16 elements 5x5x15 cm for ND tests (SS-NDT); from 6 SA-B specimens, after destructive tests: 24 elements (undamaged parts, 4 from each specimen) 4x4x76 cm for ND and D tests in bending (SS-B); Defect-free specimens (DF): from S A-C samples, 2x2x4 cm: 33 specimens for longitudinal tests (DF-CL); 22+22 specimens for both radial (DF-CR) and tangential (DF-CT) tests; from SA-B samples, 2x2x40 cm: 35 specimens for bending tests (DF-B). Table 1 specifies for each group of specimens the ND and D tests performed. Tab 1. Non-Destructive (H: hygrometric; U: ultrasonic; S: sclerometric; R: resistographic) and Destructive (C: compression; B: bending) Tests. 132 PART II- ASSESSMENT OF REFERENCE PROPERTIES Visual inspection Preliminary, the conservation state of the selected elements is examined by checking timber features and defects, signs of damage and deterioration. In particular, on the lateral faces of SA-C specimens macroscopic longitudinal cracks due to shrinkage are detected; whereas, ring shakes, large isolated knots or knots groups are surveyed on the SA-B specimens. Therefore, as a result of the visual structural grading, according to UNI 11119 (2004) standard, all specimens are assigned to the third class. Non-destructive tests (NDT). The following ND techniques are employed [3]: Hygrometric tests, for the evaluation of the moisture content of wood; Ultrasonic (U) tests, for the determination of the elastic properties of wood; Sclerometric (S) tests, for the assessment of the quality and surface hardness; Resistographic (R) tests, for the detection of density variations and internal defects of wood. For each specimen, the average values of NDT measures, such as ultrasonic stress wave speed (SWS), sclerometric penetration depth (PD), resistographic mean amplitude (Am), are calculated. Since in situ surveys allow only perpendicular to grain measures on the accessible external surfaces of timber members, laboratory tests are performed in both longitudinal (L) and transversal (T) directions as respect to grain orientation for evaluating the relations between L and T ND variables. Destructive tests (DT) Compression (C) and bending (B) tests were carried out for determining the mechanical behaviour of timber elements in terms of stiffness, load bearing capacity and collapse mechanisms [4]. Statistical analysis of laboratory data The experimental results are critically examined and compared, with aim to obtain statistical ND and D parameters, such as average values, standard deviations and coefficients of variation. 133 PART II- ASSESSMENT OF REFERENCE PROPERTIES Determination of NDT-DT correlations By means of a linear regression approach the following relations are examined [1, 7]: Correlations between NDT parameters, relating the L and T measures by U, S and R tests; Correlations between DT parameters, defining the mechanical behaviour in C and B; NDT-DT correlations, using both simple and multiple models for ND estimation of density, modulus of elasticity and strength of the material. In order to identify the best combination of NDT parameters for the prediction of wood density, simple and multiple linear regression analyses have been carried out. The goodness of regression fit, such as the fitting of the linear model to a given body of data, is formally assessed by the coefficient of determination (R2). Note that 0 ≤ R2 ≤ 1, high values indicate a strong linear relationship between the variables involved in the model. As an example simple and multiple correlations are presented in Fig. 2. Fig. 2. Correlations: a) Density vs compression strength; b) Density vs sclerometric+resistographic parameters Combined method for timber mechanical characterization Based on the results achieved, the method consists in the determination of the density of timber through the combination of in situ sclerometric and resistographic parameters in transverse direction. Once estimated the density, the strength and modulus of elasticity both in compression and in bending are evaluated through the correlation with density. Indication for executions are also provided. 134 PART II- ASSESSMENT OF REFERENCE PROPERTIES Further development The extension of the database would allow to reach more and more robust correlations for in situ mechanical characterization of existing timber members. Acknowledgments The research activity is developed within the projects PRIN 2006, PROHITECH 2004-2009, DPC-RELUIS 2010-2013 and 2014. References [1] Faggiano B., Grippa M.R., Marzo A., Mazzolani F.M., 2009. “Experimental evaluation of the mechanical properties of wood by means of non-destructive compared techniques for the characterization of existing wooden structures”. In Consolidation of timber structures, ed. M. Piazza, Hevelius Publisher, pp. 25-78, Italy, 2009 (in Italian). [2] Faggiano B., Grippa M.R., Marzo A., Mazzolani F.M., 2011. “Experimental study for nondestructive mechanical evaluation of ancient chestnut timber”. Journal of Civil Structural Health Monitoring: Volume 1, Issue 3, page 103-112. [3] Faggiano B., Grippa M.R., Marzo A., Mazzolani F.M., 2010. “Experimental analysis on old chestnut timber by means of non-destructive techniques”. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June. [4] Grippa M.R., Faggiano B., Marzo A., Mazzolani F.M., 2010. “Combined methods for in situ mechanical identification of ancient timber structures based on non-destructibe tests”. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June. [5] B. Faggiano, M.R. Grippa, A. Marzo, F.M. Mazzolani, 2010. Structural grading of old chestnut elements by compression and bending tests. 11th World Conference on Timber Engineering (WCTE2010), Riva del Garda, Italy, 20-24 June 2010. [6] B. Faggiano, M.R. Grippa, 2012. Mechanical characterization of old chestnut clear wood by non-destructive and destructive tests. In: World Conference on Timber Engineering. vol. III, p.359-364, Auckland (New Zealand), 16-19 July 2012. [7] B. Faggiano, M.R. Grippa, B. Calderoni, 2013. Non-destructive tests and bending tests on chestnut structural timber. Advanced Materials Research Vol. 778 (2013) pp 167-174© (2013) Trans Tech Publications, Switzerland, doi:10.4028/www.scientific.net/ AMR.778.167 135 PART II- ASSESSMENT OF REFERENCE PROPERTIES 136 PART II- ASSESSMENT OF REFERENCE PROPERTIES Combine information from visual and NDT/SDT methods Artur Feio1, José Saporiti Machado2 1) 2) Department of Architecture, University Lusíada, Portugal, [email protected] Department of Structures, LNEC, Portugal, [email protected] Abstract Visual strength grading (VSG) standards are generally the most common nondestructive method used for assessing the mechanical properties of timber member in situ. The limitations of the full application of visual grading rules to timber members in situ lead to the necessity to provide a set of simplified rules for this task. However given the subjectivity and the limitations related to the application of visual grading the results can be supported/validated by complementary information provided by non and semi-destructive testing (NDT/SDT) methods. The present paper discusses how VSG information can be optimized facing a particular timber member and how its information can be combined with other type of NDT/SDT information. Background Structural evaluation of ancient or recent timber structures presents particular problems (related to inherent wood material properties) and difficulties. In situ evaluation (without damaging) of timber structural elements represents an initial and crucial step for the success of the rehabilitation process. Support for nondestructive inspection works includes nowadays a variety of tools offering valuable information about the quality and biodeterioration status of timber elements. Appraisal and repair of ancient timber structures has become a major topic of interest in the last decades. This renewed interest considerably increased the number of technical interventions and design developments. Conservation or rehabilitation of existing timber structures imply extensive knowledge about the properties of materials from which the structure is made. This knowledge constitutes the support for short-term structural behaviour assessment as well as to foresee the continuous adaptation and capacity of response of the material under long-term actions. 137 PART II- ASSESSMENT OF REFERENCE PROPERTIES Due to the high variations intra and inter species, a large volume of wooden material is needed to be tested to characterize its mechanical properties with a minimum level of confidence [1]. Quality control and preservation of artistic value were considered important issues leading to the development of some nondestructive and semi-destructive test methods (NDT/SDT) for wood, which sometimes were used in the evaluation of the mechanical and physical properties of other materials [2]. Combined with a visual grading survey, these evaluation methods are an excellent complement to achieve a good level of reliability in the structural analysis, diagnosis and inspection of existing constructions. Visual Strength Grading The evaluation of a timber structure begins by conducting a preliminary survey that includes an appraisal of the general quality of the timber members. This evaluation consist in examining directly, and preferably at close distance, checking and registering wood features, signs of damage or deterioration, sometimes with the help of simple instruments (knife, chisel, hammer, etc.), providing a rapid means of identifying areas that may need further investigation. This is an essential part of diagnosis but the results depend severely on the experience of the person carrying out the task. Since modern design standards require quantitative more than qualitative parameters, visual inspections, as the basis of any visual strength grading (VSG) appraisal, are crucial in the inference of mechanical properties. Visual grading is done mainly based on national standards trying to optimize the grading results for the timber resources of the country, taking into account growth conditions, local preferences for certain cross sections, silviculture differences, and historical developments concerning structural applications [3]. All the VSG standards are based on indirect visual methods focus in understand the effect of important macroscopic strength-reduction reducing characteristics, such as knots and slope of grain, upon the basic quality of a timber member, defined by the properties of its clear wood zones. Therefore mechanical properties of wood elements are highly dependent on the inherent wood properties of each species as well as on the presence and type of defects [4]. Appraisal in situ includes the identification of the wood species, selection of a proper VSG standard and consequent allocation of suitable reference mechanical properties in terms of allowable stresses, characteristic values or strength class. VSG was the first non-destructive testing method to be applied for the sorting of sawn timber according with their mechanical characteristics. The simplicity of its application, not requiring any special equipment, made this method also the one first adopted for the in situ assessment of structural timber members. However in this preliminary survey other NST/SDT methods are already used as support to VSG results (e.g. moisture meters). 138 PART II- ASSESSMENT OF REFERENCE PROPERTIES Such properties are then used for a first structural analysis. If results showed that structural failed complied with the ultimate state requirements then a more detailed evaluation – detail survey – of the timber members should be carried out or the structure demolished [5]. The focus of this second evaluation is on critical members of the structure (more stressed or involved in failure has shown by the first structural analysis results). Recent publications address the way VSG should be adapted to on site conditions [5, 6, 7, 8]. These publications try to optimize the grading process (optimal visual grade) by considering the most important defects present in a timber member and the type of stress applied. The use of NDT/SDT methods to ensure a more reliable prediction of timber member’s properties is vaguely mentioned. For instance, [7] establishes criteria for the diagnosis of old timber elements and strength grading can be performed using both on site inspections and NDT techniques. Prepared in the scope of COST Action IE0601, [5] proposed a first harmonized method for determining the structural grade based on visual grading appraisal supported in the current European procedures and standards. Although NDT for strength prediction is presented as an option in some cases, the level of reliability was thought to provide always an over conservative prediction (safe side). This document is also the reference document for the WG 10 of the CEN/TC 346/WG 10 activity (Conservation of cultural heritage - Historic Timber Structures) aiming the final preparation of a harmonised visual strength grading methodology that could be approved by CEN. However, there are several restrictions to the full application of visual grading standards to timber members in situ. VSG standards were developed having in mind the grading of sawn timber at sawmill yards. The full application on site of the rules applied at the sawmill yard is not possible or logical and leads to gross underestimation of the real mechanical performance of timber members. Considering the biased and subjectivity of the grading process, dependent upon human judgment, and variability associated to each visual grade, it is expected that a large proportion of the pieces real resistance would be largely underestimated [9, 10]. However the estimation of the serviceability properties of timber constructions, by means of the VSG standards, is not entirely reliable due to the many factors: • timber is a highly anisotropic material – heterogenetic material; • specific to a particular wood species and provenance, the possibility of extrapolation to other wood species and origins is not certain – correlation inaccuracy; • susceptible to human error, given the limitation of its full application in situ – measurement error. VSG principles can be differentiated between those following the concept of characteristic values [11, 12] and those following the concept of allowable working stress [7, 13, 15]. Since VSG is a group classification based on a heuristic approach with limited 139 PART II- ASSESSMENT OF REFERENCE PROPERTIES support from models (e.g. statistical), limited options remains for a possible upgrade of a timber member. In fact, in the absence of the data used for defining the grades of a certain VSG standard, the only option is to shift a timber member from one grade to another (lower or upper), not being possible to derive intermediate grades. For making these changes significant, the data used for the derivation of the visual strength grades or at least a probabilistic model adjustable to the timber species under analyse, needs to be available [16]. When no grading standard is available to a certain species, it is selected one appropriate to a species showing similar wood anatomy and wood density. For example, while [12] establishes different grading criteria for different timber groups, [7] applies the same grading criteria to all species. In-situ diagnosis of ancient timber structures has been described by several au thors [5, 17, 18, 19, 20]. All the authors state that an initial visual inspection of the entire structure and of the singular elements is required in order to determine the original timber characteristics and the changes suffered due to service conditions. This survey follow several steps, beginning with the purpose of a general prediction of mechanical properties and ending in a thorough examination using NDT/SDT. But an important characteristic of several ancient timber structures is that they can effectively bear higher loads than expected [21], which stresses the need of adequate procedures for diagnostic and assessment of the real bearing capacity, which cannot be obtained with a simple visual inspection. Combine visual and NDT/SDT methods Recent guidelines propose the upgrading of preliminary VSG application by conditioning it upon the stress condition and position of defects in relation to applied stress. As referred, and based on this, recent standards and studies establish that strength grading can and should be performed using both on site inspections and NDT techniques [1, 5, 22, 23]. Thus, NDT/SDT can be used to increase the precision of the prediction of the mechanical properties provided by visual grading. Generally these methods are used as validation of visual information and not combined in the sense of a fusion process between the data obtained from visual observation and other type of information (NDT/SDT methods). Usual applications of these methods are related with the prediction of: • the element residual section by analyzing abnormal density variations in the element, generally associated with mass loss; • density; • important mechanical properties (bending, shear, tension and compression 140 PART II- ASSESSMENT OF REFERENCE PROPERTIES strength, local and global stiffness) by measuring one or more indicative parameters that can be correlated with it. There are several NDT/SDT that can be applied to wood and wood composites namely: thermography [24, 25], sonic stress waves [26], X-Ray [27, 28], isotope method [29, 30], hardness tests [31], drilling resistance [20, 32, 33], moisture content meter and core drilling [34, 35, 36]. Among these, core drilling, the moisture content meter and drilling resistance currently play key roles in the preliminary survey. The large majority of research and in-situ application relies on the use of NDT/SDT results to support or confirm visual grading measurements. Drilling resistance is the most often used method to get information about the presence of hidden features and their extent (e.g. knots, decay and fissures). Other NDT/SDT methods (e.g. dynamic modulus of elasticity or penetration resistance) are used as independent variables in regression models. The upgrading of VSG information (reference properties) using other types of information (NDT/SDT methods) is limited to a few studies. The development of these methods is in fast progress; however, owing to safety concerns, high costs involved, technical issues, etc., their use has been quite limited in structural timber evaluation. One of the main constrains continues to be the lack of generalized procedures or standards concerning the application of NDT/SDT methods, although recent publication attempt to harmonize the way these methods are used [37, 38, 39]. Although some publication shows the advantages of combining (joining) information from VSG with those from NDT/SDT methods [40] very few present methods that can be used for a true combination of information [41, 42]. Conclusions VSG will remains as the basic method for assessing the mechanical performance of timber members in situ. However several studies agrees on the fact that the sole use of these method can lead to the demolishing of safe structures and that other NDT/SDT methods should be used to ensure a proper assessment procedure. The question about how to combine this information is still under study but will probably depend upon many variables (e.g. type of structure, load stresses involved, type of evaluation) making that the expert will have to make the final decision upon which method to use and how to use all the methods and data for taking a final decision. 141 PART II- ASSESSMENT OF REFERENCE PROPERTIES References [1] Feio A O, Lourenço P, J S. (2007) Non-Destructive Evaluation of the Mechanical Behavior of Chestnut Wood in Tension and Compression Parallel to Grain. International Journal of Architectural Heritage 1:272 – 292. [2] Riggio M, Tomasi R, Piazza M (2014) Refurbishment of a traditional timber floor with a reversible technique: the importance of the investigation campaign for the design and the control of the intervention. International Journal of Architectural Heritage 8:74-93. 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Italian Organization for Standardization (UNI). [8] UNI 11035-1 (2003) Structural timber — Visual strength grading: terminology and measurement of features. Italian Organization for Standardization (UNI). [9] Bonamini G (1995) Inspection and evaluation. D3/1-9. Timber Engineering STEP 2 – Design and structural systems. Centrum Hout. The Netherlands. [10] Yeomans D (1999) The problems of assessing historic timber strengths using modern building codes. The use of and Needs for Preservation Standards in Architectural Conservation, ASTM STP 1355, L. B. Sickels-Taves Ed. American Society for Testing and Materials. [11] EN 1912 (2012) Structural Timber – Strength Classes – Assignment of Visual Grades and Species. CEN European Committee for Standardization, Brussels. [12] UNI 11035-2 (2003) Visual strength grading rules and characteristic values for Italian Structural Timber Population. Italian Organization for Standardization (UNI). [13] ASTM D245 (2012) American Society for Testing and Materials, Annual Book of Standards, Standard Practice for Establishing Structural Grades and Related Allowable Properties for Visually Graded Lumber. ASTM, West Conshohocken, PA. [14] ASTM D1990 (2012) American Society for Testing and Materials, Annual Book of Standards, Standard Practice for Establishing Allowable Properties for Visually-Graded Dimension Lumber from In-grade Lumber. ASTM, West Conshohocken, PA. [15] BS 4978 (2007) British Standards Institution. Specification for the Visual Strength Grading of Softwoods. BSI, London. [16] Faber M H, Köhler J, Sorensen J D (2004) Probabilistic Modeling of Graded Timber Material Properties. Journal of Structural Safety 26:295-309. [17] Uzielli L (1992) Valutazione della capacità portante degli elementi strutturali lignei. L’Edilizia 12:753-762. 142 PART II- ASSESSMENT OF REFERENCE PROPERTIES [18] Ross R, Brashaw B, Pellerin R (1998) Non-destructive evaluation of wood. 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In Proceedings STREMAH VIII, Series: Advances in Architecture, Vol. 15: pp. 835-842. 143 PART II- ASSESSMENT OF REFERENCE PROPERTIES [35] Kasal B (2005) Estimate of the Design Values of the In-Situ Wood Structural Members Based on Semi-Destructive Experiments. In Proceedings of the International Conference The Conservation of Historic Wooden Structures, Florence, Vol. I: pp. 304-306. [36] Romagnoli M, Nocetti M, Sarlatto M (2005) Datazione Dendrocronologica di Strutture Lignee nei Tetti in Italia Centro-Meridionale. Limiti e Prospettive. Proceedings of the International Conference The Conservation of Historic Wooden Structures, Florence, Vol. I: pp. 19-23. [37] Riggio M, Anthony R W, Augelli F, Kasal B, Lechner T, Muller W, Tannert T (2014) In situ assessment of structural timber using non-destructive techniques. Materials and Structures, 47:749-766. 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Available from www.civil.uminho.pt/masonry 144 PART II- ASSESSMENT OF REFERENCE PROPERTIES Assessment of timber floors by means of nondestructive testing methods Tiago Ilharco1, Thomas Lechner2 & Tomasz Nowak 3 1 NCREP- Consultancy on Rehabilitation of Built Hertage, Ltd., Science and Technology Park of University of Porto (UPTEC), Praça Coronel Pacheco no. 2, 4050-453 Porto, Portugal. 2 NCC Construction Sverige AB, Division of NCC Technology & Sustainable Development, SE-405 14 Gothenburg, Sweden; Chalmers University of Technology, Dept. of Civil and Environmental Engineering, SE-412 96 Gothenburg, Sweden 3 Faculty of Civil Engineering, Wroclaw University of Technology, Wybrzeze Wyspianskiego 27, Wroclaw 50-370, Poland Abstract In the process of rehabilitation of built heritage, the preservation of timber floors is an essential issue. These structures have characteristics that are not entirely known, namely the connections between elements, the load distribution between beams, the importance of secondary elements, such as struts and floorboard, for the attenuation of vibrations and reduction of deformations of the floor, etc. If properly analysed and considered, these aspects can contribute to upcoming well-succeeded interventions, improving the global behaviour of the floors and, consequently, of the buildings. One of the focuses of the present paper is the assessment of the global behaviour of timber floors by means of dynamic analysis, which is one of the Non Destructive Tests (NDT) used to evaluate the reference properties of the wood. In particular, this technique allows estimating the timber floors’ stiffness and, consequently, assessing their efficiency and integrity. Furthermore, the paper focuses on the use of other NDT, namely involving stress-wave timing, X-ray and resistance drilling, which can provide very useful information about these characteristics. The information obtained with the combined NDT allows a better understanding of the timber floors behaviour and the implementatio of more efficient rehabilitation and (or) strengthening techniques. Assessment and assessment strategy of timber floors Historical structures represent a part of the cultural heritage of every nation and societies pay considerable attention to their preservation and maintenance. The insitu assessment of timber elements and their properties is essential in the continuous maintenance and preservation of historical timber structures. Much of the damage observed in historical timber structures can be attributed to 145 PART II- ASSESSMENT OF REFERENCE PROPERTIES biodegradation. The deterioration of structural members results in changes in geometry and load-bearing capacity. The replacement of members that have deteriorated may not be an acceptable option for structures of historical significance and redesign may be necessary to sustain the functionality of the structure. The structural strength assessment of timber structures, which uses various procedures and evaluation tools, is based on a multidisciplinary approach aimed at providing information about the mechanical properties and actual condition of timber members and the mechanical behaviour of joints. Abnormal structural behaviour can be suspected when the strength and stiffness of a structure is diminished due to deterioration, creep and the natural ageing of old timber [1, 2] which implies changes in load-bearing capacity. Strategies for the analysis of structures of significant cultural value must therefore be established. A structural investigation procedure should be based on adapting a general assessment methodology [3-6] to evaluate the structural condition and the mechanical performance of the floor structures in an efficient manner. The methodology comprises the following steps: 1) Diagnosis of the structure from previous repair work and action during service life 2) Preliminary assessment and visual inspection 3) Detailed assessment and investigation including material testing with nondestructive and quasi-non-destructive testing methods at critical sections 4) Evaluation of the results of the material tests 5) Structural analysis and evaluation of results This methodology shall include global and local NDT, namely with seismographs, resistance drilling machines, pilodyn, stress-wave timing, X-rays, etc. The thorough interpretation of the tests’ results and the estimation of timber floors’ properties can only be achieved with an analysis of the state of conservation, along with a constructive/structural characterization. The characterization of the wood species and of its density is also an important step to build a preliminary model of the mechanical behaviour of the floor. Global assessment through dynamic response The discussion about the global assessment of timber floors through dynamic response will be systematized in four main topics: 1) the dynamic behaviour of timber floors; 2) the techniques and instruments used to assess this behaviour; 3) the prediction of the wood reference properties; 4) the identification of the damaged areas based on the dynamic analysis. These topics will be analysed through an overview of this subject and making use of results from several NDT performed in timber floors of old buildings in Portugal included in structural survey campaigns. 146 PART II- ASSESSMENT OF REFERENCE PROPERTIES The dynamic behaviour of timber floors In residential buildings, the design of timber floors taking into account the vibration limit state has in consideration the excitation caused by the movement of people, which produces vibration frequencies of about 2Hz and 3,5Hz for walking and running steps, respectively. The dynamic response of a floor is determined by several factors, such as its mass, stiffness, damping and geometrical and structural characteristics, namely the existence of struts, the thickness of the floorboard, the type of connection between beams and walls, etc. In most cases, the floor stiffness ensures a satisfactory dynamic behaviour. However, the traditional deflection criterion does not always guarantee satisfactory vibration behaviour [7]. The issue of vibration induced by people walking on timber floors is more complex than the static behaviour due to the resonance phenomena. Resonance occurs when the frequency of the impacts that forces the vibration coincides with the natural frequency of the floor, resulting in an increase in the magnitude of vibration, leading to an eventual structural failure [8]. In an occupied building, with high permanent loads, the increased mass may decrease the floor natural frequencies to "dangerous" levels, since timber floors themselves have low mass (50-100kg/m2). Therefore, it is fundamental that the timber floors’ design respect the vibration limit states to fulfil comfort and safety requirements. [9] concluded that two criteria for lightweight floors with fundamental frequencies above 8 Hz should be considered: one related to the deformation due to a concentrated load and other to the speed of the vertical vibration. These criteria were adopted in [10] in the design of timber floors to the vibration limit state, stating that the vibration levels should be estimated by tests or calculations, taking into account the parameters that determine floors’ dynamic behaviour, namely mass, stiffness and damping coefficient. The knowledge of all these characteristics allows the assessment of the natural vibration frequencies and vibration modes associated to each frequency, i.e. of the response of timber floors when subjected to known dynamic actions. Description of the method and instruments Dynamic tests Dynamic tests using ambient vibration are one of the most effective nondestructive in situ testing techniques to identify the mechanical characteristics of structures. The existence of highly sensitive sensors allows testing without imposing a forced excitement on the structure and considering only environmental dynamic actions, such as wind, traffic, movement of persons etc. [11]. Still, some authors consider that, in the case of timber floors, the forced vibration allows a stronger response and may provide more consistent results [12]. 147 PART II- ASSESSMENT OF REFERENCE PROPERTIES Instruments used and precautions to have during data acquisition For measurements of the ambient vibration of timber floors, seismographs that include tri-axial accelerometers (GeoSIG GSR-18bit), with an acquisition frequency of 250Hz, can be used, resulting in temporal registries of the accelerations to which the structure is subjected, Fig. 1. The seismographs allow the transference of the information to a computer to be analysed. Nowadays, there are simple electronic devices, such as smart phones, which are equipped with accelerometers and provide reliable results, Fig. 2. Fig. 1. Frequency measurement on a single timber beam. Fig. 2. Calibration of smart phones accelerometers with seismographs. The registration of the dynamic response of a structure is a fundamental phase of the tests. If the acquisition is carried out with errors, it will be very difficult to correct them during the post-processing phase. It is, therefore, essential to perform a careful planning of the tests, defining the equipment to use, its location and the duration of the test. The positioning of the devices should be chosen so as to avoid areas of zero modal displacements and the data acquisition, in particular using ambient vibration, should be made by recording the dynamic response of the structure over a pre-defined time interval. Some other specific precautions should be considered during the tests, such as not disturbing the floor with the introduction of additional masses, such as those given by the test operators, and taking into account the presence of superimposed dead loads and its position. Data processing and results achievement After processing the collected data, the dynamic identification is done through the determination of the natural frequencies and the corresponding modes of vibration, which can consist on vertical, horizontal or coupled modes, depending on the main direction of vibration. One of the used methods is the Advanced Method of Frequency Domain Decomposition [13], currently implemented in the software ARTeMIS [14]. The fundamental frequencies of vibration of the floors are identified using the peaks observed in the records in the frequency domain (obtained via Fast Fourier Transforms, FFT). Fig. 3 show an example of the data obtained in the frequency 148 PART II- ASSESSMENT OF REFERENCE PROPERTIES domain, identifying the direction of higher vibrations associated. The value of the 1st frequency is 9.1Hz (z) and the 2nd is 10.0Hz (y). Fig. 3. Identification of the main frequencies of a timber floor (y and z). Prediction of reference properties The influence of the constructive elements of the floors Timber floors are simple structures with a complex behaviour that depends on the performance of the whole system: the beams, the struts and the floorboard. In fact, the load distribution factor conferred by struts and floorboard, designated ksys in [10], which accounts their stiffening effect, is essential to the estimation of the MOE when using the natural frequencies obtained in the dynamic tests. [15] determined that, in a common timber floor, the load distribution factor is 1,15, close to the one defined by [10] (1,1). Some in situ tests performed by [16] indicated that this factor can be even higher. The connections between different structural elements have also a strong influence in the vibrational behaviour of the floor. Analysis of the results and prediction of the modulus of elasticity (MOE) The dynamic tests performed with accelerometers positioned in different locations of a timber floor allow estimating some of the reference properties of the floor, namely the MOE. This approach can include simple calculations or more complex numerical models, which reproduce the in situ tests through numerical modal analysis. In this case, the numerical results are fitted to the results obtained experimentally by adjusting the mechanical properties through an iterative process. One must note that it’s a very complex task to properly simulate the timber floors, namely due to their geometrical irregularities, types of connections between structural elements, etc. All these characteristics should be carefully integrated in the numerical structural analysis and, therefore, the calibration process should also be based on the data resulting from the visual inspection (geometrical, structural and conservation assessment) and other in situ tests. If the estimation of MOE is developed through more simple calculations, rather than with numerical models, the need for understanding thoroughly the geometrical/ structural characteristics of the timber floors is the same. For a simply supported beam, the fundamental frequency f1 can be calculated using Eq. (1). Although the equation is defined for simply supported beams, [10] suggests its use for timber 149 PART II- ASSESSMENT OF REFERENCE PROPERTIES floors simply supported on the four sides. In this case, “(EI)long” is the stiffness of the plate equivalent to the floor in the direction of the beams; “m” is the value of the mass per unit area and “L” is the span of the floor. f1 = π (EI )long 2 L2 m (1) E= 4 × f1 × L4 × m Ilong × π 2 2 (2) [8] states that the frequencies obtained in situ are typically up to 50% higher than the frequencies estimated using Eq. (1), thus suggesting its multiplication by a factor up to 1,5. This is due to the mentioned stiffness conferred, particularly, by the nailed floorboard and to the support conditions of the beams in the walls, which, in fact, don’t correspond to simple supports. “(EI)long” must account the increase of stiffness of the timber floor due to these conditions and should be obtained multiplying the stiffness of a simply supported beam (EI) by a stiffness factor (Sf) that, according to the frequency results obtained by [8], can go up to 2,25. The MOE of the floor can be estimated following Eq. (2). Some experimental campaigns in a set of chestnut beams [16], including dynamic and bending tests [17] indicated a good approximation between the results of MOE obtained in both tests when multiplying the Eq. (2) by a value between 1,2 and 1,5 (equivalent to increase the stiffness of a simply supported beam with a factor (Sf) of 1,5 to 2,25). This methodology is very useful to estimate the behaviour of timber floors in their present conditions and, in particular, in their future use, regarding, for instance, an increase of the live loads. The results can indicate the need to strengthen the timber floor in order to increase its stiffness and improve its dynamic behaviour. Identification of damaged areas Dynamic tests have the advantage, compared to other NDT methods, of allowing a global assessment of floors by measuring the frequencies and modes of vibration. However, they don’t allow the separate analysis of the structural elements and may even lead to the occultation of some local damages. Therefore, the use of other NDT methods, such as X-ray, resistance drilling, stress-wave timing, etc. is fundamental to analyse thoroughly the state of conservation of timber floors. Still, since the dynamic response of the floor depends on the type of structural elements and connections, as well as on their level of degradation, these tests allow evaluating the global condition of a floor, helping in the detection of damaged areas. The dynamic identification of other structural elements of a building, particularly walls, may also help to assess the behaviour of timber floors. In the particular case of a building in the city centre of Lisbon, whose in situ tests were conducted in collaboration with the National Laboratory of Civil Engineering (LNEC), the observation of two opposite facades responding in phase for lower modes indicated that the timber floors were effectively linking both walls [18]. This result, together with the observations made during the survey, confirmed the good condition of the 150 PART II- ASSESSMENT OF REFERENCE PROPERTIES timber floors. On the other hand, in a specific area of the main facade, an anomalous behaviour was detected, with the identification of modes associated with a “free” vibration of this area. This result indicated that the connection between the timber floor and that area of the wall was deficient, probably due to the degradation of some timber beams, situation confirmed afterwards with a detailed survey. Local assessment As previously stated, the use of NDT, such as X-ray, resistance drilling, stress-wave timing, is fundamental in the local assessment to analyse thoroughly the state of conservation of timber floors and thereby the structural health of timber floor structures and their performance regarding the strength and stiffness values. Once the critical sections are identified from a preliminary investigation, the corresponding actions on the floor structure can be quantified and therefore serve as a valuable input in the global analysis of the structure to achieve an as accurate response as possible. Appropriate properties, such as density (ρ), the modulus of elasticity (MOE) and the cross-sectional properties, relating to the quality and health of single members need therefore to be determined using NDT. The sequence of use for different assessment devices to detect and localise internal deterioration and damage, for example, is of great importance in an effective assessment procedure. It is therefore preferable initially to identify members requiring further investigation using global measurements, before applying methods such as resistance drilling and X-ray that require more effort and time. The discussion about the local assessment of timber floors treats the techniques and instruments used to assess the structural soundness and performance. This also implies the prediction of local and semi-global material properties as well as the identification of damage and deterioration of structural timber members. Those aspects are integrated in the single method. These steps are presented in an overview and results from NDT investigations performed from a timber floor investigation of a historical structure in Sweden are roughly included in this survey. NDT techniques for local assessment purposes Among a number of different NDT tools to investigate timber structures, stress wave timing, X-ray measurements and Resistance drilling were studied to efficiently assess material properties and locally assess the performance of timber floor structures Stress-wave timing The transmission time is highly correlated with the modulus of elasticity (MOE), Eq. (3), which is of great importance for evaluation of the structural soundness of 151 PART II- ASSESSMENT OF REFERENCE PROPERTIES beams, purlins and columns in large timber structures [19]. Several commercial instruments, such as FAKOPP®, are available to measure and assess transmissiontime in materials. MOEdynamic = ρ " v 2 (3) where ρ is the density and v the transmission time of the stress wave. Stress wave measurements are a simple and efficient measurement technique to identify the internal soundness and condition of structural elements, but also to determine stiffness parameters for structural analysis. This technique requires an appropriate measurement strategy and approach to efficiently determine the structural performance of in-situ elements and to successfully detect internal damage, but also the extent of both external and internal damage. Such a stress-wave-based condition assessment strategy is simply illustrated in Fig. 4, where critical areas from the visual inspection were measured stepwise in different directions to identify decay and its extent on the structural element at different locations along the beam. Fig. 4. (Right) Illustration of a stepwise (1-5) stress-wave-based assessment approach along a structural beam and (left) measurements in different directions to detect the extent of the damage/deterioration (A-B, C-D and E-F), adopted from [20]. Decayed and degraded wood show clear increases in stress wave transmission times, which also leads to a significant loss of strength [20]. An increase of the velocity sound by about 30% results in a loss of strength by about 50% [21, 22]. The longitudinal propagation of the stress waves vary from 4000 m/s to 5500 m/s depending on the wood species. Transverse propagation of the stress waves are about 25% of the value in the longitudinal direction and is mainly used as a qualitative parameter to assess the condition of structural elements and is the most efficient way to detect decay and its extent [23]. An appropriate measurement strategy to efficiently determine the structural performance as aforementioned is illustrated in Fig. 4. Comprehensive longitudinal measurements on single element properties and the structural soundness were explored on a historical floor structure in Sweden [24]. 152 PART II- ASSESSMENT OF REFERENCE PROPERTIES The average velocity from the measurements throughout both of the timber floors was 4969 m/s (std. dev. 335 m/s), which is in the range of sound and good performing timber. The principle to detect eventual deterioration as illustrated in Fig. 4 was performed on a historical floor structure in Sweden [24] in the upper and the lower floor, where the measurements for the upper floor showed rather constant velocities for all measurements with a slight decrease near the column, so no signs of degradation/ deterioration were captured. In comparison to the upper floor, the lower floor, implied some signs of degradation/deterioration within the support region, where the velocity (3916 m/s) was about 20% lower than the velocity measured for sound members. On-site X-ray investigations The application of digital imaging processing and increasing resolution has made it possible to use quantitative assessments of components, such as the internal deformation of fasteners, the dimensions of hidden elements and strains [25]. Until recently, the opportunities for X-ray investigation have been used for the qualitative assessment of timber structures, but the opportunities to carry out quantitative evaluation are of great importance to evaluate the on-site structural behaviour. The portability of available X-ray devices was a great step forward which especially facilitates the in-situ operation of e.g. timber structures. Portable units have shown to be promising, both with regard to quality and feasibility [26]. The ability to penetrate wood with lower-level energy X-rays and to record images with adequate quality, was evaluated in 1996 and further evaluations identified technical and logistical issues [27]. It is a well-known fact that timber density correlates well with other significant parameters such as MOE and bending strength (modulus of rupture, MOR), which makes it possible to provide indirect information about these properties by X-ray imaging, since real-time radiography (radioscopy) allows the study of component behaviour under moderate loads and is particularly suitable for timber structures due to the density differences. In order to obtain correct density data the X-ray equipment must be calibrated and an example of this is presented and thoroughly described by [26]. Mapping damage and deterioration of timber and mechanical connections is another powerful application for implementation of X-ray equipment on-site. As most of the portable X-ray equipment delivers images in a two-dimensional perspective, additional help using resistance drilling, for example, may be needed for the volumetric mapping of deterioration as a result of insect attacks. In many cases, a two-dimensional image is sufficient for determining the severity and progress of the invisible damage [28, 29], as decay due to rot and high moisture content can be seen and determined by measuring the area of the void. In general, the qualitative radiographs from the investigation of a historical timber floor in Sweden [24] showed that the grain structure of the members was intact at 153 PART II- ASSESSMENT OF REFERENCE PROPERTIES critical sections. Radiographs of connections showed that the connection details were generally in good condition at the inspected locations except at one location where signs of deterioration close to the support structure was found, see Fig. 5, as verified by using resistance drilling. The effect of local interior deterioration in structural elements needs to be taken into account in the general assessment and should be remedied. Fig. 5. A qualitative radiograph (A) & (B) of a beam in a floor structure indicates hidden deterioration (in the centre), as drilling resistance results verified. Resistance drilling Resistance drilling can be used to detect and quantify the internal condition and decomposition of the wood in timber structural elements. Although the drilling resistance causes tiny holes, it can be considered as a negligible influence on the structure, but should be preferably planned properly in the assessment in order to minimize the surgical intervention. The use of that small diameter needle-like drill (1.5-3.0 mm at the tip) was introduced by Rinn [30]. Nowadays, there are some different commercial instruments available, e.g. IML RESIF400-S® (Fig. 13). The rate at which the wood is penetrated is constant. The torque needed to maintain a constant penetration rate corresponds to the drilling resistance and is graphically recorded versus drilling depth. Zones of lower drilling resistance can be identified as the ones with lower density. As a consequence those zones usually have lower strength and elasticity. Moreover, lower drilling resistance may indicate decayed zone, cavities, cracks and crevices. Peaks in the graph correspond to high resistance and high density. They also indicate the presence of knots in the cross section. Declines and low points correspond to low resistance and low density, including decayed zones, cavities or cracks (Fig. 6). Totally decayed wood shows no drilling resistance. The drilling resistance is proportional to the relative variations in density, i.e. that decreasing drilling resistance is followed by decreased torque of the drill. A Resistance Measure (RM) parameter was implemented that allowed the comparison between the density of the drilling resistance and mechanical and physical properties of the timber. The RM parameter is though defined as the integral of the area of the drilling diagram divided by the length l of the drilled perforation [31], see Eq. (4). = (4) 154 PART II- ASSESSMENT OF REFERENCE PROPERTIES Fig. 6. (Left) IML RESIF400-S® and (right) density profile of drilling measurement. Drill shape and dimensions (mm) are shown in lower left corner. This method is used to a great extent in the quantification of deteriorated timber. Resistance drilling enables to locate defects and structural discontinuities in timber members without affecting the performance, which is particularly important in the case of heritage structures [32, 33]. An investigation of a historical timber floor structure in Sweden showed that the coefficient of variation (CoV) of the obtained RM values is high [24], which increases the uncertainty when it comes to correlating the RM values with the wood parameters. In investigations of structural timber members in different historical structures carried out by the authors, partly reported by [34], the coefficient of variation reached values up to 37%. Uncertainty about the potential for evaluating wood strength parameters using the drilling-resistance method was raised. It was found that many parameters, such as wood moisture content, drill-bit sharpness and drilling angle and direction, affect the drilling-resistance diagram [35]. The main purpose of the drilling-resistance method was therefore not the assessment of the mechanical properties of wood but simply the qualitative investigation of wood based on internal material defects. Due to its local measurement character, the parameter estimation requires several measurements. Drilling resistance measurements can also serve as an input for determining effective cross-sectional areas of timber beams that affect the second moment of area and the load-carrying capacity of structural members in general. Strength and Stiffness predictions from NDT The densities from the radiographic measurements and the MOE calculations from the stress-wave measurements as mentioned previously might serve as an input in the analyses of the material resistances of the individual structural elements. 155 PART II- ASSESSMENT OF REFERENCE PROPERTIES For this evaluation, the characteristic bending strength, , (MOR), and shear strength, , , for example can be calculated according to [36] and [37] respectively, using the following expressions: (5) [ ] = 0.002065 ∙ , , ! [ ] = 0.2 ∙ ," , (6) The static MOE (MOEstatic) is usually acquired from the dynamic MOE by a linear relationship equation according to Eq. 7 [38], but they can also be obtained directly from the density measurements, Eq. 8 according to [36]. ! = 407.2 + 0.796 ∙ ! = 25.186 ∙ G .-./. '() ! (7) (8) The quantitative evaluation of the mechanical properties and the density using stress-wave timing and radiographic measurements provided both good agreement and reasonable input for the structural analysis. It is, however, important to remember that there may be some uncertainty about the correlations for timber between the output from the measured properties and the strength parameters using assessment techniques that might weaken the estimation of the actual capacity. Conclusions The focus of the present paper is the assessment of the behaviour of timber floors with the use of global and local NDT, namely involving dynamic behaviour analysis with seismographs, stress-wave timing, X-ray and resistance drilling. The use of instruments to assess the dynamic behaviour of the floors, such as seismographs, has the advantage of allowing a comprehensive assessment of the timber floors’ global behaviour, by measuring the characteristics associated with their dynamic performance, which allow estimating MOE. It can also evaluate the global state of conservation of the floors and detect damaged areas, which are usually associated to lower natural frequencies and, consequently, to lower MOE. However, the use of seismographs does not allow the separate analysis of the structural elements that compose the floors and it may even lead to the occultation of damaged elements. For that reason, it should be used together with other NDT that can lead to the prediction of local properties, such as stress wave timing, resistance drilling and X-rays. To assess the general quality of the timber, it is sufficient to apply stress-wave measurements, in combination with resistance drilling and X-ray measurements. Reliable results can be obtained, thereby increasing the ability to minimise interventions and prolong the service life as a part of sustainable development. The extent of measurements should be adjusted to match the structural condition and existing information relating to the structure [24]. 156 PART II- ASSESSMENT OF REFERENCE PROPERTIES The combined use of these NDT allows a better understanding of the timber floors behaviour and the implementation of more efficient rehabilitation and (or) strengthening techniques. References [1] Mohager S. Studier av krypning hos trä: med särskild hänsyn till inverkan av konstanta och cyklist varierande fukttillstånd. Stockholm: KTH - Institutionen för Byggnadsmateriallära; 1987. [2] Rug W, Seemann A. Strength of old timber: Test cores from 50-400 year old timber indicates strength of old timbers corresponds to that of new. Building Research and Information. 1991;19(1):31-7. [3] ICOMOS. Recommendations for the analysis, conservation and structural restoration of architectural heritage. ICOMOS International Committee for Analysis and Restoration of Structures of Architectural Heritage; 2005. [4] Macchioni N, Piazza M. Italian standardisation activity in the field of diagnosis and restoration of ancient timber structures'. Structural Analysis of Historical Constructions, Macmillan India Ltd, New Delhi. 2006. [5] ISCARSAH. Recommendations for the analysis, conservation and structural restoration of architectural heritage. ICOMOS; 2003. [6] Cruz H, Yeomans D, Tsakanika E, Macchioni N, Jorissen A, Touza M, et al. Guidelines for the on-site assessment of historic timber structures. International Journal of Architectural Heritage. 2013(just-accepted). [7] Hu, L. J., Chui, Y. H., Onysko, D. M. (2001). Vibration serviceability of timber floors in residential construction, John Wiley & Sons, Ltd., Quebec, Canada. [8] TRADA. (1998). Vibration in timber floors, TRADA Technology Ltd, Hughenden Valley, High Wycombe, Bucks. [9] Ohlsson, S. (1988). "Ten years of floor vibration research - A review of aspects and some results." Symposium/Workshop on Serviceability of Buildings (Movements, Deformations, Vibrations), Ottawa, Canada, 435-450. [10] European Committee for Standardization CEN, EN 1995-1-1: Eurocode 5: Design of timber structures - Part 1-1: General - Common rules and rules for buildings, 2004, CEN, Belgium. [11] Caetano, E. (1992) Identificação Experimental de Parâmetros Dinâmicos em Sistemas Es-truturais. Master thesis on Civil Engineering, University of Porto. [12] Soltis, L. A., Wang, X., Ross, R. J., Hunt, M. O. (2002). "Vibration Testing of Timber Floors Systems." Forest Products Journal, 52, 75-82. [13] Brincker, R., Ventura, C. (2001) Damping Estimation by Frequency Domain. Proceedings of the 19th International Modal Analysis Conference (IMAC), Kissimee, Florida, USA. [14] SVS (2006) ARTeMIS Extractor Pro, Release 4.0, Structural Vibration Solutions, Aalborg, Denmark. [15] Blass, H. J. (1995). Load Sharing. Timber Engineering -Step 1.Lecture B16, Almere Cen-trum Hout, Holanda. [16] Ilharco, T. (2008) Pavimentos de madeira em edifícios antigos. Diagnóstico e intervenção estrutural. Master Thesis, University of Porto. [17] European Committee for Standardization 157 PART II- ASSESSMENT OF REFERENCE PROPERTIES CEN, EN 408: Timber structures – Structural timber and glued laminated timber – Determination of physical and mechanical properties, 2003, CEN, Belgium. [18] Lopes, V. et al (2010). Conference Património 2010. Porto, Portugal. [19] Wang X, Divos F, Pilon C, Brashaw BK, Ross RJ, Pellerin RF. Assessment of decay in standing timber using stress wave timing nondestructive evaluation tools. USDA Forest Service Forest Products Laboratory General Technical Report FPL-GTR-147, 12pp. 2004. [20] Dackermann U, Crews K, Kasal B, Li J, Riggio M, Rinn F, et al. In situ assessment of structural timber using stress-wave measurements. Materials and Structures. 2013:1-17. [21] Pellerin RF, Ross RJ. Nondestructive evaluation of wood: Forest Products Society; 2002. [22] Ross RJ, White RH, Pellerin RF, Wang X, Brashaw BK. Wood and timber condition assessment manual: Forest Products Society; 2004. [23] Ross RJ, Hunt MO. Stress wave timing nondestructive evaluation tools for inspecting historic structures: a guide for use and interpretation. General Technical Report Forest Products Laboratory, FPL-GTR-119, USDA Forest Service2000. [24] Lechner T, Nowak T, Kliger IR. In situ assessment of the timber floor structure of the Skansen Lejonet fortification, Sweden. Construction and Building Materials. 2014;58:85-93. [25] Kasal B., Adams A. and Drdacky M. (2008): Application of Digital Radiography in evaluation of Components of Existing Structures. RILEM Symposium on On Site Assessment of Concrete, Masonry and Timber Structures - SACoMaTiS 2008. Varenna Lake Como, Italy. [26] Lechner T, Sandin Y, Kliger R. Assessment of Density in Timber Using X-Ray Equipment. International Journal of Architectural Heritage. 2013;7(4):416-33. [27] Anthony RW. Examination of Connections and Deterioration in Timber Structures Using Digital Radioscopy. In: Bosela PA, Delatte NJ, Rens KL, editors. Third Forensic Engineering Congress. San Diego, CA: American Society of Civil Engineers; 2003. p. 320-8. [28] Rinn F., Schweingruber F. and Schär E. (1996): Resistograph and X-ray density charts of wood comparative evaluation of drill resistance profiles and X-ray density charts of different wood species. Holzforschung, Vol. 50 (4), pp. 303-311. [29] Lear G. C. (2005): Improving the Assessment of In Situ Timber Members with the Use of Nondestructive and Semi-Destructive Testing Techniques. Master of Science Master's Thesis, Civil Engineering, North Carolina State University. [30] Kasal B, Anthony RW. Advances in in-situ evaluation of timber structures. Progress in Structural Engineering and Materials. 2004;6(2):94-103. [31] Lourenço PB, Feio AO, Machado JS. Chestnut wood in compression perpendicular to the grain: Non-destructive correlations for test results in new and old wood. Construction and Building Materials. 2007;21(8):1617-27. [32] Jasieńko J, Nowak T, Hamrol K. Selected methods of diagnosis of historic timber structures principles and possibilities of assessment. Advanced Materials Research. 2013;778(2013):225-32. [33] Branco JM, Piazza M, Cruz PJS. Structural analysis of two King-post timber trusses: Nondestructive evaluation and load-carrying tests. Construction and Building Materials. 2010;24(3):371-83. [34] Jasieńko J, Nowak T, Hamrol K. Selected methods of diagnosis of historic timber structures principles and possibilities of assessment. Advanced Materials Research. 158 PART II- ASSESSMENT OF REFERENCE PROPERTIES 2013;778(2013):225-32. [35] Branco JM, Piazza M, Cruz PJS. Structural analysis of two King-post timber trusses: Nondestructive evaluation and load-carrying tests. Construction and Building Materials. 2010;24(3):371-83. [36] Dinwoodie JM. Timber: Its nature and behaviour. 2nd edition ed. London: E & FN Spon; 2000. [37] Glos P. Solid timber - Strength classes. In: Blass HJ, Aune P, Choo BS, Görlacher R, Grif-fiths DR, Hilson BO, et al., editors. Timber Engineering - STEP 1: Centrum Hout; 1995. p. 4-5. [38] Íñiguez G. Clasificación mediante técnicas no destructivas y evaluación de las propiedades mecánicas de la madera aserrada de coníferas de gran escuadría para uso estructural. Doctoral Theses Universidad Politécnica de Madrid, ETS de Ingenieros de Montes. 2007. 159 PART II- ASSESSMENT OF REFERENCE PROPERTIES 160 PART III ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 161 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 162 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS NDT imaging techniques for the inspection of timber structures Mariapaola Riggio1, Jakub Sandak2, Steffen Franke3 1 2 3 Wood Science & Engineering, Oregon State University, USA [email protected] CNR Timber and Trees Institute IVALSA, S.Michele all’Adige (TN), Italy, [email protected] Bern University of Applied Sciences, Biel/ Bienne, Switzerland, [email protected] Abstract This chapter deals with the application of NDT imaging techniques as complementary methods to be used during visual inspection. NDT imaging can be used to detect inhomogeneity and to identify the areas at the highest risk for damage in timber structures. The potential of some imaging techniques accepted and practiced for the assessment of timber structures is here discussed. 1. Introduction Visual inspection is an essential phase for the assessment of timber structures, during which vulnerability factors and visible damage can be identified. Nondestructive imaging techniques can complement visual information. According to the penetration depth of the wave field, imaging techniques make it possible to analyse either surface/subsurface features or internal heterogeneities of the wood material. Imaging methods use wave-based techniques: they analyse the response of the material to wave fields of different nature. Two different kinds of waves can be utilized: they are elastic or mechanical waves (or called stress waves) and electromagnetic waves (i.e. X-rays, gamma rays, ultraviolet rays, visible light, infrared, microwaves). Non-destructive images map a measured physical parameter, over a defined plane perpendicular to the direction of the radiation/wave transmission (e.g. radiographs, thermograms). Tomographic techniques, instead, map parameter values on a plane across the object and parallel to the direction of the radiation/wave transmission, allow cross sectional imaging. 163 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Reflectometric techniques, such as the ultrasound echo technique and the GPR, allow different kind of scans, in particular: • A-scan: a trace that show the wave transition time and the intensity of the pulse; • B-scan: a profile composing different A- scans recorded at a given distance, resulting in 2D cross sectional map on a plane parallel to the direction of the wave transmission; • C-scan: 2D cross sectional map on a plane perpendicular to the direction of the wave transmission, obtained by interpolating a horizontal layer from several Bscans. Depending on the feature of interest and the related properties, a specific imaging technique can be selected [1]. 2. Non-destructive imaging methods for inspection of timber members. In the following sections some imaging techniques applicable for the inspection of timber members on site are described. 2.1. Optical methods: photogrammetry 2.1.1. Principle of the method Photogrammetry (wave field in the visible range) can be used to extract threedimensional metric models from photographic images. It also allows reconstructing a textural database for the selected surfaces of an object. It can be adopted for analysing the extent and position of material features, visible on the inspected element surface [2]. Close range photogrammetry basically involves the use of a network of photographs of an object taken from different angles. In monoscopic photogrammetry, convergent shots at different scale can be used, thus allowing the adoption of much more flexible geometric acquisition schemes than those of the stereoscopic method. The monoscopic method allows the use of non-metric camera, after a preliminary calibration. The accuracy of the restitution depends on several factors: primarily on the scale of the photogram, secondarily on the geometry of the acquisition scheme and on the accuracy of the interior and exterior orientation [3]. Different types of light sources could be utilized for enlightenment. The illumination angle and light source position in relation to the specific heterogeneity and camera are crucial to obtain good detecting capabilities. 164 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 2.1.2. Applications Photogrammetric techniques permit to obtain reliable metric information of defects, damage and distortions, from the analysis of orthophotos. From image data, geometrical data of the detected features can be extracted, for further analysis (e.g., measurement of strength affecting characteristics, 3D visualization and modelling of the macroscopic material features). Therefore, photogram-metry can be used for supporting advanced visual strength grading of timber elements in service and for the acquisition of metric/geometric data for the numerical analysis of wooden elements [4]. 2.1.3. General remarks Site conditions and accessibility can strongly affect the applicability of the method. Metric accuracy of orthophotos depends on the acquisition methods and the camera used. It can be advisable to use natural points (e.g. features of the wooden texture) for buddle adjustment. The photogrammetric survey should be coupled with a topographic survey of control points. In case of elements with very rough/non-planar faces, the use of orthophotos can be insufficient to completely describe the material characteristics. Radiometric quality of photographs should be ensured using constant uniform lighting. 2.2. Thermography 2.2.1. Principle of the method Thermography provides information related to the thermal properties of the sample, through a map of the temperature distribution on the surface of the object. Because of the low thermal conductivity of wood, thermography allows the detection of defects near the surface (approx. 1 mm). There are two main variations of thermography the active method (i.e. inspected element is illuminated by a heat source) or the passive one (wood surface is subjected to natural heating). 165 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS The most popular device for thermal imaging is the infrared camera, which is a thermal wave detector in the infrared domain, detecting infrared radiation emitted from the object. The thermal gradient (and not the temperature itself) makes it possible to obtain information about the integrity of the structure. The thermal gradient is calculated from the temperature distribution. 2.2.2. Applications Thermography can be used as a preliminary non-contact screening procedure, to select areas for more detailed analysis. For defects detection, active thermography is generally advisable while, in many circumstances, passive thermography can be apt to map areas with higher moisture content. Thermography is also an advisable technique, for the geometrical survey of elements hidden/covered by plaster, or by other similar thin layers [4]. It can be also used to assist visual strength grading of coated timber elements (e.g. painted historical wooden members). 2.2.3. General remarks Analysis of temperature gradients generally allows detection of most superficial and sub-superficial abnormalities. However, the thermal image does not provide any information about the depth of discontinuities. As regards information about moisture, only qualitative indication about location of moist areas can be gathered, while the technique is not appropriate for quantitative estimation of moisture content. 2.3. X-ray radiography 2.3.1. Principle of the method X-ray radiography uses electromagnetic waves with wavelengths in vacuum between 10-8 m and 10-12 m. The X-rays are absorbed depending on the material density. For wood, the X-ray absorption coefficient is defined as: µ = µ'• ρ 166 (1) PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS With µ’ as the mass absorption coefficient in [m2/kg] and ρ the density of the material in [kg/m3]. The detectable X-ray waves on the film plate depends on the pulse intensity of the X-rays, the distance of the test object to the transmitter as well as to the film plate and also the thickness of the material. In the X-ray acquisition process, the test object is located between the X-ray transmitter and the film plate. The X-rays transmitted travel through the test object and will be absorbed with different intensities before they hit the film plate. The material specific absorption of the X-rays leads to the so called radiogram which will finally be transferred into a grayscale picture. The whole volume of the three dimensional test object in front of the film plate will be reproduced as a two dimensional picture. 2.3.2. Applications The X-ray radiography is mainly used for the detection of internal heterogeneities. In typical timber elements the differentiation of various densities like soft- or hardwood, sap wood or heart wood, early or late wood. Furthermore the assumptions and growing direction of knots can be distinguished. Fungal or insect decay can be observed within the X-ray radiography as well. Normally the visual inspection is used for fungal or insect decay, but in some cases structural elements are covered or only accessible from one side, so that the mobile X-ray system can be used for detailed analyses or specification of assumptions. Further assessments of timber structures using the X-ray radiography are shown e.g. in [6-7-8]. 2.3.3. General remarks The general principle of the X-ray radiography is similar to taking a picture with a photo camera. But here for the quality of the radiogram the pulse intensity, the distance of the test specimen between the transmitter and the film plate and the thickness respectively the density of the object influence the resolution and accuracy of the method. The limitations described are observed using the X-ray unit XR 200 167 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS with a maximum photon energy of 150 KVP and X-ray dose per pulse of 0.026 0.040mSv and a test object made of European Spruce with a density of 480kg/m3 and a moisture content of about 15%. The X-ray unit can be used within to the following regulations [6]: • Increasing the distance between the transmitter and the test object results in the projection of a smaller area where the object is represented enlarged but with less sharpness and more noise. • A minimum distance between the transmitter and the film plate of about 1 meter is necessary using a film plate of 30 by 40 cm. A further reduction of this distance leads to a clear “burned” spot and unusable radiograms. • Typical structural timber elements with thicknesses up to 300 mm can reliable be assessed with the used system. For greater thicknesses the contrast vanishes and only objects with distinctly different densities, e.g. parts of steel embedded in wood are visible in the radiogram. The safety requirements for the use of the mobile X-ray system do not restrict the practical use on existing timber structures. In practical use, the safety zone for this unit is specified as follows: 3 meters around the transmitter, 30 meters in measuring direction and 11 meters perpendicular to it. In general the users carry a personal dosimeter to register any irradiation. 2.4. Microwave 2.4.1 Principle of the method Microwaves are electromagnetic waves in the frequency range between about 300 MHz and 300 GHz. The microwave technique in connection with range or flight of time measurement can be termed as radar technique (radar: radio detection and ranging) or GPR (ground penetrating radar). There are two basic microwave techniques, the transmission and the reflection. In a transmission scanner the transmitting antenna, illuminates the piece of wood, with a uniform microwave field. The probes used to evaluate the signal of microwaves can be either scatterometers/ radars, which measure the scattering properties, or reflectometers, which measure the reflectivity of the workpiece due to inhomogeneous and defects. In the first mode, the material is located between two antennas (one for transmission the other for reception), in the second mode, both antennas are located in front of the material. Usually, the following equipment is required for microwave imaging: a) two dipole or horn antennas (transmitting and receiving); b) generator of electromagnetic wave at relatively high frequency and low power; c) data acquisition system[9]. 168 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS GPR system generates a series of short pulses that travel through the material and back-scatter. GPR measurements consist in recording a profile by moving the antennas on the tested structure along a linear direction. A trace (A-scan) can be recorded every centimetre of the profile. From series of A-scans, B-scan can be generated. 2.4.2. Applications Depending on the microwave frequency and measurement hardware it is possible to detect the defect presence directly, or its presence can be noticed only by the introduction of “noise” into attenuation, phase and polarization signals. In [10] a new system for the in situ evaluation of timber structures based on microwave reflectometry is presented. The obtained results show that the reflectometric methodology can clearly highlight the presence of discontinuities inside the wood, but nature and dimension of the heterogeneities cannot be characterised. 2.4.3. General remarks Due to its high permittivity, free water in materials like wood strongly influences the reflection and transmission behaviour of microwaves. The changes of the microwave properties due to moisture can be used to treat the moisture as a material property and to detect, image and quantify it and its distribution in the object [11]. As a rule of thumb, the approximate minimum detectable defect size is around half of the wavelength of the microwave frequency used. By decreasing the microwave frequency generally the penetration depth will be enhanced, but the lateral resolution at imaging will be lowered. By taking into account the parameters of the test object (dimensions, shape, moisture content, fibre orientation) and of the measurement equipment (frequency, type of antenna, microwave power, distance of object, etc.) some optimization will be necessary to get a good compromise between the resolution and penetration depth. 2.5. Stress-wave tomography 2.5.1. Principle of the method Acoustic tomography is a technique used to reconstruct the properties of the materials under inspection from stress-wave propagation data. In acoustic tomography, the most typical parameter to measure is the time of flight (TOF), i.e. the time that 169 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS it takes for the wave to travel a distance through a medium. The transit times, recorded for each pair of transmitting-receiving points, as well as the coordinates of these points, are the input data for the tomographic analysis. Velocity maps are the output data. Local apparent velocities are computed over a Cartesian grid of square pixels, according to the geometric arrangement of the sensors on the element surface. Tomographic images are then generated as the velocity distribution throughout the inspected section. The basic equipment for stress-wave TOF data acquisition is composed by: • • • • • • an oscilloscope, for visualization and analysis of the signal; a function generator, with a given pulse repetition frequency; a timer, which controls both the trigger of the generator and the counter; a signal amplifier; a signal filter; an instrumented hammer for emitting low frequency signals (< 10 kHz); alternatively, transducers can be tapped with a steel hammer to generate sound waves; • piezoelectric transducers, which are used for emitting high frequency signals (typically, 20÷100 kHz); • piezoelectric transducers for receiving the signal (or micro-accelerometers, in case of low frequency signal); • preamplifiers, which are required in most applications on wood, because of the high attenuation of the transmitted waves in the material, especially in case of thick elements. For tomographic data acquisition, it is desirable to use a multi-channel device to speed up the measures. Alternatively, a set of probes, operating both as signal emitter and receiver, can be used. The definition of the parameters for data acquisition depends on the experimental conditions and the scale of the investigated characteristics. The minimum size of the detectable defects is predetermined, depending on the frequencies used and the geometric resolution of the tomography. Frequency range of the emitting source has to be chosen in order to optimize resolution of the analysis and attenuation of the signal. The acquisition scheme for each specific test should be carefully designed, considering the characteristics of the investigated section and the accessibility of the sensed surface [11]. 2.5.2. Applications Acoustic tomography can be applied to timber structural elements to detect strength affecting heterogeneities (i.e., knots) and damage (i.e., decay, cracks). In particular, longitudinal tomograms are useful for screening the element along the entire length, identifying problematic areas, where low velocity values are mapped. Imaging of selected transverse sections is aimed at gross estimation of the 170 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS heterogeneity extent. Very high velocity values in acoustic tomograms of wood are generally associated with knots. Low velocity areas are associated with low material density, often caused by decay. In particular, decay due to rot fungi and diffuse insect attacks can be detected by means of the acoustic tomography. 2.5.3. General remarks The main methodological aspects, which influence acoustic tomography, are the applied frequency, the number of independent measurements, the adopted acquisition scheme and the applied inversion technique. The technique permits only qualitative, large-scale analysis (e.g., maps of entire elements),whereas complementary non-destructive/semi-destructive methods should be used to obtain local quantitative information. In general, it is recommended to couple acoustic tomography with local mechanical tests, such as resistance drilling tests, for the detection of internal zones of lower densities, and with visual/photographic analysis of the element faces for correlation of internal features and external indicators [12]. 3. Conclusions For inspection of timber structures it is important to reliably detect defects, damages and material heterogeneities in wooden members. Normal praxis based on visual inspection and point measurements of drill resistance can be improved through multi-sensor, multi-scale, multiresolution analysis [13]. Most of the techniques described in the paper allow qualitative analysis of the elements and detection of the presence and location of main gross defects and damage. High-resolution photogrammetry and IR thermography have great potential as preliminary noncontact screening procedures, to select areas for introspective analysis. Stress-wave ToF tomography and microwave scanning, thanks to their completely non-destructive nature and the possibility to map large timber sections, can be adopted as large-scale global evaluation method, for decay and defect detection in the interior of the wood material, to be followed by further investigation on anomalous velocity areas. X-ray radiography can be used for more detailed investigation of specific points in the structure. 171 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS References [1] Bucur V. (2003) Nondestructive characterization and imaging of wood. Springer, Berlin/Heidelberg. [2] Riggio M., Prandi F., De Amicis R., Piazza M. (2011). Geometrical characterization of timber structural elements in the roof of S. Lorenzo church in Tenno (TN, Italy) using close range photogrammetry. CULTURAL HERITAGE Istanbul 2011. 5th International Congress "Science and Technology for the Safeguard of Cultural Heritage in the Mediterranean Basin". Istanbul, Turkey, 22-25 November 2011. [3] Kraus, K. (2007). Photogrammetry. Geometry From Images and Laser Scans. Walter de Gruyter, Berlin. [4] Riggio M, Prandi F, De Amicis R, Piazza M (2012). Use of high resolution digital images and NDT imaging techniques for the characterization of timber structural elements. In: Nondestructive Testing of Materials and Structures. O. Büyüköztürk et al. (eds), RILEM Bookseries 6:365-371. [5] Cantini L, Tedeschi C, Tiraboschi C, Binda L. Use of thermovision for the survey of a timber vault in Torino. In: Nondestructive Testing of Materials and Structures, O. Büyüköztürk et al.(eds.), RILEM Bookseries 6, Pages 1203- 1208. RILEM 2012. [6] Franke S., Franke B., Scharmacher F. (2013). Assessment of timber structures using the X-Ray technology, Advanced Materials Research, Vol. 778, pp. 321-327 [7] Brashaw B.K., Bucur V., Divos F., Goncales R., Lu J., Meder R., Pellerin R.F., Potter S., Ross R.J., Wang X., Yin Y. (2009). Nondestrucitve testing and evaluation of wood: A worldwide research update, Forest Products Journal 2009/59, pp. 7-14. [8] Wei Q., Leblon B., La Rocque A. (2011). On the use of X-ray computed tomography for determining wood properties: a review, Can. Journal for Res. 2011/41, pp. 2120-2140. [9] M. Sbartaï. Ground penetrating radar. In: In Situ Assessment of Structural Timber: Discussion of Classical and Modern Non-Destructive and Semi-Destructive Methods for the Evaluation of Wood Structures; Series: RILEM State of the Art Reports, Kasal, Bohumil; Tannert, Thomas (Eds.), Springer, 2011, Vol.7, Pages 25-36 [10] Macchioni N., Mannucci M., Olmi R., Sabrina Palanti1,d, Cristiano Riminesi. (2013) Microwave reflectometric tool for non-destructive assessment of decay on timber structures. In Proceeding of the 2nd international Conference on Structural Health Assessment of Timber Structures. Advanced Materials Research Vol. 778. Pages 281-288 Trans Tech Publications, Switzerland 172 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS [11] Schajer G.S., Orhan F.B. (2006). Measurement of wood grain angle, moisture content and density using microwaves, Holz als Roh- und Werkstoff. 64, 483– 490 [12] Dackermann U., Crews K., Kasal B., Li J., Riggio M., Rinn F., Tannert T. (2014). In situ assessment of structural timber using stress-wave measurements. Materials and Structures . 47 (5): 787-803. [13] Riggio M, Sandak J, Franke S (2015). Application of imaging techniques for detection of defects, damage and decay in timber structures on-site, SI: Appraisal of Wooden Members, Construction and Building Materials, 2015 -Elsevier (in press). 173 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 174 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Assessing the integrity and strength of gluelines Philipp Dietsch Thomas Tannert Dr.-Ing., Team Leader Timber Structures Chair of Timber Structures and Building Construction Technische Universität München, Germany Assistant Professor, PhD, PEng Associate Chair Wood Building Design and Construction The University of British Columbia, Canada 1 Introduction Historically, timber structures were characterized by wood elements which were limited both in their cross-sectional dimensions and length by the dimensions of the existing tree population in the surrounding area. The step from solid timber elements to glued(-laminated) timber elements, started by Hetzer [1], represented a significant technological progress, widening the range of application of timber structures in the building sector. Joining single boards to continuous lamellae and subsequently gluing and stacking them enabled to disengage from the size of the stem cross section and to reduce the effect of defects (e.g. knots) in the material. The results were larger and more variable (e.g. curved) geometries and timber being increasingly used, e.g. for large-span structures. Consequently, the importance of assessing large timber structures grew, naturally resulting in an increased interest of the professional community in assessment methods for existing timber structures. The need for an assessment of an existing structure can be based upon a multitude of reasons, e.g. (taken from [2]): change of the requirements to the use or to the structure (increased loading, increased service life …) doubts whether the assumptions applied during the design are fulfilled (no inspection for longer period or negative results of an investigation, unexpected degradation, accidental loads, new knowledge …) The performance of glulam beams depends on the quality of the individual lami-nations, the quality of the finger joints and the quality of the glue-lines. This chapter focuses on methods to assess the gluelines of glued timber elements. The assessment of the laminations is comparable to the assessment of solid sawn timber (moisture content, rot …) and finger joints have shown less probability of causing structural damages or failures. There are multiple methods available to assess the properties of interest. 175 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Nevertheless each method only allows assessing a certain type of property or damage. Therefore the application of just one method might not be suitable to enable confident decisions, making it necessary to combine different methods to derive a full picture about the residual performance of the gluel-ines. The objective of this chapter is therefore to present feasible methods to assess gluelines in structural timber elements and to evaluate each of them with regard to the following objectives, see also [3]: Which properties can be determined / which properties cannot be determined? How accurate and precise are the results (e.g. degree and size of damage; local/ global results)? How complex and time consuming is its application (on-site, (non-) destructive)? Which combinations of methods are useful to derive a clear picture of the structural integrity of the assessed structure? 2 Approach to the assessment of gluelines The objective of any assessment of a structure is to detect, localise and document damage, to determine the actual degree of damage, to identify the reasons for damage and to define means to repair the damage. Typically the assessment is divided into different phases, structured by the detailedness of the investigations. The obligatory visual inspection (Preliminary Evaluation - Phase 1) can be followed by more precise methods to detect and localise damage, e.g. non-destructive or semi-destructive techniques (General Investigation - Phase 2, Detailed Investigation - Phase 3). Sometimes the on-site assessment is supported by investigations in the laboratory. The sequence of a structural assessment can be summarized in a flowchart, see Fig. 1. The number of phases necessary depends on the level of doubt, the feasibility and simplicity of repair or strengthening, in combination with economic considerations. Depending on the type of structural property to be assessed and the phase of assessment, there are a number of applicable assessment methods. With respect to the assessment of gluelines, the three major properties of interest are: type of glue used, e.g. to assess its durability in given conditions integrity, i.e. potential loss of bond of the glueline due to cracking or delamination strength of the glueline, e.g. shear strength 176 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Fig.1 Illustration of the phases approach (from [4]). Methods that are applicable for the assessment of the integrity and strength of glu-elines are described in the following. Hereby the described methods are listed in the order 1) property of interest and 2) frequency of application. Each description is concluded by a short evaluation of the method in tabular form. 177 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 3 Methods to determine the type of glue used 3.1 Review of documentation (and visual inspection) Before starting any assessment of a structure, adequate attention should be given to any existing documentation. A thorough review of documentation can give an expeditious overview of the structure which would require more time if all necessary information had to be acquired on site. Some information can only be drawn from existing documentation, since it is simply not obtainable anymore by other means (e.g. producer, conditions during gluing, previous inspections …). In the case of historical structures, original planning documents are in most cases not available anymore, but chances are that they can be found in historical archives. For buildings constructed after the turn to the 20th century, copies of original blueprints or sketches may be available which contain useful dimensions. If a building has already undergone renovation or reconstruction, newly established documentation, based on measurements of dimensions in the existing building is sometimes available. For such cases or for recently constructed buildings, documentation is – in many countries - kept in administrative offices of the building authorities (municipalities or states). In other countries, such documentation is kept by the building owner. Companies involved in the design and construction are also a good source to receive planning documentation (original designs). If these sources do not reveal the necessary information, openly available literature can be an eligible source since quite a few buildings are covered in books on architecture or architectural magazines as well as magazines for structural engineers or craftsmen. In the case of glued timber elements, existing documentation can yield information on e.g. wood species and strength class; type of glue, producer and gluing process; transportation, gluing on site and coatings. Such information can oftentimes eliminate costly and time-expensive assessment methods. If the type of glue cannot be identified by available documentation, it can - in the case of resorcinol glue - be determined by its apparent characteristics, i.e. its dark colour and its typical odour when scoring the surface. A white glue line is oftentimes an indicator for urea-formaldehyde or melamine formaldehyde glue (at least for buildings constructed before the millennium). A first indication which of the two types of glue was used is given by the age of the glued timber element: the first melamine glues were used from 1975 onwards. 3.2 Laboratory tests The most common objective potentially necessitating laboratory tests for glued timber specimen is the determination of type of glue. A first indication can be derived from a boiling test on the basis of EN 314-1 [5] or, more recent, EN 302[6]. The sample, mostly a drill core (see chapter 5.1) is exposed to boiling 178 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS water for six hours and subsequently to cold water for two hours. Specimens featuring a glue line from urea-formaldehyde will in most cases fall apart during this treatment, since this type of glue is not permanently moisture proof. Specimens featuring a glue line from melamine-formaldehyde should still be intact and should still deliver acceptable strength when tested. It is the authors experience even specimens with glue lines from melamine-formaldehyde sometimes fail during this treatment. A more accurate option is to use spectral analysis to identify the type of glue used. This method is based on a differentiation by means of the different absorption spectra of substances. A common tool for this analysis is the X-ray diffractometer. Table 1 Laboratory tests - Evaluation. Type Optical; thermo-mechanical; Application non-stationary; semidestructive Phase III (Rare) Extent Local / Global Time / Cost High / Medium Validity of results Good (exact) Constraints Rather complex and time-consuming; only in laboratory 4 Methods to assess the integrity of gluelines 4.1 Visual inspection A visual inspection is part of every structural assessment and is a mandatory basis for further examinations. It should be carried out in combination with a review of existing documentation and planning documents (see preceding paragraph). The latter can aid to receive a clearer picture of the structure before the actual assessment on-site. It helps to determine, if the structure was carried out according to plans and to carry out comparative calculations in order to check which members are highly utilized. There is no universally valid approach to a visual inspection. Every engineer has to find an individual approach according to his/her experiences.There is a multitude of reference books and check-lists which can support the assessment of failures, e.g. [7], [8], [9]. These instructions oftentimes only apply to certain building and construction types and are only meaningful if applied by experienced engineers. The visual inspection yields an impression of the overall condition of the structure and the glued timber elements, including a first overview and registration of the visible degree of damages. All accessible structural elements are examined handson, e.g. in terms of cracks in the glueline or delamination. A magnifying glass can aid in determining the age of a crack or delamination (dust, discolouration within crack) and potential adhesion or cohesion problems. Magnifying glasses often come 179 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS with an integrated lamp to lighten the crack, enabling to take pictures magnifying the interior of the crack, see Figs. 2-5. It is self-explanatory that the visual inspection has to be well documented. Thereby, the benefits of photography as part of an easily accessible and comprehensive documentation are obvious. The captions of the pictures picked for the written documentation should include a clear indication of the location of the detail within the structure. Areas that are designated for further examination by more specific methods should be marked on site and in the documentation. A building book has proven to be a good tool to facilitate future inspections and to guarantee a consistent documentation, even with the change of authorized personnel [10]. Fig. 2 Open glueline in glulam beam. Fig. 3 Magnifying glass and camera Fig. 4 Magnified detail of open glueline, inadequate gluing during production Fig. 5 Magnified detail of open glueline, failure due to changes in timber moisture content. Table 2 Visual Inspection - Evaluation. Type Visual; on-site; non-destructive Application Phase I (always) Extent Local/ Global Time / Cost Low / Low Constraints Limited to surface; not quantifiable information; dependent on experience; accessibility can be limited Validity of Limited (qualitative; on results surface; experience) 180 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 4.2 Mapping of delaminated areas and/or cracks For a description of this method, the interested reader is referred to the chapter “Mapping of cracks and effect of environmental conditions” in this publication. Apart from the crack dimensions (length, width, and depth), the position of cracks within the structural element is essential for the evaluation of their consequence on the structural integrity of the timber element. It is also relevant if the cracks appear predominantly or with a certain frequency in the timber or in the glueline. A crack in the direct vicinity of the glueline is not in all cases an indication of adhesion or cohesion problems. The wood material in the vicinity of the gluelines is the weakest part of the lamella due to the cutting of fibres during sawing. In addition, there is a discontinuity between the density of the boards and also between the shrinkage movements of both sides. Oftentimes the cracks occur in the boundary layer next to the glue line but within the wood. The crack should therefore be closely investigated before conclusions on the failure mechanisms are drawn [11]. Table 3 Mapping of delaminated areas and/or cracks - Evaluation. Type Visual ; on-site ; Application Phase I (Frequent) Extent non-destructive Time / Cost Medium / Low Validity of results Local Constraints Local and temporary assessment; investigation of larger areas time-consuming 4.3 Stress waves - Ultrasonic Echo Technique The use of stress waves is based on the propagation of sound waves through material. Amongst the different possibilities to apply stress waves in the assessment of timber members (see e.g. [12], [13], [14]), the ultrasonic echo technique could prove promising with respect to assessing the integrity of gluelines, since it can provide information on the distribution of interior defects. The ultrasonic echo technique is based on the reflection of waves on material inhomogenities. The sonic wave passes through the element and is reflected. The so-called back-wall echo is received by the sensors. Structural irregularities produce a change in signal structure of the back wall echo. The results are given as A- and B-scans, see Fig. 6. The A-scan shows the transmission time and intensity of the pulse, while the B-scan is a composition of various A-scans that are recorded with a defined distance between them, see Fig 7. The B-scan is a 2D cross section through the specimen and enables to identify a change in signal structure along the measured axis. By combining several B-scans, it is possible to interpolate a horizontal layer (C-scan) that gives 3D information about the internal structure. 181 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS The experimental set-up consists of a signal generator, a preamplifier, an amplifier, a transducer and a data acquisition system. For the measurement, the sensor is placed on a surface of the element. To limit signal retardation, a specific coupling pressure or a coupler (e.g. water, oil, paste, rubber) has to be applied to create complete contact between the transducers and the material surface. In some cases, the surface of the member may need preparation as smoothing the surface though planning or sanding. In [16] it was shown that the application of shear waves and reflection measurements is mandatory if thin defects (like small cracks or delami-nations) are to be assessed. Some of the abovementioned challenges are overcome by using air-coupled ultrasonic technique [17] but its application is still limited to laboratory conditions or production control and smaller samples. Fig. 6 Illustration of A (left), B (middle) and C (right) scans, from [15] Fig. 7 Result of B-scan (transversal waves) of glulam member with crack, from [14] The technique has shown to have sensitivity to delamination [18], it is lowcost and portable. However, its application over larger areas is time-demanding. Several factors can affect the transmission of stress waves in timber, equipment application and the interpretation of results. Access to in-situ members may also limit 182 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS the use of some stress wave techniques. The ultrasonic echo technique allows the direct localization of a reflector like a back wall or any inhomogenity like damage in the structure. It is difficult, however, to locate the exact position of damage or to distinguish between one large irregularity and many small ones. Nevertheless, it can be assumed that a clear back wall echo shows that the specimen is free of defects. Systematic measurements on sample specimens with artificial imperfections are required to make qualitative conclusions from measuring results. An exact classification of damage by analysing the signal structure is not yet possible. Table 4 Ultrasonic Echo Technique - Evaluation. Type Stress Waves Application Rare (Phase III) Extent Local Time / Cost Medium / High Validity of results limited (experience, Constraints type of damage) Accessibility; sensitivity to defects; interpretation experience-dependent; time-consuming 5 Methods to assess the strength of gluelines 5.1 Shear tests on core samples Shear tests on circular core samples are used to derive the shear strength of glue lines in glued-laminated timber elements. The method was developed for production control [19], [20], [21] but is being applied to determine the shear strength of builtin glued timber members as well, although this approach is reason for discussion [22], [23]. When extracting core samples in-situ, proper drilling and orientation is important. The glue line needs to be in the centre of the specimen and perpendicular to the drill axis. The necessary equipment includes an electrical drill for sample extraction which is mounted on a supporting fixture. The equipment is temporarily fixed onto the glued timber member (e.g. by screws) to guarantee a correct drilling position and prevent lateral motion of the drill during extraction, see Fig. 9. The core samples taken from a member give information about the specific location from which they were taken. Since the quality of the glue line can vary significantly within and between members, multiple samples must to be taken to be representative for the structural member which they are taken from and to receive global estimations of a members mechanical properties. Samples should be drilled in zones featuring low stresses and/or in compression zones of critical locations, e.g. close to bearings. Access to these locations of in situ members can be very difficult. In some locations, the necessary attachment of the supporting fixture onto the member is inhibited. The drill bits need to be sharp to extract the shear core samples of approximately 35 mm in diameter and up to 120 mm in length, see Fig. 8 and Fig. 10. Voids left by drilling should be fully plugged by glued-in wood cores to restore stress-transfer, to prevent moisture and insect penetration and to restore the appearance of the member. The samples should be labeled with member, date, 183 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS location, and other pertinent information and be stored and transported in containers that provide adequate protection. The samples are usually tested in shear, but density and moisture content can also be determined. Furthermore samples can also be used for species and adhesive type identification by performing microscopic and chemical investigation. For shear testing, the specimens need to be flattened on two sides and the exact dimensions of the shear plane need to be measured before testing. The shear cores may be divided into sub-samples, featuring lengths of at least 50 mm, see Fig. 8 and Fig. 11. After reaching constant moisture content, the specimens are placed into the space between the jaws of a test machine with the glue line oriented parallel to the loading direction, see Fig. 12. Proper alignment of the specimen in the fixtures is crucial for accurate strength estimates (max. 1 mm deviation). However, the shear stresses in typical shear test fixtures are not evenly distributed and no pure condition of shear stress scan be created, rather a combination of shear and normal compressive stresses. The shear strength is determined from the load upon failure through the following equation 0.78 0.044 ∙ ∙ Fig. 8 Geometry of drill core Fig. 9 Extraction of core from glulam beam. Fig. 10 Drill core in laboratory 184 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Fig. 11 Specimens prepared from drill core Fig. 12 Shear testing of specimen In addition to the shear strength, the percentage wood failure (PWF) has to be determined after testing. This is a critical index to determine the quality of a bond and is usually measured by trained personnel by visual examination of the failure surface. In specimens with colorless glue, the surfaces are treated with chemicals (first hydrochloric acid, then by phloroglucinol) to better distinguish regions of wood failure from regions of glue-line failure [24]. The areas that turn red indicate fiber failure, as the lignin changes color. To determine PWF, usually two people independently evaluate the specimens. If their results deviate by more than a certain percentage, they consult a third person. Nevertheless, the determined PWF remains subjective, making it difficult to compare test results of different studies. Image analysis technique could be an alternative to calculate the PWF [25]. Depending on PWF, different requirements on the strength of glue lines exist [21] [26]. A higher percentage of glue failure leads to higher requirements on the reference strength to which the determined shear strength is compared. If the determined shear strength reaches the reference strength given in e.g. [21], the applicable design shear strength (listed in the respective product or design standard) may be used. In no case should the determined shear strength be used as reference shear strength for structural calculations. If the reference values are not achieved, further investigations are necessary. These include the maximum utilization of the member in shear and the size of the area under high shear stresses. Table 5 Shear tests on core samples - Evaluation. Type Mechanical; nonstationary, semi-destr. Application Phase II (meduim) Extent Local Time / Cost High / Medium Constraints Accessibility; local assessment; variation of glueline quality; percentage wood failure; semi-destructive (surfaces) Validity of High (on a local level) results 185 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 6 Conclusions As for other timber properties to be determined through assessment methods it can be stated that most assessment methods utilized today can give qualitative information but only a few non- or semi-destructive methods can give quantifiable information. Applicable methods to determine global strength parameters of built-in timber elements are very scarse. An approach would be to correlate strength parameters from measured stiffness parameters which are easier to derive. But the correlation between stiffness parameters and strength parameters for common britle failure types like tension perpendicular to grain and shear failure are too low, leaing a low level of confidence. As a consequence, all data received requires a very careful evaluation by an experienced engineer. Expert’s reports treating the structural safety of a structure featuring gued timber elemnts will oftentimes be set up from a standpoint which could be summarized as “safe on the best knwledge we have”. References [1] Hetzer O. Patentschrift Nr. 197773 vom 22. Juni 1906: Gebogener Holz-Bauteil für vereinigte Dach-Pfosten und-Sparren. Kaiserliches Patentamt, Berlin. 1906 [2] Steiger R, Köhler J. Development of new swiss standards for the assessment of existing load-bearing structures. Paper 41-102-2. In: Proceedings of the 41st meeting of CIB W-18. St. An-drews, Canada. 2008. [3] Dietsch P, Köhler J (eds). Assessment of timber structures. Shaker Publishing Company, Aa-chen (Germany). ISBN 978-3-8322-9513-4. 2010. [4] Diamantidis D (ed). Probabilistic assessment of existing structures - a publication of the joint committee on structural safety (JCSS). RILEM Publications S.A.R.L The publishing Company of RILEM. 2001. [5] EN 314-1:1993. Plywood, Bonding Quality, Part 1 – Test methods. CEN, Brussels. 1993 [6] EN 302-2:2013. Adhesives for load-bearing timber structures – Test methods – Part 1: Determination of longitudinal tensile shear strength. CEN, Brussels. 2013 [7] Görlacher R. Hölzerne Tragwerke Untersuchen und Beurteilen. Sonderforschungsbereich 315 „Erhalten historisch bedeutsamer Bauwerke“, Baugefüge, Konstruktionen, Werkstoffe. Uni-versität Karlsruhe (TH). Verlag Ernst & Sohn, Berlin. 1996 [8] Blaß H-J. Brüninghoff H. Kreuzinger H. Radovic B. Winter S. Guideline for a First Evaluation of large-span Timber Structures. Council for Timber Technology, Wuppertal. 2006 [9] SEI/ACSE 11-99. Guideline for Structural Condition Assessment of Existing Buildings. ASCE Publications. ISBN 0-7844-0432-1. 2000 [10] Dietsch P. Winter S. Assessment of the Structural Reliability of all wide span Timber Structures under the Responsibility of the City of Munich. 33rd IABSE Symposium Proceedings. Bangkok, Thailand. September 9-11 2009 [11] Brüninghoff H. Effects of (seasonal) changes in Environmental Conditions on structural Timber Elements. in: Dietsch P, Köhler J (eds.). Assessment of timber structures. Shaker Publishing Company, Aachen (Germany). ISBN 978-3-8322-9513-4. 2010 [12] Bucur V. Ultrasonic Imaging. In: Nondestructive Characterization and Imaging of Wood. Springer, Berlin. 2003. pp. 181–213. 186 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS [13] Kasal B. Lear G. Tannert T. Stress Waves. in: Kasal B, Tannert T. (eds): In Situ Assessment of Structural Timber. Springer. ISBN 978-94-007-0559-3. 2011 [14] Hasenstab A. Integritätsprüfung von Holz mit dem zerstörungsfreien Ultraschallechoverfahren. Bundesanstalt für Materialforschung und –prüfung BAM. Dissertationsreihe Band 16. Berlin. 2006. [15] Krautkraemer J, Krautkraemer H. Werkstoffprüfung mit Ultraschall. Springer, Berlin. 5th edition. 1985 [16] Dill-Langer G. Aicher S. Non-destructive detection of glue line defects in glued laminated timber. WCTE 2008 Conference Proceedings. Miyazaki, Japan. 2008 [17] Sanabria Martín S. J. Air-coupled ultrasound propagation and novel non-destructive bonding quality assessment of timber composites. Dissertation. ETH Zurich. 2012 [18] [18] Maeva E. Severina I. Bondarenko S. Chapman G. O’Neill B. Severin F. Maev R. G. Acoustical methods for the investigation of adhesively bonded structures: A review. Canadian Journal of Physics, Vol 82, No 12. pp. 981–1025. 2004. [19] EN 392. Glued laminated timber - Shear test of glue lines. CEN, Brussels. 1995. [20] Steiger R. Risi W. Gehri E. Quality control of glulam: shear tests of glue lines. Paper 40-12-7. Proceedings of the 40th meeting of CIB-W18. Bled, Slovenia. 2007. [21] EN 14080. Timber structures – Glued laminated timber and glued solid timber - Requirements. CEN, Brussels. 2013. [22] Brüninghoff H. Shear tests on core samples - critical discussion on the evaluation of results, in: Dietsch P, Köhler J (eds). Assessment of timber structures. Shaker Publishing Company, Aachen (Germany). ISBN 978-3-8322-9513-4. 2010. [23] Tannert T. Vallée T. Müller A. Critical review on the assessment of glulam structures using shear core samples. Journal of Civil Structural Health Monitoring, Vol 2, No 1. pp 65-72. Springer. 2012 [24] Künniger, T. Automatische Bestimmung des prozentualen Faserbruchanteils bei der indust-riellen Klebfestigkeitsprüfung. FFWH Project report 2006.05. EMPA, Dübendorf, Switzer-land. 2007. [25] Yang Y, Gong M, Chui Y.H. A new image analysis algorithm for calculating percentage wood failure. Holzforschung, Vol 62. 2008. pp. 248–251 [26] ASTM D 5266. Standard Practice for Estimating the Percentage of Wood Failure in Adhesive Bonded Joints. ASTM International, Conshohocken PA, USA. 1999. 187 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 188 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Mapping of cracks in glulam beams and assessing the effect of environmental conditions Philipp Dietsch Dr.-Ing., Team Leader Timber Structures Chair of Timber Structures and Building Construction Technische Universität München, Germany 1 Introduction For the timber community, the step from solid timber elements elements to glued(laminated) timber elements, started by Hetzer [1], represented a t significant technological progress, widening the range of application of timber structures in the building sector. The results were larger and more variable (e.g. curved) geometries and timber being increasingly used, (e.g. for largespan structures. Consequently, the importanec of assessing large timber structures grew. naturally resulting in an increased interest of the professional community in assessment methods for existing glulam structures. The performance of glulam beams depends on the quality of the individual laminations, the quality of the finger joints, the quality of the glue-lines and the integrity of the cross-section which is made up of single lamellae which are stacked and glued to cross-sections. The most frequent damage affecting the integrity of the cross-section is cracking. Cracks are a form of stress relief. The reason for the frequent occurrence of cracks in grain direction of timber elements is the very low tensile strength perpendicular to the grain of wood. The reason for tensile stresses perpendicular to the grain in glulam elements can be manifold: external loading, internal stresses due to deviation forces in e.g. curved members, uneven shrinkage of the cross-section due to changes in moisture content (moisture gradients). The objective of this chapter is to present feasible methods to map cracks, to assess environmental conditions and to evaluate each of them with regard to the following objectives, see also [2]: What can be determined / what cannot be determined? How accurate and precise are the results (e.g. degree and size of damage; local/ global results)? How complex and time consuming is its application (on-site, (non-) destructive)? 189 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 2 Approach to the mapping and assessment of cracks The objective of any assessment of a structure is to detect, localise and document damage, to determine the actual degree of damage, to identify the reasons for damage and to define means to repair the damage. Typically the assessment is divided into different phases, structured by the detailedness of the investigations, see e.g. [2]. The number of phases necessary depends on the level of doubt, the feasibility and simplicity of repair or strengthening, in combination with economic considerations. The detection and assessment of cracks is part of almost every assessment of timber structures, especially largespan glulam structures. While a partial detection of cracks is performed during the first site-visit, a detailed investigation, including a complete mapping of all cracks may be carried out during the detailed inspection. With respect to the assessment of cracks, the major properties of interest are: Location, length and depth of crack Reasons for the crack (inevitable, remedial measures possible) Effect of crack on structural safety (stress transfer) of timber element 2.1 Manual/visual mapping of cracks Fig. 1 Common equipment for the mapping of cracks: magnifying glass; thickness gauge; laser distance measuring device; folding rule Fig. 2 Measurement of crack depth with thickness gauge (0.1 mm) Fig. 3 Indication of crack depth with folding rule Fig. 4 Magnifying glass and camera 190 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS The most common approach to detection and documentation of crack distribution as well as measurement of crack dimensions is to use a thickness gauge (0,1 mm) and a tape measure/folding rule, see Fig. 1 - Fig. 3. A magnifying glass can aid in determining the age of a crack (dust, discoloration within crack) and potential adhesion or cohesion problems if cracks appear mainly in the glueline, see Fig. 4 [3]. It is self-explanatory that the mapping and assessment of cracks has to be well documented on the timber element and in the written documentation, including clear indication of the location of the crack within the structure, see Fig. 5 and Fig. 6. The marking/mapping of crack width, depth and crack tips is important to analyse possible changes in crack dimensions over time. This is essential for structures which are subjected to seasonal environmental changes, leading to changing timber moisture content which can have an influence on crack dimensions. I t = 60 mm II t = 45 mm Numbering Largest depth incl. location Marking of crack ends Fig. 5 Example of marking of cracks on structural timber element Element / Axis Cracks: Pos: i di View from xi di ℓi wi N E S W 1 Moisture measurement: yes no 2 Crack width Crack length Crack depth Distance from e.g. bottom flange Distance from e.g. support Comments Fig. 6 Example of written documentation of cracks The determination of the crack dimensions aids to assess the remaining residual cross section of structural elements. In this context the crack depth is of particular importance since it indicates the residual cross-section to transfer stresses, see Fig. 7. The crack depth should be measured at multiple locations along the crack. [4] indicates possible space intervals for the measurement of crack depths. For longer cracks, these intervals (measurement at each ¼ of the length) should be reduced. Diverging cracks are problematic in that aspect since their real depth cannot be accurately measured with a thickness gauge, see Fig. 8. A core sample can give clearer information, see Fig. 9 and Fig. 10, nevertheless this remains a local and destructive measure. 191 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Thickness Gauge di Remaining cross-section Remaining cross-section to transfer shear stresses or tensile stresses perpendicular to the grain Remaining cross-section from measurement Fig. 7 Schematic of crack depths and remaining cross-section to transfer stresses Fig. 8 Difficulty to accurately measure depth of diverging cracks with thickness gauge Fig. 9 Indication of crack depth on a core sample, here: crack in glueline Fig. 10 Magnification of crack in a core sample, here: crack in glueline Table 1 Manual mapping of cracks - Evaluation. Type Visual; on-site; non-destructive Application Phase I (always) Extent Local Time / Cost Medium / Low Constraints Local and temporary assessment; depth of diverging cracks cannot be examined accurately; time-consuming Validity of Limited (incertitude results about crack depth) 2.2 Alternative methods – potential for application Potential options to manual assessment and mapping of cracks are optical devices or laser scanning. Preliminary investigations have shown, however, that laser scanning incorporates the same drawbacks as manual measurement with a thickness gauge since it requires a straight crack of sufficient width [5]. The light-section method constitutes another option. However, this method requires adequate crack width which is not always given. 192 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Another method to assess the location and dimension of cracks is the ultrasoundecho-technique whereby the air-coupled ultrasonic technique seems to be the most promising [6] since it is low-cost and portable. Currently its application is still limited to laboratory conditions or production control and smaller samples. Its application over larger areas is time-demanding. The ultrasonic echo technique allows the direct localization of a reflector like a back wall or any inhomogenity like damage in the structure. It is difficult, however, to locate the exact position of damage or to distinguish between one large irregularity and many small ones. For a description of the ultrasound-echo-technique, the interested reader is referred to [3] (this publication) and to [6]-[11]. Radiography (X-Ray) represents another option since it can deliver information on the internal structure of members. Detection of cracks using radiography requires that the crack be of adequate size, at least 2% of the member thickness [12], and the crack being oriented parallel to the radiation beam. In combination with the requirement to access the opposing sides of a member, these can constitute exclusion criteria when assessing glulam elements. Safety issues and high initial costs of the equipment constitute additional drawbacks of radiography. For a description of this method, the interested reader is referred to [13]-[15]. 2.3 Evaluation of the consequence of cracks To evaluate the consequence of a crack on the structural integrity of the timber element, information on the crack dimensions (length, width, and depth) and especially the position within the structural element is essential, Fig. 11 and Fig. 12. h =hap Tension perp. ℓ Shear Shear max t,90,max m max max t,90 Fig. 11 Consequence of cracks - Schematic illustration of the distribution of bending stresses, shear stresses and tensile stresses perpendicular to the grain in straight beam and curved beam, from [16] 193 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS The measured crack dimensions and location are to be evaluated individually for each structure. This includes the structural system, the relevance of the structural element, building use and environmental boundary conditions to determine the causes and possible consequences of cracks. Within the scope of structural boundary conditions it should to be differentiated between cracks in areas of high shear and areas of high tension perpendicular to the grain stresses, Fig. 11 and Fig. 12. Some literature indicates permissible crack depths for such areas, e.g. [17]-[20]. ℓ 0 10 20 Bending stresses/ Bending capacity σm,d [MN/m2] fm,d [MN/m2] 0 1 2 Shear stress/ Shear capacity τv,d [MN/m2] fv,d [MN/m2] 1 t = 70 2 t = 85 3 t = 45 5 4 t = 50 t = 85 6 t = 65 7 t = 90 Illustration of crack distribution ℓ 0 20 40 60 80 100% Explanation: 0 20 40 60 80 100% 0 20 40 60 80 100% Percentage of member width (b = 160 mm) Required width according to standards (max. permissible crack depth) Required width considering distribution of shear stresses over member depth Required width considering distribution of shear forces over member length Remaining width respectively remaining crack depth Fig. 12 Schematic of remaining member width in dependence of location and depth of cracks in comparison to required width to transfer existing stresses, here shear stresses, from [21]/[22] 194 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS It is also relevant if the cracks appear predominantly or with a certain frequency in the wood or in the glueline. A crack in the direct vicinity of the glueline is not in all cases an indication of adhesion or cohesion problems. The wood material in the vicinity of the gluelines is the weakest part of the lamella due to the cutting of fibres during sawing. In addition, there is a discontinuity between the density of the boards and also between the shrinkage movements of both sides. Often times the cracks occur in the boundary layer next to the glue line but within the wood. The crack should therefore be closely investigated before conclusions on the failure mechanisms are drawn [23]. 3 Assessing the effect of environmental conditions 3.1 Measurement of temperature and relative humidity The measurement of temperature and relative humidity is part of every assessment of a structure. Information on the macroclimate is – among other things - needed for a comparison with the timber moisture content. The measurement of air temperature and humidity should be realized in the vicinity of the structural component by means of thermometer and hygrometers. The relative humidity is commonly measured by capacitative hygrometers which measure the change in the dielectric constant of a material between two condensator plates during water adsorption. The drawback of measurements carried out during an assessment of a structure is that these represent temporary measurements and do not allow for extrapolation with respect to seasonal changes of macro climate. Information on the latter is e.g. necessary to explain moisture gradients in the timber elements. In these cases, the monitoring of environmental conditions, which can be coupled with the monitoring of timber moisture content, represents a feasible solution [24]. 3.2 Measurement of wood moisture content The measurement of wood moisture content can be realized by several methods. The traditional method of measuring moisture content is the gravimetric method – i.e. oven drying of wood specimens. It necessitates the extraction of specimen from the timber element. These are weighed before kiln-drying them at a temperature of 103 °C േ 2 K until constant mass is achived. The moisture content u is determined from the ration between the mass of water in the moist specimen (mu-mdr) and the mass of the kiln-dried specimen (mdr). Investigations on the moisture gradient in timber elements are possible but difficult since this necessitates the extraction and segmentation of specimen without influencing the moisture content. The method is standardized, see [25]. Since this method is a destructive method and rather time-consuming, it is less suitable for in-situ investigations. One common method to determine timber moisture content in situ is the dielectric / capacitative method. Wood changes in proportion to its moisture content, i.e. its dielectric constant increases with increasing moisture content. For 195 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS measurements, a condensator is placed on the wood surface, the wood acts as dielectric, see Fig. 13. The meters do not penetrate the wood material, i.e. only measurements of the average wood moisture content near the surface (< 35 mm) are possible, measurement of a moisture gradient is impeded, see Fig. 15. The method is standardized, see [26] and delivers an acceptable accuracy for wood moisture contents from 2 % up to the fibre-saturation point [27], [28], although temperature considerably affects the dielectric properties of wood [30]. Fig. 13 Commercially available device using the capacitative method, from [24] Fig. 14 Commercially available device using the resistance method, from [24] Fig. 15 Schematic of areas measured by capacitative method, from [24] Fig. 16 Schematic of areas measured by resistance method using insulated and noninsulated electrodes, from [24] The most commonly applied method to determine timber moisture content in situ is the resistance method with hand-held moisture meters, see Fig. 14. Since water has a much higher conductivity than wood, the electrical resistance decreases with 196 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS increasing moisture content [29]. In practice, two electrodes are rammed into the wood or attached to the surface with a defined distance of usually 30 mm between them and the resistance to electrical current is measured between them. The electrodes should be teflon-insulated to measure moisture content in clearly defined depths of the cross-section, see Fig. 16. This allows for collecting moisture content readings at multiple depths (e.g. 10, 30 and 50 mm) to evaluate moisture gradients. The method is standardized, see [31] and delivers an acceptable accuracy of ± 1,0 % for wood moisture contents between 6% and the fibre-saturation point (28 % - 30 %). Above the fibresaturation point, the accuracy decreases considerably. Below 6 %, the electrical resistance reaches very high values which are challenging to measure. Another factor influencing the electrical resistance of wood is the material temperature, see Fig. 17. The resistance decreases with increasing temperature, see e.g. [27], [28]. Moisture readings can also be affected by species and direction of measurement (parallel or perpendicular to grain). If the wood contains salts, terpens, oils or preservatives, the resistance-measurementmethod is not adequate and should be replaced by the distillation method [27]. Fig. 17 Influence of wood MC (x-axis) and temperature on electrical resistance of wood (y-axis) , from [28] Fig. 18 Influence of wood moisture content on select wood properties, from [27] 2.3 Evaluation of the effect of environmental conditions Changes in wood moisture content lead to changes of virtually all physical and mechanical properties (e.g. strength and stiffness properties) of wood, see Fig. 18. The existence of high moisture content can initiate decay or growth of fungi. Another effect of changes of the wood moisture content is the associated shrinkage or swelling of the material. Shrinkage and swelling are significantly more pronounced in radial and tangential direction than in 197 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS longitudinal direction. Since the outermost sections of the wood cross-sections will adapt to the climatic conditions at first, the resulting moisture gradient and the associated shrinkage or swelling will lead to equilibrium of internal compression and tension perpendicular to the grain stresses in the crosssection. Although these stresses are partly reduced over time by relaxation processes, an excess of the tension perpendicular to the grain strength results in instant stress relief in form of cracks, see Fig. 19. In case of shrinkage of the cross-section, the cracks will appear on the surface of the cross-section, in case of swelling of the cross-section, the cracks can develop inside the cross-section. The effect is more pronounced in larger cross-sections, for example large or block-glued glulam members. When the free shrinkage or swelling of the member is restrained, due to e.g. fasteners or reinforcing elements, the equilibrium of internal stresses is suspended, resulting in larger stresses and correspondingly larger, deeper cracks, see Fig. 20. Moisture gradient ∆uoutside ∆uinside Stresses perp. to grain Initial MC t = 0 Moisture gradient 0 < t < ∞ σt,90 σc,90 Equilibrium MC t = ∞ ft,90 Fig. 19 Schematic of moisture gradient (left) due to changed environmental conditions and resulting stresses perpendicular to the grain due to shrinkage (right) Moisture gradient ∆uoutside ∆uinside Stresses perp. to grain Initial MC t = 0 Moisture gradient 0 < t < ∞ Equilibrium MC t = ∞ σt,90 ft,90 Fig. 20 Schematic of moisture gradient (left) and resulting stresses perpendicular to the grain in case of restrained free shrinkage (due to e.g. connections) of the timber beam (right) 198 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Low or high moisture contents or severe changes of the same can sometimes be attributed to local conditions (e.g. roof leakage) but in the majority of cases, they can be explained by the climatic conditions, depending on the construction type and use of the building, and seasonal variations of the building climate [32]. Hereby it has to be differentiated between (see Fig. 21) changes of moisture content between the various phases of processing and shape until the timber element is finally subjected to the environmental conditions during operation of the building seasonal changes of moisture content due to seasonal changes of environmental conditions during operation of the building changes in climatic conditions due to temporary interventions (e.g. renovations) or changes of use (temporary or permanent) of the building Fig. 21 Sketch of a possible „moisture chain“, i.e. exposure to moisture from the tree to gluedlaminated timber elements in the building In closed, insulated and heated buildings (e.g. living spaces, office spaces, gymnasiums, production and sales facilities), featuring constant but dry climate, the most severe change of timber moisture content will mostly occur during the first winter of operation, after assembly and closure of the building. Here, surface treatment e.g. in the form of products which damp the moisture absorption and release in the first years of operation of the building could be a means to counter fast drying of newly installed elements. Strong but periodic changes of moisture content can occur in buildings with seasonal change of use (e.g. ice-skating rinks) or in buildings with a considerable influence of the outdoor climate on the indoor climate (e.g. unheated and non-insulated buildings like riding rinks, stables, warehouses). For this group, the application of insulation on the roof could help to 199 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS dampen the strong changes of indoor climate and correspondingly the timber moisture gradients. In case of temporary interventions or changes of use, care should be taken during such interventions to realize a dampened and controlled change of moisture content (e.g. in form of evaporation basins or surface treatment). For a more detailed description of these effects, the interested reader is referred to [32]. References [1] Hetzer O., Patentschrift Nr. 197773 vom 22. Juni 1906: Gebogener Holz-Bauteil für vereinigte Dach-Pfosten und-Sparren, Kaiserliches Patentamt, Berlin, 1906. [2] Dietsch P., Köhler J. (eds), Assessment of timber structures, Shaker Publishing Company, Aachen (Germany), ISBN 978-3-8322-9513-4, 2010. Dietsch P., Tannert T., “Assessing the integrity and strength of gluelines”. This publication. DIN 4074-1, Strength grading of wood – Part 1: Coniferous sawn timber, DIN, Berlin, 2008 [3] [4] [5] Talke D., Capturing cracks in timber constructions with the David laserscanner, Bachelor Thesis, Chair of Timber Structures and Building Construction, Technische Universität München, 2011. [6] Sanabria Martín S. J., Air-coupled ultrasound propagation and novel non-destructive bonding quality assessment of timber composites, Dissertation, ETH Zurich, 2012. [7] Bucur V., ”Ultrasonic Imaging”. In: Nondestructive Characterization and Imaging of Wood. Springer, Berlin. 2003, pp. 181–213. [8] Kasal B., Lear G., Tannert T., „Stress Waves“, in: Kasal B., Tannert T. (eds): In Situ Assessment of Structural Timber, Springer, ISBN 978-94-007-0559-3, 2011 [9] Hasenstab A., Integritätsprüfung von Holz mit dem zerstörungsfreien Ultraschallechoverfahren, Bundesanstalt für Materialforschung und –prüfung BAM, Dissertationsreihe Band 16, Berlin, 2006. [10] Krautkraemer J., Krautkraemer H., Werkstoffprüfung mit Ultraschall, Springer, Berlin, 5th edition, 1985. [11] Dill-Langer G., Aicher S., “Non-destructive detection of glue line defects in glued laminated timber”, WCTE 2008 Conference Proceedings, Miyazaki, Japan, 2008. [12] Raj B., Jayakumar T., Thavasimuthu M., Practical Non-Destructive Testing, 2nd ed. Woodhead Publishing, Abington, UK, 2002. [13] Kasal B., Lear G., Anthony R., “Radiography” in: Kasal B, Tannert T. (eds): In Situ Assessment of Structural Timber, Springer, ISBN 978-94-007-0559-3, 2011. [14] Bucar V., Nondestructive Characterization and Imaging of Wood, Springer, Berlin, 2003. [15] Kasal B., Anthony R., “Advances in in-situ evaluation of timber structures”, Progress in Structural Engineering and Materials, Vol. 6, No. 2, 2004, pp. 94-103. [16] Dietsch P., Kreuzinger H., Winter S., “Design of shear reinforcement for timber beams”, CIB-W18/ 46-7-9, Proceedings of the international council for research and innovation in building and construction, Working commission W18 – timber structures, Meeting 46, Vancouver, Canada, 2013. 200 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS [17] Frech P., „Beurteilungskriterien für Rißbildungen bei Bauholz im konstruktiven Holzbau“, Bauen mit Holz, Vol. 89, No. 9, 1987, pp. 582-585. [18] Erler K., Alte Holzbauwerke Beurteilen und Sanieren, 3.Auflage, Verlag Bauwesen, Berlin, 2004. [19] Radovic B., Wiegand T., „Oberflächenqualität von Brettschichtholz“, Bauen mit Holz, Vol. 107, No. 7, 2005, pp. 33-38. [20] Blaß H.-J., Brüninghoff H., Kreuzinger H., Radovic B., Winter S., Guideline for a First Evaluation of large-span Timber Structures, Council for Timber Technology, Wuppertal, 2006. [21] Dietsch P., Einsatz und Berechnung von Schubverstärkungen für Brettschichtholzbauteile, Dissertation, Technische Universität München, 2012. [22] Dietsch P., & Schänzlin J., personal communication, 17.8.2010. [23] Brüninghoff H., “Effects of (seasonal) changes in Environmental Conditions on structural Timber Elements”, in: Dietsch P., Köhler J. (eds.): Assessment of timber structures, Shaker Publishing Company, Aachen (Germany), ISBN 978-3-8322-9513-4, 2010. [24] Dietsch P., Franke S., Franke B., Gamper A., “Methods to determine wood moisture content and their applicability in monitoring concepts”, Journal of Civil Structural Health Monitoring, Vol. 4, No. 3, 2014 [25] EN 13183-1:2002, Moisture content of a piece of sawn timber - Part 1: Determination by oven dry method, European Committee for Standardization CEN, Brussels, Belgium, 2002. [26] EN 13183-3:2005, Moisture content of a piece of sawn timber - Part 3: Estimation by capacitance method, European Committee for Standardization CEN, Brussels, Belgium, 2005. [27] Kollmann F., Coté W. A., Principles of Wood Science and Technology I: Solid Wood, Springer, Berlin, 1968. [28] Niemz P., Physik des Holzes und der Holzwerkstoffe, DRW-Verlag, LeinfeldenEchterdingen, 2003. [29] Villari E., Annalen der Physik und Chemie - Untersuchungen über einige Eigenschaften des mit seinen Fasern parallel oder transversal durchschnittenen Holzes, Bd. CXXXIII, Leipzig, 1886. [30] James W.L., “Fundamentals of hand held moisture meters: An outline”, Proceedings of ASTM Hand-held Moisture Meter Workshop, Forest Products Society, Madison, WI, 1994, pp. 13–16. [31] EN 13183-2:2002, Moisture content of a piece of sawn timber - Part 2: Estimation by electrical resistance method, European Committee for Standardization CEN, Brussels, Belgium, 2002. [32] Dietsch P, Gamper A, Merk M, Winter S, “Monitoring building climate and timber moisture gradient in large-span timber structures”, Journal of Civil Structural Health Monitoring, Vol. 4, No. 3, 2014. 201 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS 202 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS Estimation on-site of decay in timber structures by means of penetration methods Alessandra Gubana1), Ezio Giuriani2) 1) DICA, University of Udine, Italy, [email protected] 2) DICATA, University of Brescia, Italy, [email protected] Summary The problem of the evaluation on-site of decay in timber structures can be faced from different points of view and reliable information are necessary to decide on the structural adequacy, the possibility of preservation, the kind of the eventual strengthening intervention or the need of substitution. The assessment of in situ timber members is always firstly based on visual inspection, the information so obtained can be deepen by several techniques proposed and applied to locate and quantify deterioration, such as sonic and ultrasonic techniques [1], application of electromagnetic waves [2], resistance drilling [3], screw resistance [4], hardness test [5], pylodin [6] and penetration test [7]. Correlations to predict mechanical properties are also disposable in literature, but not always strong or reliable [8]. An organic and extensive state of the art is reported in [9]. Among all these different tests, those based on penetration into the cross section of structural elements seem to be particular interesting for the structural assessment, as the information obtained can be useful and sufficient to check and verify the load bearing capacity of timber elements. Penetration tests in general can give information about the layers decay, as the response of wood to the penetration is different in relation to the density of the material. The presence of decay, due to organic attacks or moisture variations or any other causes, in generally alters this material property. Moreover, when it is necessary to check the deformation or the bearing capacity of a timber beam, it is important to know the cross section stiffness, which is determined by the dimensions of the base and the depth of the beam. So if a structural element is affected by external decay, and if its deepness is known, it is possible to rely only on the dimensions of the no decayed internal part of the cross section. As it is well known, the inertia dependence on the beam depth size varies with the third power and an error in computing this dimension has a relevant consequence on the final evaluation. 203 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS On the other hand, if the decay is not superficial, but only internal, the penetration up to the core or across the section can reveal inside decay which do not appear during the visual inspection. All the penetration techniques tries to give this information, even if some are more suitable for the structural assessment. The results of every test herein described is affected by the influence of the different angles of inclination of the pin penetration. The pylodin technique consists in the measure of the penetration of a thin rod after only one constant energy blow: this means that if the external layer density is high, the penetration length is small and the other way round. In this case the response is just a medium of the consistency of the different layers crossed by the rod. Screw-withdrawal tests resistance consists in the measure of the required force to pull out a screw of 4 mm diameter and 18 mm length and it can be similarly put in relation with the decay of the layers crossed by the screw itself. Different length can be used to explore deeper inside. As in the pylodin test, the results correspond to a medium values of the characteristics of the crossed layers. Resistance drills use small diameter needle-like drills to bore into timber members and it measures the resistance the drill bit encounters as a function of the penetration depth. The results are given in terms of graphs, where peaks correspond to higher resistance or density, while lowest points are associated with lower response and are index of possible decay. Experience is necessary to correctly interpreter the result data. The pushing pin device [10] is based on the same principle, as a pin is gradually pushed into the timber perpendicular to the surface by rack and pinion gear, driven by two opposite manual cracks moved by hands. The device is equipped with a linear magnetic position sensor and a force sensor, which allow to measure the progress of the force and the displacement of the pin. The so called Wood Penetration test [7,8] can be regarded as an extension to timber structures of the dynamic soil penetration test, as it is based on the insertion into timber structural members of a steel graduated rod, which advances by means of repeated constant energy blows transmitted by a rebound hammer. The test makes possible to distinguish between different degrees of decay as a function of the number of blows necessary for each centimetre layer penetration. This technique proved to be effective and reliable for investigating the extent and depth of wood decay. The test was frequently proposed and adopted in Italy and several ancient building timber structures were checked by means of this methodology. The test is easy to perform and the output data, shown in terms of penetration histograms, which vary along the penetration depth (Fig.1), can be interpreted very clearly by structural engineers: it is so possible to determine the depth of the decayed layers and consequently the reliable dimensions of the resisting timber sections. 204 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS (a) (b) Fig. 1. (a) State of decay of a timber truss arch; (b) Penetration test results (from [7]). In conclusion all the penetration tests are useful to investigate the resistance opposed by wood to the penetration of thin rods, and a simple and clear information about the depth and the position of the decayed layers can be taken from the output data or graphs in a less easy or easier way, depending on the instruments involved. 205 PART III - ASSESSMENT OF THE INTEGRITY OF STRUCTURAL TIMBER MEMBERS In most cases for timber beam and timber elements structural assessment this information is more important and decisive than the precise knowing of timber strength resistance or elastic modulus. Acknowledgments The present paper is a result of the activities of COST FP1101 Action “Assessment, Reinforcement and Monitoring of Timber Structures”. References [1] R.J. Ross, R.F. Pellerin, Nondestructive testing for assessing wood members in structures: a review. Gen.Tech.Rep. FPL-GTR-70, US Department of Agriculture, Madison, WI, Forest Product Laboratory, 1991. [2] M. Lualdi, L.Zanzi, and L.Binda, Acquisition and processing requirements for high quality 3D reconstruction from GPR investigations, Proceedings NDT-CE International Conference, 2003. [3] F. Rinn, Resistographic inspection of building timber, Proceedings Pacific Timber Engineering Conference, Gold Coast, Australia,1994. [4] Z. Cai, M.O. Hunt, R.J. Ross, L.A. Soltis, Screw withdrawal – A means to evaluate densities of in-situ wood members, International Symposium on NDT of Wood, Richmond, USA, (2002), pp.277-281. [5] J.G. Sunley, A comparison of the Janka and Monnin methods of testing the hardness of timber and wood products, J.Inst. Wood Science, 14 (1965), pp.40-46. [6] P. Hoffmeyer, The Pilodyn Instrument as a Non-Destructive Tester of the Shock Resistance of Wood, Proceedings of the 4th Symposium on the non-destructive testing of wood, Wash-ington State University, 1978 , pp.47-66. [7] E. Giuriani, A. Gubana, A penetration test to evaluate wood decay and its application to the Loggia monument, RILEM Materials and Structures, 1993, 26, 8-14. [8] E. Giuriani, A. Marini, S. Cominelli, A. Gubana, The Penetration Test to Evaluate Wood Decay after 20 Years Timber Structure Assessment Experience, Proceedings of SHATIS 2013, Trento, 2013. [9] B. Kasal, T. Tannert, In Situ Assessment of Structural Timber, State of the Art Report of the RILEM Technical Committee 215-AST, 2010. [10] M.Kloiber, J.Tippner, V.Hermankova, J.Stainbruch, Comparison of results of measuring by current NDT methods with results obtained through a new device for wood mechanical resistance measuring, Proceedings of SAHC 2012, Wroclaw, pp.2035-2043. 206 PART IV CASE STUDIES 207 PART IV- CASE STUDIES 208 PART IV- CASE STUDIES Assessment through NDT of the state of timber structures of the historic buildings of Catalonia Marcel Vilches Casalsa, Carles Labèrnia Badiaa and Vladimir Rodríguez Trujillob a Catalan Institute of Wood (INCAFUST). Lab. and Technical unit of Lleida. Parc Científic i Tecnològic. Edifici H2 • E-25003 Lleida, Spain, [email protected], [email protected] b Timber Building Consultant. C/Fontrodona 1, AT 2a E-08004 - Barcelona, Spain, [email protected] Abstract The wood was the material most commonly used for the construction in cities and towns of Catalonia in the past, for this reason, nowadays a lot of diagnosis in timber structures are performed. The NDT, in the diagnosis of old buildings, help to complete the inspections, therefore in some diagnosis we have used NDT, like Microsecond timer or drilling resistance device, to improve the assessment conditions of the structure. In order to NDT are reliable previous studies of laboratory should be made, for getting warranty correlations. These correlations presented by different authors have been used in some inspections of old buildings in Catalonia, in which timber roofs and the floors of the buildings are analyzed with NDT. These methods have been a complement for deciding the strength class of the timber putted in the old buildings. Keywords Nondestructive techniques, timber structures, diagnosis, old buildings, Catalonia Introduction Historically, the timber has been the material most used for construction of the resistant structures (roof, floors, …). For this reason, a lot of rehabilitations of catalan historic buildings are performed in timber structures, that can be degraded by biotic pathologies. Nowadays, the development of the NDT for the evaluation of properties of timber also are used in the inspection of the structures as a complementary tool for deciding the strength class of timber. The main advantage of the NDT is that they don't produce damage in the examined sample and we can continue using the timber elements. The acoustic methods are most used in the diagnosis of timber, permitting to predict the modulus of elasticity with the transfer speed of the wave. The densitometers also are 209 PART IV- CASE STUDIES employed as NDT for determining the density of timber, so this physic property is a good indicator of the mechanic properties. In this case the estimations are in a point and his information is complemented by other methods, as ultrasonic or vibration techniques for calculating dynamic modulus of elasticity, which is a good estimator of the real elasticity of the material. Technicians and researchers, before using the NDT in the inspections, first have performed several studies in laboratory for obtaining good correlations between the values of the nondestructive methods and the properties of timber (MOR, MOE and density). Normally, for the acoustic methods are correlated the dynamic modulus of elasticity1 and the MOE2 and MOR3, but the Pearson correlation coefficients do not exceed the 80% [2, 4, 5, 6]. Although it is difficult to find higher correlations that give better warranties, it should be taken into account that these techniques must be a help to the inspections of timber structures. The case of the densitometers is similar, inasmuch the correlations between density and the values obtained of the tool used can vary between the 50% and 70%. Methodology Species identification The timber specie identification of the inspections is performed through a macroscopic identification of a sample extracted in situ. The macroscopic description includes the observation of several characteristics of the timber to the naked eye or with help of a magnifier of 10x. The structure, size and form of the tissues are different in almost all timber species, so that every timber specie can be avowed. Xy-lotheque samples are used for the macroscopic description, with the three cutting planes: transversal, radial and tangential. Moisture content The moisture content in the inspections is determinate with a xylohygrometer of electrical resistance (FMW), that permits obtaining the moisture content of the timber with a microprocessor and we can know the moisture quickly. This tool has a sensor on top and measures the moisture content holding the sensor on the timber element. The measuring range of the humidity is 2 to 30%, with a resolution of 0.1% and an accuracy of 0.5%. The measuring depth is 10 to 20 mm, adjustable to intervals of 1 mm. 1 Edyn =ρ(v2 ) ρ=Density,v=wave speed 2 MOE=A+B·Edyn 3 MOR=A+B·Edyn 210 PART IV- CASE STUDIES Determination of density For the determination of density we used a drilling resistance device, model IML Resi F300S. This tool is an electrical drill that is introduced, with a constant speed, in the timber and it measures the degree of resistance offered. It is a good technique for the inspection of service structures. The drill does holes of 3 mm of diameter. Normally, it is used to verify the status of certain critical points, as the inspection of hidden timber parts, which building are sensitive to the material loss, thus decreasing the strength capacity. Determination strength properties Another tool used is the Microsecond Timer (FAKKOP), which is based on the generation of the impact waves, with a frequency of resonance of 23 kHz. The function of this tool is based on the higher absorption capacity of the impact waves of the wood degraded and the wood healthy. The impact waves are generated with the mechanical hammer impact on an electrical transmitter. The mean of the wave speed is performed with a timer and an electronic receptor that detects the transit time. Case of study Old Building at the Pyrenees This building, where teaching activities were performed, has an old construction and is distributed in ground floor, first floor, second floor and penthouse floor. Structurally is built with walls of load and horizontal floors with timber beams (Figure 1). Fig. 1 Exterior building front view and beams of the second floor 211 PART IV- CASE STUDIES In the inspection was observed that all timber of the structure was performed with the same specie, for this reason a wood piece of a beam was extracted for the specie identification. The identification showed that the genus of the specie was Pinus sp., probably Pinus sylvestris. The moisture content was determined with a contact hygrometer, obtaining humidity around 10% of the timber elements. So that, the characteristic values of elasticity will be modified for the 12% of humidity. The density, used for determining the dynamic modulus of elasticity, was determined in laboratory with beams that were not to the inspection. We made drilling resistance curves in areas free of defects, in eight beams of Scot pine, with similar dimensions and characteristics to the beams of the inspected building. We had these eight elements available in laboratory for an own characterization project and we used them for this analysis because we did not make the drilling resistance curves on the elements of the inspection in situ by unavailability of the drilling resistance device. The moisture content of the eight beams in the moment of drilling was approximately of 12% and the mean of coefficient of growth was of 6 mm by ring in each beam. With mean values of the drilling resistance, of the beams of laboratory, and the correlation obtained by Acuña et al. [1], for Pinus sylvestris, a density of 411 kg/m3 was consider for the inspected timber (Table 1). Table 1 Density values obtained with the mean values of the drilling resistance of different timber elements of Pinus sylvestris Timber elements Mean values of Drilling resistance (%) Density valuesa (kg/m3) Pinus sylvestris 13 23,34 412,53 Pinus sylvestris 21 38,06 423,71 Pinus sylvestris 22 18,52 408,87 Pinus sylvestris 23 25,51 414,18 Pinus sylvestris 81 15,42 406,51 Pinus sylvestris 81b 12,24 404,10 Pinus sylvestris 82 25,75 414,36 Pinus sylvestris 83 14,25 405,62 a Mean 411,24 ρ=394,797+0,7598·Drilling resistance Mean Value (r2 = 0,82) [1] With the density value can be calculated the MOEdyn, but this density will not be considered for the assignation of the strength class, as this property is not a limiting factor because it has higher values than 400 kg/m3. For this reason, in order to estimate the strength class of the timber inspected we decided to consider only the MOE and the MOR obtained with impact waves. The analyzed timber structure of Pinus sylvestris showed a good conservation, which has given an excellent structural functionality. We only found an excessive 212 PART IV- CASE STUDIES deformation in some beams of the first floor. This was originated by the prolonged action of humidity of the water tubing of the top floor. The other beams near the water tubings didn’t observe any degradation signs of the timber. In the penthouse we didn’t find any kind of alteration. Once the condition of the timber structure was valued positively we performed the assignation of the strength class with the help of the time-of-flight of ultrasonic waves values. Six pieces of timber were analyzed, two bottom chords, which formed the trusses of roof, two beams of penthouse and two beams of the second floor, and in each of them were measured three readings wave speed (Figure 2). The measures were performed on the central part of the timber pieces, with a distance between sensors of approximately two and three meters (Table 2). Fig. 2 Evaluation of the bottom chords of the trusses of roof with the el Microsecond timer Table 2 Values of time transmission, the mean value of the time and the wave velocity in each timber element analyzed Element Time 2 (µs) Time 3 (µs) Mean value Distance WaveVelocity (µs) (cm) (m/s) Bottom chord Penthouse 480 DEF 482 480 480,60 215 4.473,57 Bottom chord Penthouse 434 LLLM 435 435 434,60 217 4.993,10 Beam 4 Penthouse 315 314 315 314,60 171 5.435,47 Beam 5 Penthouse 331 332 331 331,30 177 5.342,59 Beam 11 Second 634 630 632 632,00 290 4.588,61 Beam 13 Second 664 663 662 663,00 283 4.268,48 Floor Time 1 (µs) 213 PART IV- CASE STUDIES These values of time-of-flight of ultrasonic waves were for determining the dynamic modulus of elasticity and with this value we can allocate the strength class using the equations of bending strength (MOR) and modulus of elasticity (MOE), published by Íñiguez (2007) for Scots pine. The bottom chord obtained a characteristic value of the bending of 23,49 N/mm2, of 35,14 N/mm2 for the beams of penthouse and of 20,83 N/mm2 for the beams of the second floor, assigning them respectively a class C22, C35 and C20. In return, the elasticity values limited the strength class of the inspected elements, obtaining characteristic values of 7.404 N/mm2 for the bottom chords, 9.403 N/mm2 for the beams of penthouse and 6.541 N/mm2 for the beams of the second floor, assigning them respectively a class C14, C18 and C14 (Table 3). Table 3 Wave speed, mean modulus and bending values of each element. Characteristics values of Mean modulus and bending. Strength class assigned MOEdyna (N/mm2) MOEb (N/mm2) MORc (N/mm2) Bottom chord Penthouse 8.230,09 DEF 6.655,74 23,14 Bottom chord Penthouse 10.252,63 8.151,82 LLLM 30,02 Beam 4 Penthouse 12.149,83 9.555,19 36,47 Beam 5 Penthouse 11.738,13 9.250,65 35,07 Beam 11 Second 8.658,79 6.972,85 24,60 Beam 13 Second 7.492,75 6.110,33 20,64 Element a b Floor MOEd (N/mm2) MORe (N/mm2) Strength class 7.403,78 23,49 C14 9.402,92 35,14 C18 6.541,59 20,83 C14 Edyn =ρ v2 ρ=411kg/m3 ,v=wave speed MOE=A+B·Edyn =579,5+0,7548·Edyn (r2 = 0,74) [4, 5] c MOR=A+B·Edyn =-4,84+0,0034·Edyn (r2 = 0,60) [4, 5] Mean values e 5th percentile values d We didn't use the visual grading for allocating the strength class because the timber elements of the penthouse were hidden by the ceiling and we couldn't see the singularities of timber. The beams of the first and second floor were painted and we neither could see the defects of timber. 214 PART IV- CASE STUDIES Conclusions Nowadays the speed of the wave transmission is, together with visual classification, the NDT technique more used. The disadvantage of these methods are the low correlations, because they don’t fulfill with the expectative. The values of the elasticity and the resistance prediction with the nondestructive variables are between 40% and 70% of the mechanical properties; however these techniques are a good complement for the rehabilitation of buildings with timber structure, to estimate a strength class of the timber elements. The drilling resistance device is a good tool for predicting biotic degradations in hidden areas and the difficult access areas, as the timber beams ends embedded in masonry walls. This tool also serves like estimator of the timber density, using the mean value of the drilling resistance curve as indicator [3, 6]. The results obtained by the authors reinforce the utility of this tool in the inspections, but it is necessary to use different NDT techniques for getting an adequate diagnostic. Bibliography [1] Acuña, L.; Basterra, L.A.; Casado, Mª. M.; López, G.; Ramón-Cueto, G.; Relea, E.; Martínez, C.; González, A. (2011). Aplicación del resistógrafo a la obtención de la densidad y la dife-renciación de especies de madera. Materiales de construcción. Vol. 61, 303, 451-464 [2] Arriaga, F; Íñiguez, G; Esteban, M; Bobadilla, I. (2009) Proposal of a Methodology for the Assessment of Existing Timber Structures in Spain. Proceedings of the 16th International Symposium on Nondestructive Testing of Wood (pp. 145-151) [3] Casado, M; Pinazo, O; Martínez, C; Vegas, F; Pando, V; Acuña, L; Relea, E. (2005) Deter-minación de la capacidad resistente mediante métodos no destructivos. Aplicación en vigue-tas de forjado de un edificio singular. Actas IV congreso forestal español. 4CFE05[523] [4] Esteban Herrero, M., Arriaga Martitegui, F., Bobadilla Maldonado, I., Íñiguez González, G. y García Lantarón, H. (2009) Análisis y consolidación de la estructura de madera del edificio antiguo del aserradero de Valsaín, Segovia. Actas V congreso forestal español. 5CFE01-[614] [5] Iñiguez, G. (2007). Clasificación mediante técnicas no destructivas y evaluación de las pro-piedades mecánicas de la madera aserrada de coníferas de gran escuadría para uso estructural. Tesis Doctoral. UPM. Escuela técnica superior de ingenieros de montes [6] Ramón, G; Basterra, A; Casado, M; Acuña, L. (2005) Analysis of the structural timber diagnosis techniques at the cultural patrimony with an architectural project orientation. I Jornadas de investigación en construcción. Tomo 1 215 PART IV- CASE STUDIES 216 PART IV- CASE STUDIES SDT methods as part of a conservation process Dulce Franco Henriques1*, André Santiago Neves1 1 Civil Engineering Departament, ISEL - Instituto Superior de Engenharia de Lisboa, Portugal. * corresponding author: [email protected] Abstract This paper refers to the assessment on site by SDT (semi-destructive testing) methods of the consolidation efficiency of a conservation method developed by [1]. This is a solution for improve the physic and mechanical characteristics of wood moderately degraded by fungi, avoiding its substitution and contributing to the conservation of building heritage. The decay level and the evaluation of the proposed solution efficiency were checked on site by SDT methods of drill resistance and of penetration resistance. The objective was to assess the consolidation efficiency on site by SDT. The technique involves traditional methodologies used in the conservation of wooden cultural heritage area applied to wooden elements in buildings. This study set out to ascertain on site the mechanical performance of scots pine (Pinus Sylvestris L.) wood degraded by fungi after treatment with a biocide product followed by consolidation through impregnation with a polymeric product. The SDT methods used showed good sensitivity to the presence of the products and could evaluate their effectiveness. Introduction This conservation process was developed in order to help keeping the timber in buildings that lies slightly deteriorated but yet has strength capacity determined on site. The process of consolidating degraded timber by impregnation consists of forcing a specific fluid material into it, which when hardened will restore its integrity and improve the physical and mechanical characteristics [2-4]. In addition to strengthening the wood structure, the materials used may also provide some protection against biological pests [5,6]. However it was found that synthetic consolidants, including epoxies, do not significantly increase the resistance of wood against fungi [5-7]. So the application of biocides before or with the consolidant became necessary and the use of boron was a possibility because of its good fungicide and insecticide properties [8,9]. The pair of products which showed the best mechanical results by laboratory tests was an epoxy consolidant and a boron-based biocide [10-12]. 217 PART IV- CASE STUDIES After that it was necessary to evaluate the efficiency of the method in wooden elements in buildings [10]. This evaluation was done using the SDT methods of drill resistance and of penetration resistance due to the superficiality of the consolidation (up to 15 mm) and to the necessity of some tools sensitive to that. The drill resistance device has been seen as a reasonable tool to evaluate mechanical characteristics of timber, even though that was not its original objective [14], nor its most usual application field. Due the sensibility of the tool several authors have recently been evaluating wood properties like the density of some species with the drill resistance equipment in laboratory conditions to estimate this characteristics in timber applied on site [10,14-17]. The mechanical strength and modulus of elasticity have also been correlated with the drill resistance results [14-16]. The penetration resistance technique is also applied to evaluate the surface physic-mechanical characteristics of timber as well as the level of damage of the timber, which depends on its surface hardness and density [10,15,17]. Case study This case study presents the in situ experimental conservation process performed on six moderately degraded sections of structural timber elements from a XIX century palace: three floor beams, a staircase, a wall and a roof beam. In every case the degradation was located in a small part of the element with an extent generally lower than 80 cm. The laboratorial development of the process considered it applicable to wood degraded by fungi, with mass losses lower than 20%. This value is regarded as a limit for the intervention success. For higher values of mass loss, laboratory tests indicated that the resistance was lower than the minimum structural class of Scots Pine [1,18]. The evaluation of the local timber elements condition was made with a drill resistance device and with an penetration resistance device before and after the treatment and consolidation application. The main goals of the use of nondestructive techniques in situ were the evaluation of the local degradation condition [19,20] as well as a physical / mechanical efficiency evaluation of the applied treatment and consolidation products. Materials and Methodology Treatment and Consolidation The process consists on an initial application of a boron-based aqueous biocide (Bora-care® - Nisus Corporation). On a second stage, and after the stabilization of 218 PART IV- CASE STUDIES the water content, the two component consolidation product is applied (EPO 155 ® + K 156® - C.T.S. Srl.). This pair of products was selected among others with a similar individual efficiency, because they proved to have the best joint mechanical efficiency [1,11,12]. Both products were applied on the timber elements by brush (Fig.1). It is also possible to resort to injections whenever it is justifiable [10]. In each of six timber element to be analyzed, three analysis zones were determined: in sound wood (zone C), to control, moderately degraded by fungi (Zone A) and heavily degraded by fungi (Zone B), for comparison Fig. 1. Application of consolidant a) Wall; b) Staircase; c) Pavement beam 1 [18] Evaluation tools Aiming to identify local timber elements condition, drill resistance and penetration resistance equipments were used. To assess the increase of mechanical strength after applying the proposed method, the devices were used before and after the treatment and consolidation application. As verified by [1], the penetration depth of consolidation product is in the order of 10-15 mm. Therefore, the drill resistance measure was determined in an extension of 10 mm for nonstructural elements and 15mm for structural elements, always excluding the initial 2 mm, considered as a perturbation zone. It was verified that drill resistance equipment allowed the identification of strength increase through the density profiles analysis [18]. By a comparative analysis penetration resistance equipment also allows the identification of strength increases, identified by a reduction of the penetration depth. Results The results are presented through medium values comparing the situation before and after treatment and consolidation in each timber element moderately degraded by fungi. 219 PART IV- CASE STUDIES Comparing C and A zones is possible to get a rough idea of timber decay levels through both drill resistance and penetration resistance methods, but was no possible to quantify it because of the great variability of results obtained [10,18]. Also with C and B zones, used as references, it is possible to see the significance of the resistance gain after the application of the process. In fact, as shown in table 1, the values of zone A after the treatment and consolidation, in a great number of the cases, approached the registered value for sound wood (zone C). Table 1 - Summary results of tests performed Timber Properties – mean values Element Zone A moderately degraded Initial Wall Staircase Timber beam 1 Timber beam 2 Timber beam 3 Roof beam Moisture content (%) Drill resistance Penetration resistance (mm) Moisture content (%) Drill resistance Penetration resistance (mm) Moisture content (%) Drill resistance Penetration resistance (mm) Moisture content (%) drill resistance penetration resistance (mm) Moisture content (%) Drill resistance Penetration resistance (mm) Moisture content (%) Drill resistance Penetration resistance (mm) 5 8,5 10 6,4 14,1 7 11,8 14,8 9 10,8 19,7 9,5 9,1 24,4 9,5 9,4 19,3 Treated and consolidated 5 9,2 10 8,7 11,4 8 15,6 13,9 9 11,1 18,2 9 12,3 19,1 9 11,1 18,4 Property variation 0% 8% 0% 36% -19% 14% 32% -6% 0% 3% -8% -5% 35% -22% -5% 18% -5% Zone B (heavy degr.) Initial Zone C (sound) 2 6,3 7 1,0 17,8 3 7,0 21,3 8 8,2 37,3 8 5,98 38,1 7 5,8 34,3 12 13,1 12,3 9 11,6 11,4 7 12,8 16,2 8,5 11,7 16,6 9 10,3 18,0 Initial The penetration resistance and the drill resistance measurements are affected by moisture content and to obtain correlations of those values with wood properties one must adjust the measurement to a common wood moisture content, such as 12% [21]. For the purpose of this study the goal was to equilibrate de MC for the initial conditions to be possible to do the value comparison in almost the same conditions. The rise in the drill resistance measurements and the decrease in penetration depth, point to the increase in mechanical strength after the application of the conservation process proposed. Unable to perform the penetration resistance test on the wall because this element was not supported, which influences the results. For other elements a tendency 220 PART IV- CASE STUDIES to decrease of the penetration resistance penetration was generally verified, which indicates a gain of mechanical resistance. Final comments The SDT methods of drill resistance and penetration resistance were very important auxiliary instruments to assess and confirm on site the results obtained in laboratory for the treatment and consolidation process [18]. Conclusions of the case study: • Efficiency of consolidation by impregnation as a technique of local mechanical strength increase of wood moderately degraded by fungi, applied after the biocide treatment; • SDT drill resistance and penetration resistance as methods suitable for assessment of consolidation efficiency levels; • Good sensitivity of the methods to the superficiality of the conservation method (up to 15 mm); • Suitability application of that technique on site. Acknowledgments The authors would like to thank the Foundation for Science and Technology (FCT) for the financial support in the CONSERV-TIMBER project (ref. EXPL/ECM-COM/ 0664/2012). Also would like to thank East-Banc, owner of the building for their willingness. References [1] Henriques, M. D., 2011. Treatment and consolidation of pine wood degraded by fungi in structural elements of ancient buildings. (In portuguese). PhD Thesis. Lisboa: Instituto Superior Técnico. [2] E. Schaffer, 1074, Consolidation of painted wooden artefacts, Stud. in Conserv. 19, 212-220. [3] J.R. Loferski, 2001, Technologies for wood preservation in historic preservation, Archives and Museum Informatics 13, 273-290. [4] S.M. Nakhla, 1986, comparative study of resins for the consolidation of wooden objects, Studies in Conservation, 31, 38-44. [5] A. Unger, W. Unger, 1994,Conservation of wooden cultural property, Proceedings of The International Research Group on Wood Preservation, IRG/WP 94-30038, Bali, Indonesia. [6] A. Unger, A.P. Schniewind, W. Unger, 2001, Conservation of wood artefacts - A handbook, Springer-Verlag, Germany. [7] J.-D. Gu, 2003, Microbiological deterioration and degradation of synthetic polymeric materials: recent research advances, International Biodeterioration & Biodegradation, 52, 221 PART IV- CASE STUDIES 69-91. [8] F.C. Jorge, L. Nunes, C. Botelho, 2004, Boron in wood preservation: problems, challenges and proposed solutions. An overview on recent research. Journal of the Faculty Science Technology, University Fernando Pessoa 1, 3-15. [9] S.N. Kartal, W.J. Hwang, K. Shinoda, Y. Imamura, 2006, Laboratory evaluation of boroncontaining quaternary ammonia compound, didecyl dimethyl ammonium tetrafluoroborate (DBF) for control of decay and termite attack and fungal staining of wood. Holz Roh – Werkstoff, 64, 62–67. [10] Henriques D.F., Nunes L., Brito J. de, 2011 “An experimental approach to the treatment and consolidation of degraded timber elements from a XIX century building”. SHATIS – International Conference on Structural Health Assessment of Timber Structures. LNEC, Lisbon, Portugal, pp. 47-48; [11] Henriques, D., Brito, J., Duarte, S. & Nunes, L., 2013a. Consolidating preservativetreated wood: Combined mechanical performance of boron and polymeric products in wood degraded by Coniophora puteana. Journal of Cultural Heritage, 15, 10-17. [12] Henriques, D., Nunes, L. & Brito, J., 2013b. Mechanical evaluation of timber conservation processes by bending tests. Advanced Materials Research, 778, 612-619. [13] Rinn, F. 1994, ‘One minute pole inspection with RESISTOGRAPH micro drillings’, in Intern. Conf. on wood poles and piles, March 21-23, Fort Collins, Colorado, USA. [14] Feio, A., 2006. Inspection and Diagnosis of Historical Timber Structures: NDT Correlations and Structural Behavior. PhD Thesis. Braga: Universidade do Minho. [15] Palaia, L., Monfort, J., Sánchez, R., Gil, L., Álvarez, A., López, V., Tormo, S., Pérez, C., Navarro, P., 2008, ‘Assessment of timber structures in service by using combined methods of non-destruct testing together with traditional ones’, 9th Inter. Conf. on NDT of art, Israel. [16] Branco, J.M., Piazza, M., Cruz, P.J.S. 2010, ‘Structural analysis of two King-post timber trusses: Non-destructive evaluation and load-carrying tests’, Con. Build. Mat, 24, 371–383. [17] Iniguez, G., Arriaga, F., Esteban, M., Bobadilla, I.González, C., Martinez, R., 2010. Insitu non-destructive density estimation for the assessment of existing timber structures. WCTE - Word Conference on Timber Engineering. [18] Neves, A. S., 2013. Assessment, treatment and consolidation of timber in ancient buildings (In portuguese). Master Thesis. Lisboa: Instituto Superior de Engenharia de Lisboa. [19] Tannert, T., Kasal, B. & Anthony, R., 2010. RILEM TC 215 In-situ assessment of structural timber: Report on activities and application of assessment methods. World Conference on Timber Engineering. Trentino, Itália: Curran Associates, Inc. [20] Machado, J., 2013. In situ Evaluation of the Reference Properties of Structural Timber Menbers. Use of Available Tools and Information. Structural Health Assessment of Timber Structures. Trento, Itália: Trans Tech Publications Ltd, Switzerland, 137- 144. [21] Kasal, B., Anthony, R., 2004, Advances in situ evaluation of timber structures, Prog. Struct. Eng. Mat.6, 94–103. 222 PART IV- CASE STUDIES Advanced model based assessment of existing timber structures Kiril Gramatikov1), Toni Arangjelovski2) and Marija Docevska3) 1) Prof. Ph.D., University "St.Cyril and Methodius"-Skopje 2) Assistant Prof. Ph.D., University "St.Cyril and Methodius"-Skopje 3) Ms.C. student, grad.civ.eng., University "St. Cyril and Methodius"-Skopje Introduction Assessment of the timber structures in R.Macedonia follows the procedure where proof load test was used to verify the available stress state and serviceability state of deflections. This procedure is given in the national standard MKS U.C9.300/1984 [1]. The knowledge and experience in the field of assessment of new and existing or damaged structures, gained from the past years gives us enough data to harmonize behaviour of existing structures according to the standard EN1995-1 as a special case of assessment known as design code assessment. For example the standard ISO13822 [2] gives instructions that structures designed and constructed based on earlier codes may be considered safe to resist loads if there is no evidence of significant damage, distress or deterioration, planned maintenance ensures sufficient durability and structure has demonstrated satisfactory performance for sufficiently long period of time for displacements. Despite this fact, for two case studies we have performed structural reliability verification, on the basis of the proof load test results. For this purpose we have used Level 3: Advanced Model Based Assessment given in Annex A of SAMCO F08a Guideline for the Assessment of Existing Structures [3]. Structural reliability analysis was performed for: • Glued laminated timbers Structure, Cambered beam span of L=24.00m BrewerySkopje • Glued Laminated Pedestrian Timber Bridge in Struga, Two-hinged arch, span of L=26.00m plus two simple supported beams span of L=12.5m each. For these structures design documents and data from serviceability test after observed damage and after construction by proof load test were available [4, 5 and 6]. The semi-probabilistic approach was used based on limit state principle to define partial safety factors. The targeted reliability level for the ultimate limit state 223 PART IV- CASE STUDIES and serviceability limit state was defined using the table C.1: Target reliability indices for assessment of existing structures [3]. For ultimate limit state reliability index β was set to β=4.27, for design working life (e.g.50 years) and for high consequences and probability of failure P f=10-5. For the irreversible serviceability limit state reliability index β=1.5 for the remaining working life and probability of failure Pf=10-1. These values are the same as given in the Eurocode EN1990. Reliability verification was done using the Reliability Based Code Calibration program "Code Call" developed by Joint Committee on Structural Safety [7, 8]. Case study: Cambered beam L=24.90m, Brewery Skopje First structure analyzed in this study is a roof glued laminated timber structure constructed for the Coca-Cola section of Brewery-Skopje, shown in figure 1. The structure is consist of cambered glued laminated timber beams, span of 24.00m, with curved intrados in the middle of the span, 6° slope on the extrados and 4.5° slope on the intrados. Fig. 1. Industrial building of Coca Cola section, Brewery Skopje One year after the construction, cracks parallel to the grain direction were appeared at the middle of the height where cambered beam is joined with the steel bracing near the supports. To obtain the accurate state of the stresses and deflec224 PART IV- CASE STUDIES tions, of damaged cambered beam, proof loading test was performed. The structure was loaded in ten different phases, but in this paper we have analyzed only the ninth phase, in which the test load simulates approximately 90% of the full value of snow load. The reliability index β was calculated for different values of partial safety factor for the material γM (1.0; 1.10; 1.20; 1.30). The results are given in Figure 2. Reliability index β for γM=1.20 and ratio between variable and total stresses α=0.74 (for this case) is 4.71. It means that probability of failure for β=4.71 is Pf=10-6. Fig. 2. Reliability index β for different values of γM as a function of stresses ratio α Case study: Pedestrian Bridge over Crn Drim River, Struga As a second case study in this paper, assessment of existing glued laminated pedestrian bridge over Crn Drim River in Struga was analyzed (Figure 3). The bridge is consist of two parallel main beams which are composed as twohinged arch beams with span of 25.70m and two single supported beams with span of 12.50m on both sides of the arch as access ramps. Proof load test was performed for variable load of 5KN/m2 which corresponds to design variable load. The test load was set in three unsymmetrical and four symmetrical phases of loading. We were considering only the two phases for which we obtaied maximum measured deflections. The reliability index β was determined for the coefficient α=0.84 according to the measured deflections from the permanent and variable load. For this value of α, reliability index β=1.50 was obtained as shown on the figure 4. For this value of β, the probability of failure Pf is 10-1. 225 PART IV- CASE STUDIES Fig. 3. Two hinged arch pedestrian bridge over Crn Drim river in Struga Fig. 4. Reliability index β for irreversible serviceability limit state of deflection for different values of α Conclusion From the results of reliability verification analysis, for the two cases of structures, following issues can be concluded: 226 PART IV- CASE STUDIES • For the two type of structure, the special case of assessment new code assessment EN1995 can be applied using Level 3: Advanced Model Based Assessment. • Analysis of ultimate limit state for the cambered beam L=24.00m, for the ratio of stresses α=0.74, reliability index β was calculated β=4.27 for value of partial factor for the materials γm=1.2 and for the loads γG=1.35 and γQ=1.5. • Proving irreversible serviceability state of deflections in the case of the pedestrian bridge, two-hinged arch, span of L=26.00m, reliability index was obtained β=1.5, for the given value of de-flections according to serviceability test after construction. • Structures designed and constructed by the old codes, which during the serviceability period have satisfactory behavior also fulfill the design criteria according to Eurocode EN1995. References [1] MKS U.C9.300/1984-Design of glued laminated timber structures, Technical requirements [2] SAMCO Final Report 2006, F08a Guideline for the Assessment of Existing Structures, Dr.W.Rucker, F.Hille, R.Rohrmann, Federal Institute of Materials Research and Testing, Division VII.2 Buildings and Structures, Unter den Eichen 87, 12205 Berlin, Germany. [3] ISO 13822 "Bases for design of structures - Assessment of existing structures", 2001 [4] K. Gramatikov, "Report on initial analysis for the state of stresses and deflections in the roof structure for the Coca-Cola section", Brewery Skopje, 1996 [5] Kiril Gramatikov, Experimental Testing and Assessment of the Bearing Capacity of GluLam Timber Structure at Skopje Brewery”, Report Faculty of Civil Engineering, 2002 [6] S.Atanasovski, K.Gramatikov "Assessment of the bearing capacity of glulam timber bridge in Struga", Report Faculty of Civil Engineering Faculty 2003 [7] Joint Committee on Structural Safety, Probabilistic Model Code, 12th draft version 2000, in-ternet version http://www.jcss.ethz.ch, 2014 [8] Joint committee on Structural Safety, CodeCal, Reliability Based Code Calibration program updated 12 June 2013, internet version: http://www.jcss.ethz.ch, 2014 227
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